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Pd nanocrystals were produced with uniform truncated-cube shape and a narrow size distribution, yielding controlled surface area fractions from low Miller index ({100}, {110}, {111}) crystalline facets. Details on the structure and morphology of the nanocrystals were obtained by combining X-ray powder diffraction line profile analysis, high-resolution transmission electron microscopy and surface electrochemistry based on Cu underpotential deposition.

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Portable Document Format (PDF) file https://doi.org/10.1107/S1600576715015964/ks5481sup1.pdf
TEM, HRTEM images and particle size distributions of the nanocrystals used in this work; XRD pattern from an empty kapton capillary. Details of electrochemical characterization


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