Acta Crystallographica Section C
Acta Crystallographica
Section C STRUCTURAL CHEMISTRY

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STRUCTURAL
CHEMISTRY

Volume 50| Part 8

ISSN: 2053-2296

August 1994 issue

Highlighted illustration

Cover illustration: Spiro[3-germabicyclo[3.1.0]hexane-3,9'-[9]germafluorene], see Ogawa, Takeuchi, Manuel & Boukherroub, pages 1337-1339.

inorganic compounds

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NbSb₂

A. Rehr and S. M. Kauzlarich

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Cu₃Bi₄V₂O₁₄, a new compound

G. B. Deacon, B. M. Gatehouse and G. N. Ward

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Li₃BS₃

P. Vinatier, P. Gravereau, M. Ménétrier, L. Trut and A. Levasseur

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Redetermination of the structure of LaMo₅O₈ by single-crystal X-ray diffraction

P. Gall and P. Gougeon

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A short dynamically symmetrical hydrogen bond in the structure of K[Mg(H_0.5SO₄)₂(H₂O)₂]

J. Macíček, S. Gradinarov, R. Bontchev and C. Balarew

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metal-organic compounds

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Bis(tert-butylammonium) molybdate(VI)

P. Román, A. San José, A. Luque, J. M. Gutiérrez-Zorrilla and M. Martínez-Ripoll

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A pyridine-2-thiolato molybdenum complex

P. Yu, L. Huang and B. Zhuang

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A pseudo-octahedral tungsten oxo compound, [WO(C₁₈H₁₂O)(C₁₃H₁₃P)₃].C₇H₈

J. L. Kerschner, C. E. Kriley, P. E. Fanwick and I. P. Rothwell

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Tris(4,6-dimethylpyrimidine-2-thiolato-N,S)cobalt(III) monohydrate: a complex with three stable four-membered N,S-chelate rings

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Ferrocenyltriphenylsilane

R. T. Palmer, L. J. Radonovich and F. B. McCormick

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Isothiocyanatobis(1,10-phenanthroline)copper(II) perchlorate, [Cu(NCS)(phen)₂]ClO₄

O. J. Parker, J. L. Manson and G. L. Breneman

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A mononuclear oxovanadium(IV) complex [VO(H₂L)(SO₄)].5H₂O derived from a potentially dinucleating tetraaminodiphenol macrocyclic ligand (H₂L)

S. Ghosh, M. Mukherjee, A. K. Mukherjee, S. Mohanta and M. Helliwell

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Bis(o-methoxyphenyl)tin dibromide

J.-N. Ross, J. Wardell, G. Ferguson and J. N. Low

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Chlorobis{2-[(dimethylamino)methyl]phenyl-C¹,N}(pyridine)vanadium(III)

A. L. Spek, J. J. H. Edema and S. Gambarotta

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{1,3,5,7-Tetraazabicyclo[3.3.1]nonane-3,7-bis(acetato)-N³,N⁷,O,O''}nickel(II)

Z. Trávníček and J. Marek

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Bis(tetrapropylammonium) hexachlorodicuprate(II)

G. Hu and E. M. Holt

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cis-Ammine(benzoylhydrazine-N)dichloroplatinum(II)

J. Macíček, N. Dodoff and N. Spassovska

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Platinum(II) triamine complexes: cis-[PtCl(NH₃)₂(C₁₀H₁₃N₅O₅)]NO₃.2H₂O and [PtCl(C₂H₈N₂)(C₄H₆N₂)]NO₃

G. M. Arvanitis, D. Gibson, T. J. Emge and H. M. Berman

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Bis(3-bromoimidazolium) tetrachloropalladate(II)

G. Valle and R. Ettorre

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Triethylammonium hydrogen dichlorotris(diphenylphosphinito-P)rhodium(III) tetrahydrofuran (1/1)

D. J. Irvine, D. J. Cole-Hamilton, J. C. Barnes and R. A. Howie

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cis-Bis[3-sulfido-1,3-bis(2-thienyl)prop-2-enone-O,S]palladium(II)

L. A. M. Baxter, A. J. Blake, F. J. J. Dijksma, R. O. Gould and G. A. Heath

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Dichloro(1-trimethylsilyl-1,5-cyclooctadiene)palladium(II)

N. S. Begum, B. S. Bandodakar and G. Nagendrappa

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Cyclopentadienyl(thioacetamide-S)bis(triphenylphosphine-P)ruthenium(II) tetrafluoroborate

C. D. Bryan, A. W. Cordes and M. Draganjac

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A redetermination of the X-ray structure of the hexanuclear mixed-metal cluster [Ru₅Rh(μ₆-C)(CO)₁₃(μ-CO)(η⁵-C₁₀H₁₅)]

T. Adatia, M. McPartlin, J. Morris, H. Curtis and J. Lewis

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Silver 2-pyrimidinolate dihydrate, [Ag(C₄H₃N₂O)].2H₂O: a case of pseudosymmetry

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Bis(dimethylglyoximato-N,N')(ethyl)(triphenylphosphine)rhodium(III)

V. Kettmann, M. Dunaj-Jurčo, D. Steinborn and M. Ludwig

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[Au(ⁿBuPPh₂){(Ph₂PS)₃C}].CH₃CN: an irregular three-coordinate Au_I complex

R. J. Staples, S. Wang, J. P. Fackler Jnr, S. O. Grim and E. de Laubenfels

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Co-crystallized bis(μ-tert-butylphosphido)bis(di-tert-butylgallium) and tetra-tert-butylcyclotetraphosphane

K. Kirschbaum and D. M. Giolando

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The 18-crown-6 potassium salt of a Meissenheimer anion, [K(C₇H₃Cl₃N₃O₆)(C₁₂H₂₄O₆)]

J. C. Barnes, J. Main and J. D. Paton

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(Nitrato-κO)(triphenylphosphine-κP){3,6,9-trithiabicyclo[9.4.0]pentadeca-1(11),12,14-triene-κ³S^3,6,9}mercury(II) nitrate hydrate hemiethanol solvate

R. Kivekäs, R. Sillanpää, L. Escriche, M. P. Almajano, F. Teixidor and J. Casabó

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Benzyl(bromo)diphenyllead

U. Fahrenkampf, M. Schürmann and F. Huber

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A hydrate of the sodium salt of a penem carboxylic acid

Y. Oyama, S. Imajo, R. Tanaka and M. Ishiguro

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Di-μ-chloro-bis[dichlorotris(2-propanol)cerium(III)] at 153 K

M. Schäfer, R. Herbst-Irmer, U. Groth and T. Köhler

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organic compounds

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3,5-Dimethoxybenzoic acid and the second polymorph of the 2:1 adduct of 3,5-dinitrobenzoic acid with ethylenediamine

D. E. Lynch, G. Smith, K. A. Byriel and C. H. L. Kennard

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2',3'-Didehydro-2',3'-dideoxy-5-hydroxymethyluridine

U. Pugazhenthi, L. T. J. Delbaere, S. V. P. Kumar, A. L. Stuart and S. V. Gupta

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Thiamin acetate, C₁₂H₁₇N₄OS⁺.C₂H₃O₂⁻

J. S. Casas, A. Castiñeiras, M. D. Couce, J. Sordo and J. M. Varela

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2-Thymin-1-ylethyl ester of N-tert-butoxycarbonyl-L-tryptophan, C₂₃H₂₈N₄O₆

K. Fukuyama and M. Irie-Fujii

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An isocoumarin derivative from Paepalanthus bromelioides

K. Tomita and W. Vilegas

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2(RS)-r-2-[(RS)-1-(4-Chlorobenzoyloxy)ethyl]-2-ethyl-1,3-dioxolan-c-4-ylmethyl-4-chlorobenzoate

U. Berens and G. Raabe

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(±)-8-Phenyldinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepine

K. Tani, T. Yamagata and K. Nagata

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Tris(2,6-dimethoxyphenyl)phosphine sulfide monohydrate

S. Hayase, T. Erabi and M. Wada

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A dimeric (phenylsulfonyl)oxazolidine

J. Hirschler, B. Berger and M. Bolte

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A γ-hydroxyvinylsulfoximine, C₂₃H₃₁NO₃S

B. Berger and M. Bolte

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N-Chlorosulfonyl-L-proline benzyl ester

A. J. Ibbett, D. J. Watkin and J. H. Jones

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2,6-Bis(p-nitrophenylthiomethyl)pyridine

R. Sillanpää, R. Kivekäs, L. Escriche, G. Sánchez-Castelló and F. Teixidor

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2-(o-Methoxyphenoxy)-1-methylbenzimidazole, C₁₅H₁₄N₂O₂

K. T. Vasudevan, Puttaraja and M. V. Kulkarni

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1:1 Molecular complex of trimethoprim and sulfametrole

G. Giuseppetti, C. Tadini and G. P. Bettinetti

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Molecular co-crystals of carboxylic acids. 16. 1:1 Adduct of 3-nitrobenzoic acid with 3-amino-1H-1,2,4-triazole

D. E. Lynch, G. Smith, K. A. Byriel and C. H. L. Kennard

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2-(3-Benzyloxy-4-nitrophenyl)oxirane, an intermediate in the synthesis of formoterol

K. Chandra Mohan, K. Ravikumar, T. V. S. K. Vittal and C. K. Gido

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Monohydrates of two isomers of aminotoluenesulfonic acid

A. J. Shubnell and P. J. Squattrito

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An m-carboranedicarboxylic acid dianilide

S. V. Lindeman, G. A. Kats and L. G. Komarova

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Bis(triphenylphosphine)iminium hexafluorophosphate dichloromethane solvate (1/1)

A. J. Blake, G. Freeman, B. F. G. Johnson and G. S. McDougall

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1,7,9-Trimethyl-2,6-purinedione monohydrate, C₈H₁₀N₄O₂.H₂O

M. Parvez and G. Ferguson

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Fluorinated barbituric acid derivatives

D. D. DesMarteau, W. T. Pennington and G. Resnati

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Substituted diphenyl oxalates

C. George, P. M. Lahti, D. A. Modarelli and A. Inceli

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3-[5-(3-Nitrophenyl)furfurylidene]-2,4-pentanedione, C₁₆H₁₃NO₅

J. Lokaj, V. Vrábel, J. Sivý, D. Ilavský and A. Koreňová

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Synthèses et structures de deux acides 5,6-dihydro-6-[aryl]-4-{2-[aryl]-éthényl}-2-oxo-2H-pyrane-3-carboxylique

A. Valla, M. Giraud and D. Ginderow

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2-Acetyl-1,8-dihydroxy-3,6-dimethylnaphthalene

G. Müller, M. Lutz and J. Lachmann

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5,11,17,23-Tetra-tert-butyl-25,26,27,28-[(5-methylfurfuryl)oxycarbonylmethoxy]calix[4]arene

G. Ferguson, Y. Li, M. A. McKervey and E. Madigan

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Structure of a triazaoxatricyclodecadiene derivative. Partial disorder and a packing energy study

G. Gelli, E. Cadoni, M. Pani, M. M. Carnasciali, A. Mugnoli and P. Beltrame

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Roburic acid, a triterpene 3,4-seco acid

T.-T. Jong and C.-T. Chen

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6-Amino-5-hydroxyiminomethyl-1,3-dimethyluracil

J. N. Low, G. Ferguson, M. N. Moreno-Carretero and F. Hueso-Ureña

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4-Amino-2-methylthio-6-oxo-1,6-dihydropyrimidine and its 1-methyl derivative and 4-amino-2-methoxy-1-methyl-6-oxo-1,6-dihydropyrimidine and its 5-nitroso derivative

J. N. Low, S. N. Scrimgeour, C. Egglishaw, R. A. Howie, M. N. Moreno-Carretero and F. Hueso-Ureña

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Acetamide hydrochloride

L.-K. Liu, F.-T. Luo and L.-C. Hsieh

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2,3,4,5,6-Penta-O-acetyl-D-galactonic acid 1'-phenyl-2'-ethoxycarbonylvinyl ester

J. Kopf, D. Abeln, P. Köll, R. Meisel and K. Peseke

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Spiro[3-germabicyclo[3.1.0]hexane-3,9'-[9]germafluorene]

K. Ogawa, Y. Takeuchi, G. Manuel and R. Boukherroub

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1-(3-Benzoylphenyl)ethanone (I) and 3-benzoyl-α-methylbenzeneacetamide methylene chloride solvate (2/1) (II)

D. Matak, M. Vinković and M. Dumić

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1-Tosyl-1H-pyrrolo[2,3-c]pyridine-5-carboxylic acid ethyl ester

A. Chiaroni, C. Riche, M. Dekhane and R. H. Dodd

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Product of a Paterno–Büchi reaction of pentafluorobenzaldehyde and 4-tert-butyl-1-acetoxycyclohexene

C. P. Brock, M. A. Lloyd, S. Vasudevan, D. S. Watt and H. Morita

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Two N-saccharin peracids

N. Feeder and W. Jones

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2-(4-Cyanobenzoylaminomethyl)-1-methyl-5-(3-thienyl)-2,3-dihydro-1H-1,4-benzodiazepin-4-ium p-toluenesulfonate

O. M. Peeters, N. M. Blaton, R. L. Meurisse and C. J. De Ranter

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5-(2,4-Dichlorophenyl)-2-[(3-furoyl)aminomethyl]-8-methoxy-1-methyl-2,3-dihydro-1H-1,4-benzodiazepin-4-ium p-toluenesulfonate

O. M. Peeters, N. M. Blaton, R. L. Meurisse and C. J. De Ranter

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4-Hydroxyacetophenone oxime (I) and 4-hydroxy-3-methylacetophenone oxime (II)

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2'-Hydroxypropiophenone oxime

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(1S,2S,5R,6S)-(+)-6-Carbanilino-1,5-dimethyltricyclo[3.2.0.0^2,6]heptane

T.-T. Jong, M. Y. Jean and T. J. Lu

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Molecules isoelectronic with 2,2,2-triphenylethanol: multiple hydrogen-bonding modes in the structures of O-tritylhydroxylamine, Ph₃CONH₂, and triphenylmethanesulfenamide, Ph₃CSNH₂

C. Glidewell and G. Ferguson

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(2S,3R,4S,5R,6S,7R,8R,9S)-1,2,3,4,5,6,7,8,9-Nonaacetoxydecane

K. Lewinski, J. A. Marshall and S. Beaudoin

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Refinement of a twinned structure with SHELXL93: meso-2,2'-[1,6-bis(methylamino)-3,4-dithia-1,6-hexanediyl]diphenol

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Configuration of (E)-2-(1-hydroxy-1-methyl-2-oxopropyl)-2-(methylthio)thiolane S-oxide

J.-S. Brunck, J. Voss, H. Viebrock and F. Olbrich

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addenda and errata

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The structures of alkalides and electrides. II. Structure of caesium bis(15-crown-5) electride. Erratum

D. L. Ward, R. H. Huang, M. E. Kuchenmeister and J. L. Dye

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Kudos

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Special and virtual issues

Acta Crystallographica Section C is planning special issues on

The Structural Chemistry of Homogeneous and Heterogeneous Catalysts

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Full details are available on the special issues page.

The latest virtual issue, featuring Coordination polymers and with an introduction by Len Barbour, was published in July 2014.

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