Acta Crystallographica Section C
Acta Crystallographica
Section C STRUCTURAL CHEMISTRY

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STRUCTURAL
CHEMISTRY

Volume 49| Part 3

ISSN: 2053-2296

March 1993 issue

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inorganic compounds

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Structure de RbAlAs₂O₇

H. Boughzala, A. Driss and T. Jouini

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Cs₄Mo₂₁S₂₅: a new structure type containing Mo₉ and Mo₁₂ condensed clusters

P. Gougeon and M. Potel

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Structure of (NH₄)₃H(SeO₄)₂ in high-temperature phases I and II

K. Łukaszewicz, A. Pietraszko and M. A. Augustyniak

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Redetermination of the structure of barium peroxide by single-crystal X-ray diffraction

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Structure of dilithium tetraammonium cyclo-hexaphosphate tetrahydrate

O. S. M. M. Elmokhtar, M. Rzaigui and A. Jouini

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Structure of Nb₅(Ge_x,Sn_1−x)₂Ge, x = 0.25

M. Tanaka, H. Horiuchi, T. Shishido and T. Fukuda

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Single-crystal structure of K₃Nb₈O₂₁

A. Benabbas, M. M. Borel, A. Grandin, A. Leclaire and B. Raveau

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metal-organic compounds

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Seven-coordinate manganese(II) complexes of 2,6-bis[1-(2-hydroxyethylimino)ethyl]pyridine

S. Brooker and V. McKee

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Structure of μ-carbonato-1κ²O¹,O²:2κ²O¹,O³-bis[(acetylacetonato)(N,N,N',N'-tetramethylethylenediamine)nickel(II)] (acetylacetonato)aqua(methanol)(N,N,N',N'-tetramethylethylenediamine)nickel(II) tetraphenylborate

K. Yamada, K. Hori and Y. Fukuda

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Structure of acridinium trans-tetrachlorobis(dimethyl sulfoxide)ruthenate(III)

M. Calligaris, N. Bresciani-Pahor and R. S. Srivastava

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Structure of dichloro(2-pyrimidinol-κN,O)mercury(II)

M. Quirós and C. Enrique

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The first zwitterionic and bent-sandwiched hafnacarborane 4',5,5',6-Li(THF)-1,1'-commo-Hf(THF)Cl[2-(SiMe₃)-3-(Me)-2,3-C₂B₄H₄]₂

H. Zhang, L. Jia and N. S. Hosmane

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Low-temperature structures of catena-(bipyrimidine-N,N')bis(thiocyanato)copper(II) and poly-(μ-bipyrimidine-N,N',N'',N''')tetrakis(thiocyanato)dicopper(II)

G. De Munno, G. Bruno, F. Nicolò, M. Julve and J. A. Real

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Structure of the dinuclear platinum monohydrido bridged complex [(PEt₃)₂HPt(μ-H)PtH(PEt₃)₂][BPh₄]

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Structure of bis(dimethylammonium) bis(tetrabutylammonium) β-octamolybdate

Q. Wang, X. Xu and X. Wang

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Structure of tetrakis(μ-acetato)-bis(4-pyridylmethanol)dicopper(II)

N. N. Hoang, F. Valach and M. Melník

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Structure and solid-state tin-119 and tellurium-125 NMR spectra of 2,2,4,4,6,6-hexakis(trimethylsilylmethyl)cyclotristannatellurane

F. W. B. Einstein, I. D. Gay, C. H. W. Jones, A. Riesen and R. D. Sharma

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Structures of bis(triphenylphosphine)gold(I) hexafluorophosphate, [Au(PPh₃)₂]PF₆ (1), and bis(triphenylphosphine)gold(I) nitrate, [Au(PPh₃)₂]NO₃ (2)

R. J. Staples, C. King, M. N. I. Khan, R. E. P. Winpenny and J. P. Fackler Jnr

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Structures of {diethyl 2-[(8-hydroxy-κO-2-quinolyl-κN)methyl]malonato(2–)-κC²}(pyridine)palladium(II) and the analogous ethyl complex

A. Yoneda, G. R. Newkome, Y. Morimoto, Y. Higuchi and N. Yasuoka

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organic compounds

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Structure of a non-mesogen porphyrin, 5,10,15,20-tetrakis[4-(1-hexyloxy)phenyl]porphyrin

M. G. Walawalkar, M. Nethaji and V. Krishnan

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Structure of methyl 4-O-benzoyl-6-bromo-3-tosyl-2,6-dideoxy-β-D-arabino-hexopyranoside

M. J. Jedrzejas, R. J. Baker, R. W. Binkley, R. L. R. Towns, N. Adair, M. Andras, F. Anwari, Z. Chen, R. Huff, X. Liu, R. A. Martuch and M. Skladany

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A chloride of a substituted heterocyclic analogue of chrysene: C₁₉H₁₇N₂O⁺.Cl⁻

O. Johnson and D. W. Jones

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Structure du 11,11'-bi[3-éthylènedioxy-17β-cyano-5-hydroxy-17α-triméthylsiloxy-19-nor-5α-androst-9(10)-ène] monohydrate

D. Ginderow, G. Teutsch and J.-P. Mornon

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2,8-Diphenoxy-2,8-dithioxo-1,3,7,9-tetraaza-2λ⁵,8λ⁵-diphosphatricyclo[7.3.0.0^3,7]dodekan

U. Engelhardt and B. Stromburg

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Structure of the new electrophilic fluorinating agent 1-chloromethyl-4-fluoro-1,4-diazoniabicyclo[2.2.2]octane bis(tetrafluoroborate) and two of its monoquaternary analogues

R. E. Banks, I. Sharif and R. G. Pritchard

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Structure of N-acetyl-L-homocarnosine monohydrate

J. A. Campbell, A. A. Freer and D. J. Robins

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Structure of 2-phenyl-2-dehydrosparteine

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Structure of 1-{4-[2-(diethylamino)ethoxy]phenyl}-2-(4-methoxyphenyl)-1-phenylethan-1-ol, the non-steroidal antiestrogen MER25

M. B. Hossain, J. Symersky, S. C. Neely, D. van der Helm and R. A. Magarian

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Structure of (–)-β-hydrastine

Rajnikant, K. N. Goswami, V. S. Yadava, V. M. Padmanabhan and S. K. Banerjee

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2-Carboxybenzenediazonium chloride monohydrate

C. J. Horan, C. L. Barnes and R. Glaser

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Structure of an organic photochromic compound. 6,7,8a,9-Tetrahydro-17,17-dimethylnaphtho[1'',2'':5',6'][1,4]oxazino[3',2':2,3][1,4]oxazino[4,3-a][3H]indole

A. T. Hu, M.-S. Wang and S.-L. Wang

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Determination of the stereochemistry of oxandran-3-one; a novel methyltriterpene from Oxandra asbeckii (Annonaceae)

W. F. Tinto, L. C. Blair, A. J. Lough, S. McLean and W. F. Reynolds

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Functionalized hydrocarbons with condensed ring skeletons. XI. Tetramethyl tricyclo[8.4.0.0^2,7]tetradeca-1,8-diene-5,5,12,12-tetracarboxylate and its corresponding tetradec-8-ene

M. Drouin, N. Michel-Dewez and A. G. Michel

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Structure of (±)-egenine

P. Dokurno, M. Gdaniec, Z. Kosturkiewicz, D. Matecka and M. D. Rozwadowska

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Structure of ethyl phenyl selenone

H. Hoier, H. L. Carrell, J. P. Glusker and C. P. Spears

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Structure of the molecular complex of anthracene with 1,8:4,5-naphthalenetetracarboxylic dianhydride

H. Hoier, D. E. Zacharias, H. L. Carrell and J. P. Glusker

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Structure of 4-(5-cyano-2-furyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarbonitrile

J. Kožíšek, H. Paulus, Š. Marchalín and D. Ilavský

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Structure of 12b-hydroxy-5-methyl-1,2,3,4,4a,5,6,12b-octahydro-12H-benzo[a]xanthen-12-one

R. M. Letcher, K.-K. Cheung and T.-Y. Yue

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Structure of 5,6,11,12-tetrahydro-2,5,8,11-tetramethylphenomazine

S. M. Prasad, S. P. Narayan, D. K. Mandal and S. C. Gupta

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short format (metal-organic compounds)

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Dimanganese octacarbonyl complexes with bridging phosphanido ligands

U. Flörke and H.-J. Haupt

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Redetermination of the structure of trans-tetraamminebis(thiocyanato-N)nickel(II)

E. Ďurčanská, J. Kožíšek, J. Ďurík and V. Kettmann

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Structure of bis(4-methylpyridine-N)copper(I) bromide

M. J. Jedrzejas, R. A. Martuch, R. L. R. Towns, R. J. Baker, S. A. Duraj and A. F. Hepp

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Structure of bis(benzenesulfonato-O)tetrakis(pyridine-N)copper(II)

M. J. Jedrzejas, R. L. R. Towns, R. J. Baker, S. A. Duraj and A. F. Hepp

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Structure of an allotropic form of [bis(trimethylsilyl)amido]dichloro(η⁵-cyclopentadienyl)titanium

F. Laurent and J.-P. Legros

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Bis(tetraethylammonium) nickel tetrakisthiophenolate: a new polymorph

A. L. Rheingold, K. S. Beall, P. J. Riggs and S. E. Groh

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short format (organic compounds)

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Structure of 3-(p-chlorophenyl)-3,4-dihydro-1H-2,3-benzothiazine 2,2-dioxide

B. E. Rivero, M. A. Bianchet and R. D. Bravo

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Structure of 6-chloro-3,4-dihydro-1H-2,3-benzothiazine 2,2-dioxide

B. E. Rivero, M. A. Bianchet and R. D. Bravo

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Structure of 4-methylpyridinium bromide

M. T. Andras, A. F. Hepp, P. E. Fanwick, R. A. Martuch and S. A. Duraj

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Structure of diphenyl carbonate

J. A. King Jnr and G. L. Bryant Jnr

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Structure of two polymorphic acylpyridinium salts

G. L. Bryant Jnr and J. A. King Jnr

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Structure of 19-methylstrychninium (S)-{S-[(R)-1,2-di(ethoxycarbonyl)ethyl] O-methyl phosphorodithioate}

C. E. Berkman, E. J. Fernandez, C. M. Thompson and S. F. Pavkovic

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Structure of (3aα,4α,7α,7aα)-2,2-dimethyl-3a,4,7,7a-tetrahydro-1,3-benzodioxolane-4,7-diamine

M. F. Mackay, M. G. Banwell and S. L. Richards

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Structure of N-(2-furylmethyl)-α-cyano-2-furanacrylamide

O. Durruthy, R. Pomés, F. Fajardo and A. Dago

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Structure of ethyl 5-(2,2,2-trichloro-1-hydroxyethyl)furan-2-carboxylate

O. Durruthy, R. Pomés, F. Fajardo and A. Dago

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8-(N-Methyl-N-tosylamino)bicyclo[4.2.0]octane-7-spiro-2'-oxacyclopropane

J. Feneau-Dupont, J.-P. Declercq, S. Vanwetswinkel and C. Genicot

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Structure of the p-nitrobenzoate ester of 3-endo-(p-methoxybenzyl)isoborneol

I.-H. Suh, B.-I. Seo, D. E. Lewis, W. P. Jensen and R. A. Jacobson

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Structure of a highly potent anxiolytic dipeptoid

T. Debaerdemaeker, T. Heigl and K. Steiner

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3-Cyano-3-dimethylamino-4-ethoxy-1-phenyl-2-azetidinone

J. Feneau-Dupont, J.-P. Declercq, M. C. Labille, Z. Janousek and H. G. Viehe

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regular structural papers (inorganic compounds)

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Structure of a new siliconiobate K_6.5Ca_0.75Nb₁₄Si₄O₄₇

M. M. Borel, J. Chardon, A. Grandin, A. Leclaire and B. Raveau

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Redetermination of the structure of α-tetraphosphorus trisulfide diiodide at 180 K

B. W. Tattershall, N. L. Kendall, A. McCamley and W. Clegg

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regular structural papers (metal-organic compounds)

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Bis[1,2-bis(diphenylphosphino)ethane]platinum(II) iodide bis(deuteriochloroform) solvate

G. Ferguson, A. J. Lough, A. J. McAlees and R. McCrindle

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Structure of the two-coordinate cadmium complex bis(pentafluorophenyl)cadmium(II), [Cd(C₆F₅)₂]

H. Strasdeit, I. Büsching, A.-K. Duhme and S. Pohl

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Structure of bis[pentaamminechloroiridium(III)] hexachloroplatinate(IV) dichloride

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Structure of potassium theobrominium tetrakis(thiocyanato)palladate(II) monohydrate

T. Giraldi, M. R. Taylor, M. I. Moreno-Vida, J. Ruiz-Sanchez, J. M. Salas-Peregrín and E. Colacio

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Structure of tetracarbonyl[N,N,N',N'-tetramethylethylenediamine-N,N']molybdenum(0)

M. A. Bakar, H.-K. Fun, K. Chinnakali, S.-G. Teoh, O. B. Shawkataly and F. M. Lopez

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Structures of 2-amino-3-methylpyridinium bis(1,2–dithiooxalato-S,S')metallates(II) (M = Ni, Pd and Pt)

P. Román, J. I. Beitia and A. Luque

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Chlorobis(N-phenylsalicylideneaminato-O,N)manganese(III): a manganese Schiff-base complex derived by an electrochemical route

C. A. McAuliffe, R. G. Pritchard, L. Luaces, J. A. Garcia-Vazquez, J. Romero, M. R. Bermejo and A. Sousa

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cis-Dichloro(di-n-butyl sulfide)(tri-n-butylphosphine)platinum(II)

I. Michaud-Soret, J. Kozelka and C. Bois

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Structure of bis(2-aminothiazole)dichlorozinc(II)

J. Macíček and K. Davarski

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regular structural papers (organic compounds)

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Structure of 4-(9-phenanthryl)-N,N-dimethylaniline

L. Van Meervelt

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Structures of two (1:1) adducts of [α,α-bis(3,3,3-trifluoropropynyl)]benzyl benzoate and furan

M. G. Barlow, B. Beagley, R. G. Pritchard, S. Tajammal, A. E. Tipping and A. P. Wright

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Structure of pentabenzylcyclopentadiene

H. Schumann, F. H. Görlitz and L. Esser

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(+)-2,2'-(1,1'-Binaphthyl)phosphate salt of methyl (11R)-11-{[2-(4-benzylpiperidino)ethyl]thio}-6,11-dihydrodibenz[b,e]oxepin-2-carboxylate

N. Hirayama, T. Sugaya, S. Tomioka, E. Ohshima and H. Obase

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Tetramethyl tert-butylcalix[4]arene tetraketone

G. Ferguson, J. F. Gallagher and M. A. McKervey

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Structures of furo[2,3-b]indolizine derivatives

A. Kakehi, K. Kitajima, S. Ito and N. Takusagawa

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Quinine model study: stereospecific aldol condensation/reduction

B. E. South, R. P. Kashyap, D. A. Minter, M. Krawiec and W. H. Watson

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Hexanitrodiphenylmethane

A. Cousson, J. Lelièvre, A. P. Chatrousse, F. Terrier and P. G. Farrell

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4-[2-Benzoyl-1-(benzoylmethyl)ethyl][2.2]paracyclophane

V. G. Kharitonov, D. Yu. Antonov, V. I. Rozenberg, V. A. Nikanorov, A. I. Yanovsky and Yu. T. Struchkov

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Structure of trans-decafluoroazobenzene

K. Chinnakali, H.-K. Fun, O. B. Shawkataly and S.-G. Teoh

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Structure of zizyberannalic acid

K. Sekar, S. Parthasarathy, A. B. Kundu and B. R. Barik

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Structure and absolute configuration of a monohydrate of calcipotriol, (1α,3β,5Z,7E,22E,24S)-24-cyclopropyl-9,10-secochola-5,7,10(19),22-tetraene-1,3,24-triol

S. Larsen, E. T. Hansen, L. Hoffmeyer and N. Rastrup-Andersen

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Structure of β,β-trehalose

C.-K. Lee and L. L. Koh

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Structure of N-(3-phthalimidooxypropyl)trifluoroacetamide

L. Van Meervelt

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An original linkage between arabinose and a pyranopyrimidine derivative via a sulfur atom

A. Tomas, Nguyen-Huy Dung, B. Viossat, A. Esanu and A. Rolland

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Structure determination of (1S;S_s)-3-methoxy-1-phenyl-2-(p-tolylsulfinyl)-2-propen-1-ol (C₁₇H₁₈O₃S)

R. Retoux, C. Guillot and C. Maignan

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Structure of 5-amino-1,3,4-thiadiazole-2-sulfonamide, an inhibitor of the enzyme carbonic anhydrase

J. C. Pedregosa, G. Alzuet, J. Borrás, S. Fustero, S. García-Granda and M. R. Díaz

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Structures of pyrazole derivatives. I. A potential bioisoster of thromboxane synthetase inhibitors

I. Caracelli, J. Zukerman-Schpector, E. J. Barreiro and A. C. C. Freitas

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Structures of three alicyclic α-dioximes with a ring size of six to eight

N. R. Streltsova, V. K. Bel'sky and Y. Z. Voloshin

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Structure of p-isopropylcalix[4]arene–toluene (1/1) complex

M. Ohtsuchi, K. Suzuki, A. E. Armah, Y. Yamagata, S. Fujii, K. Tomita, Z. Asfari and J. Vicens

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short communications

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Structure of MoAs₂O₇: corrigendum and addendum

E. Hums, H. Burzlaff and W. Rothammel

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On the crystal structure of bis(dipicolinato)ferrate(III) dihydrate

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Structure of phenazine. Erratum

K. Woźniak, B. M. Kariuki and W. Jones

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Kudos

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