In situ/operando plug-flow fixed-bed cell for synchrotron PXRD and XAFS investigations at high temperature, pressure, controlled gas atmosphere and ultra-fast heating

Bischoff, B.; Bekheet, M.F.; Dal Molin, E.; Praetz, S.; Kanngießer, B.; Schomäcker, R.; Etter, M.; Jeppesen, H.S.; Tayal, A.; Gurlo, A.; Gili, A.

doi:10.1107/S1600577523009591

Journal of Synchrotron Radiation Journal of
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Figure 4
Comparison of measured versus theoretical Pt lattice parameters as a function of temperature. Experimental data were recorded at 50/100°C intervals under an Ar flow rate of 10 Nml min⁻¹. Standard deviation values as small as 0.00001 Å are determined for all experimental data.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 31| Part 1| January 2024| Pages 77-84

https://doi.org/10.1107/S1600577523009591

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