Acta Crystallographica Section C
Acta Crystallographica
Section C STRUCTURAL CHEMISTRY

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STRUCTURAL
CHEMISTRY

Volume 50| Part 4

ISSN: 2053-2296

April 1994 issue

Highlighted illustration

Cover illustration: 1,1';2,2'-Bis- [mu] -dimethylsilyl-bis[1,2-dicarba-closo-dodecaborane(12)], see Kivakäs, Romerosa & Viñas, pages 638-640.

inorganic compounds

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Two lithium chloroberyllo(phosphate/arsenate) sodalites: Li₄Cl(BePO₄)₃ and Li₄Cl(BeAsO₄)₃

W. T. A. Harrison, T. E. Gier and G. D. Stucky

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Synthesis and structures of two isostructural phosphites, Al₂(HPO₃)₃ and Ga₂(HPO₃)₃

R. E. Morris, M. P. Attfield and A. K. Cheetham

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X-ray Rietveld structure refinement of Ca, Sr and Ba meta-antimonates

B. G. DeBoer, R. A. Young and A. Sakthivel

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β-Dicobalt pyrophosphate

A. El Belghitti, A. Boukhari and E. M. Holt

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Isomorphous crystals: K₂HPO₄ and K₅Na(HPO₄)₃

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LiGaSi₂O₆

A. Sato, T. Osawa and H. Ohashi

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Strontium cobalt(II) diarsenate

J.-C. Horng and S.-L. Wang

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metal-organic compounds

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Tricarbonyl(η⁶-trimethylphenylsilane)molybdenum

E. C. Alyea, G. Ferguson and V. K. Jain

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[Me₃PhN]₂[WCl₆] und [PPh₄]₂[W₂Cl₆O₂(μ-N)(μ-Cl₂PO₂)], ein μ-N-Nitridowolframat mit Dichlorophosphatbrücke

U. Müller, I. Sens, R. Wollert and K. Dehnicke

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Cd(2,2'-bipyridine-N,N')Ni(CN)₄, a highly bent close two-dimensional network of [Cd-{(NC)Ni_1/4}₄]_n

M. Hashimoto and T. Iwamoto

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(Hexasulfanediyl)di(pyridine-N)zinc

H. Li, S. Du and X. Wu

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μ-(O,O'-Diethyl dithiophosphato-2κS:3κS')-oxo-1κO-tri-μ₃-sulfido-1:2:3κ³S;1:2:4κ³S;1:3:4κ³S-tris(triphenylphosphine)-2κP;3κP;4κP-tricoppertungsten

S. Du and X. Wu

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Azido(η⁵-cyclopentadienyl)bis(triphenylphosphine)ruthenium(II)

M. M. Taqui Khan, M. M. Bhadbhade, M. R. H. Siddiqui, K. Venkatasubramanian and J. A. Tikhonova

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cis-Bis(9-carbazolyl)(1,2-dimethoxyethane)-cis-bis(tetrahydrofuran)ytterbium(II)

C. T. Abrahams, G. B. Deacon, B. M. Gatehouse and G. N. Ward

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A new orthorhombic crystal form of dichloro[(–)-(R,R)-2,2-dimethyl-4,5-bis(diphenylphosphinomethyl)-1,3-dioxolane-P,P']platinum, [{(R,R)-diop}PtCl₂]

C. Ganter, A. G. Orpen, P. Bergamini and E. Costa

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Dichlorobis(5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidine-N³)zinc(II)

J. M. Salas, M. A. Romero, A. Rahmani and R. Faure

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(5,5-Dimethyl-4,7-diazadecane-1,10-diamine-N,N',N'',N''')(perchlorato-O)copper(II) perchlorate

T. H. Tahirov, T.-H. Lu, K. Shu and C.-S. Chung

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[(2RS,5SR,8SR,12SR,15SR)-2,5,8,12,15-Pentaazahexadecane-κ⁵N^2,5,8,12,15]copper(II) diperchlorate

T. H. Tahirov, T.-H. Lu, Y.-L. Liu and C.-S. Chung

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[(4RS,7SR,11RS)-4,12-Dimethyl-4,7,11-triazatridecylamine-N,N',N'',N''']nickel(II) diperchlorate

T. H. Tahirov, T.-H. Lu, K. Shu and C.-S. Chung

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[N,N'-Bis(3-aminopropyl)-trans-1,2-cyclohexanediamine-N,N',N'',N''']di(perchlorato-O)copper(II)

T. H. Tahirov, T.-H. Lu, K. Shu and C.-S. Chung

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Benzenethiolato(triphenylphosphine)gold(I)

J. P. Fackler Jnr, R. J. Staples, A. Elduque and T. Grant

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(o-Methoxybenzenethiolato)(triphenylphosphine)gold(I) diethyl ether solvate

J. P. Fackler Jnr, R. J. Staples and R. G. Raptis

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Dichloro(2,6-diacetylpyridine dioxime-κ³N,N',N'')copper(II) 1.5-hydrate

K. A. Abboud, R. C. Palenik and G. J. Palenik

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[AuCo₃Ru(C₈H₁₁P)(C₁₈H₁₅P)(CO)₁₁].1/2CH₂Cl₂

H. J. Kakkonen, M. Ahlgrén, T. A. Pakkanen and J. Pursiainen

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A new phase of bis[2-(diphenylphosphino-κP)phenylazanido-κN](ethanolato)(oxo)rhenium(V)

G. Bandoli, A. Dolmella, F. Tisato and F. Refosco

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Two forms of cis-dimethylbis(methyl isocyanide)platinum(II)

N. H. Dryden, R. J. Puddephatt, S. Roy and J. J. Vittal

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Absolute configuration of di(perchlorato-O)tetra(pyridine-N)copper(II), [Cu(ClO₄)₂(py)₄]

Y. Agnus, M. Labarelle, R. Louis and B. Metz

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The monoclinic phase [Au₂(C₂₅H₂₂P₂)₂]Cl₂.2CH₃CN

L.-S. Liou, C.-P. Liu and J.-C. Wang

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Diamminebis[5-methylpyrimidine-2,4(1H,3H)dionato(1–)-N³]copper(II) trihydrate

M. Parvez and W. J. Birdsall

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A dinuclear copper(II) complex [Cu₂L₂](ClO₄)₂ derived from 2,6-bis(aminomethyl)-4-methylphenol (HL)

M. Mukherjee, A. K. Mukherjee, S. K. Dutta, K. K. Nanda and M. Helliwell

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Tetrapotassium μ-carbonato-μ-oxo-bis[nitrilotriacetatoiron(III)] dimethanol dihydrate

T. Fujita, S. Ohba, Y. Nishida, A. Goto and T. Tokii

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Structural characterization of mixed valence 1',2',1''',2'''-tetraethylbiferrocenium triiodide

T.-Y. Dong and C.-H. Huang

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organic compounds

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1,7-Dichloro-9-azatricyclo[4.3.1.0^3,7]decan-8-one, a hydrolysed Diels–Alder cycloaddition product from the reaction of 3,5,6-trichloro-1,2,4-triazine with hexa-1,5-diene

M. G. Barlow, R. G. Pritchard, L. Sibous and A. E. Tipping

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4,5:9,10-Dibenzo-1,7-dichloro-1,7-(14-chloromethanonitrilo)tetracyclo[5.5.2.0^2,6.0^8,12]tetradec-13-ene, a 2:1 Diels–Alder cycloaddition product of indene and 3,5,6-trichloro-1,2,4-triazine

M. G. Barlow, R. G. Pritchard, L. Sibous and A. E. Tipping

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exo,exo-4,4,12,12,16,16-Hexakis(trifluoromethyl)-17-(3,3,3-trifluoro-2-trifluoromethyl-1-azapropenyl)-3,11,17-triazaheptacyclo[12.4.1.1^6,9.0^2,13.0^3,11.0^5,10.0^15,18]icos-7-ene formed via novel 1,3-dipolar cycloaddition to quadricyclane

M. G. Barlow, R. G. Pritchard, N. S. Suliman and A. E. Tipping

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endo-(1R,9R,10R*)-9,10-Dimethoxy-12,15,15-trimethyltricyclo[9.3.1.0^3,8]pentadeca-3(8),11-diene-4,13-dione

Y. Takenaka, T. Ono, A. Uchida, Y. Ohashi, T. Furukawa, Y. Horiguchi and I. Kuwajima

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2,5-Dimethyl-4-nitroimidazole

T. A. Olszak, O. M. Peeters, N. M. Blaton and C. J. De Ranter

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Absolute configuration of (I) (–)-(3S,4R)- and (II) (–)-(3S,4S)-3-methyl-4-phenyl-4-piperidinecarboxylic acid hydrobromide

O. M. Peeters, N. M. Blaton and C. J. De Ranter

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N^α-Benzyloxycarbonyl-α-aminoisobutyrylglycyl-L-isoleucyl-L-leucine methyl ester monohydrate

M. Crisma, G. Valle, V. Monaco, F. Formaggio and C. Toniolo

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Two cyclic dipeptide anticonvulsants: cyclo-glycyl-L-phenylglycine (1) and cyclo-L-alanyl-D-phenylglycine (2)

M. B. Szkaradzinska, M. Kubicki and P. W. Codding

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Stereochemistry of transposition reactions involving polycyclic methylenecyclobutanol derivatives

S. Ianelli, M. Nardelli, D. Belletti, N. Brosse, B. Jamart-Grégoire and P. Caubère

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1,3,5-Tris[3-(2,6,6-triméthyl-1-cyclohexen-1-yl)acryloyle]benzène

D. Ginderow, A. Valla, Z. Andriamialisoa and M. Giraud

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12-Methyl-9-hydroxymethyl-9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylate lactone

J. Chen, P. R. Pokkuluri, J. R. Scheffer and J. Trotter

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An ethenonaphthalene and one of its photolysis products

P. R. Pokkuluri, J. R. Scheffer, J. Trotter and M. Yap

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The photolysis product of dimethyl 9,10-diphenyl-1,4-dihydro-1,4-ethenoanthracene-11,12-dicarboxylate

P. R. Pokkuluri, J. R. Scheffer and J. Trotter

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N-[2-(2-Formylphenyl)ethyl]-2-nitroaniline

W. Clegg, S. P. Stanforth, K. A. Hedley, E. S. Raper and J. R. Creighton

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6-Amino-5-[(E)-1,2-bis(methoxycarbonyl)vinyl]-2-methoxy-3-methylpyrimidin-4(3H)-one

J. N. Low, C. Egglishaw, G. Ferguson, J. Cobo, C. Garcia, M. Melguizo, M. Nogueras and A. Sanchez

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Stable conformations of hinokitiol and tropolone

H. Ohishi, H. Tsujibo, M. Inoue, Y. Inamori and N. Ishida

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Non-steroidal anti-inflammatory drugs. III. Structure of indoprofen: 2-[4-(1-oxo-2-isoindolinyl)phenyl]propionic acid

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Phenyl 3-fluorobenzoate

M. Shibakami, M. Tamura, T. Arimura, S. Kurosawa and A. Sekiya

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Cycloaddition products of tricyclo[6.2.1.0^2,7]undeca-2(7),4,9-triene-3,6-dione

V. Pattabhi, S. Banumathi, G. Mehta and S. Padma

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2,2'-Di-O-acetyl-3,6;3',6'-dianhydro-4,4'-dideoxy-α,α-trehalose

C. K. Lee and L. L. Koh

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3,8α-Dihydroxyestra-1,3,5(10),6-tetraen-17-one

E. W. Czerwinski, Z. Cao and J. Liehr

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5- and 7-dicyanomethylene-1,2-ethylenedithiocycloheptatrienes

K. Kubo, A. Mori, H. Takeshita and H. Tsuzuki

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2-n-Propylthiete sulfone

G. J. Gainsford and A. D. Woolhouse

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Ethyldiphenylphosphine oxide, (C₆H₅)₂(C₂H₅)PO

O. Orama and J. T. Koskinen

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Diastereomeric octahydronaphthoquinolizines

B. Cai, Y. Pan, H. Qiu, J. C. Dewan, D. J. Wink, R. B. Murphy and D. I. Schuster

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A triazine derivative

G. D. Nigam, S. Karek, C. R. Saha and S. Srinivasan

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Tris(5-acetyl-3-thienyl)methane–tetrachloromethane (2/1) inclusion compound

L. Pang, R. C. Hynes and M. A. Whitehead

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Structures of the choline ion in different crystal surroundings

K. Frydenvang, G. Hjelvang, B. Jensen and S. M. Martinho Do Rosario

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Stereochemistry of the Carroll rearrangement: structure of (+)-(2R)-2-[(1R,5R)-5-methyl-2-oxocyclopentyl]propionic acid, C₉H₁₄O₃

N. Ouvrard, A. Baldy, J. Rodriguez, M. Santelli, J. Feneau-Dupont and J.-P. Declercq

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2,9-Dioxo-1,6,8,13-tetraoxadispiro[4.1.4.3]tetradeca-3,10-diene, C₁₀H₈O₆

L. Cottier, G. Descotes, L. Eymard and R. Faure

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An intermediate in the synthesis of formoterol

K. Chandra Mohan, K. Ravikumar, T. V. S. K. Vittal and C. K. Gido

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2-Methyl-2-(4-nitrophenylazo)-1,3-indandione, C₁₆H₁₁N₃O₄

S. Özbey, E. Kendi, N. Hocaoglu, T. Uyar, T. C. W. Mak and G. L. Cascarano

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Butyl[3-(1,1,3,3,5,5,5-heptamethyltrisiloxan-1-yl)propyl]dimethylammonium bromide, C₁₆H₄₂NO₂Si₃⁺.Br⁻, at 173 and 301 K

R. Rudert and G. Schmaucks

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Cyclohexanone semicarbazone and 4-tert-butylcyclohexanone semicarbazone

G. Di Maio, S. Li, G. Portalone, K. Zhou, C. Marciante and R. Spagna

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1,1';2,2'-Bis-μ-dimethylsilyl-bis[1,2-dicarba-closo-dodecaborane(12)], C₈H₃₂B₂₀Si₂

R. Kivekäs, A. Romerosa and C. Viñas

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Structural studies on the antimuscarinic agents spiro-DAMP and hydroxy-DAMP, and comparison with related compounds

P. Sabatino, M. Recanatini, V. Tumiatti and C. Melchiorre

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Flavocommelin octaacetate

Y. Ohsawa, S. Ohba, S. Kosemura, S. Yamamura, A. Nakagawa, K. Yoshida and T. Kondo

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1-Benzyl-3-pyrazolidone hydrochloride

Q.-C. Yang, N. Ni, X.-J. Xu and Y.-Q. Tang

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1-(3-Quinolyl)-4-(2-thienyl)-1,3-butadiyne, C₁₇H₉NS

M. J. Barrow, G. H. W. Milburn, Z. Zeng, A. Sarkar and S. S. Talwar

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The Structural Chemistry of Homogeneous and Heterogeneous Catalysts

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