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Figure 5
(a) Refined PXRD patterns from in situ syntheses for all com­positions after 20 min of synthesis. (b) 2D contour plot of PDFs during the in situ experiment of x = 0.24. The inset shows the first 10 min of the experiment.

IUCrJ
Volume 13| Part 4| July 2026|
ISSN: 2052-2525
https://doi.org/10.1107/S2052252526003829