Figure 1
Transmission synchrotron X-ray Debye–Scherrer rings taken at HEMS at Petra III/DESY. Beam size: 100 µm × 100 µm, λ = 0.14235 Å. The Mar345 detector ensured a minimum of 20 measured points for the whole breadth for each of the measured peaks, while the Perkin–Elmer detector allowed measurement of approximately 10 points. |