Figure 15
(a) Sketch of the setup for a high-resolution powder diffraction experiment with the Pilatus 100k detector. (b) High-resolution powder diffraction pattern of LaB6 with E = 220680.5 eV, λ = 0.5618 Å, glass capillary 0.3 mm diameter, sample–detector distance 800 mm, step width 0.5°. Insert: peak profil reflex (221) with a resolution Δ2θ of 0.013°. (c) Four of the 80 shots to obtain the full diffractogram shown in (b). |