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Figure 4
Radial diffraction profiles captured during injection into vacuum at the LCLS. The two samples prepared with a 60:40 MO/water ratio, (a, d) V1 and (b, e) V3, exhibit the Ia3d and Pn3m phases occurring simultaneously. The positions of peaks associated with these phases are shown as vertical lines in plots (a)–(c). An Lα peak is also observed in these samples with a structure parameter of around 45 Å. The 85:15 MO/water sample, (c, f) V2, was the only sample observed with an Lc phase during vacuum injection. The Lα phase with the structure parameter 37.5 Å is also observed in this data, which is consistent with the previous studies for this composition.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 29| Part 3| May 2022| Pages 602-614
https://doi.org/10.1107/S1600577522001862
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