Figure 4
The temperature dependence of the FXS data (log scale). (a) and (c) The SAXS intensities, and (b) and (d) the amplitudes of the FCs for n = 2, 4 and 6 and q2 = 0.25 nm−1, determined at temperatures T = 229 and 297 K for the sample with a volume fraction of goethite nanorods φg = 0.05% [panels (a) and (b)], and at temperatures T = 209 and 229 K for the sample with φg = 0.5% [panels (c)–(d)]. The black arrows in panels (b) and (d) indicate the observed temperature drop of . |