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Figure 18
(a) Beam conditioning unit of XRD-2, the Pilatus diffractometer, with the Huber kappa goniometer mounted (1 – Kappa goniometer, 2 – motorized beam stop, 3 – Vortex SDD, 4 – long-distance microscope, 5 – macro camera, 6 – beam tube, 7 – entrance slits, 8 – ionization chamber (50 mm) to determine incoming beam intensity, 9 – motorized pin hole unit, 10 – support for Pilatus3 X 2M detector). (b) The fluorescence detector can be used to determine f ′ and f ′′ in the case of resonant measurements to select the appropriate excitation energy as shown here for uranium(IV). (c) This technique was applied to determine the structure of UCl2salen(MeOH)2, space group P43212.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 28| Part 1| January 2021| Pages 333-349
https://doi.org/10.1107/S1600577520014265
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