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Figure 6
(a) Rietveld refinements of the NIST CeO2 powder data obtained in the standard scan mode. The inset shows an expanded view of the high-angle data. The powder was filled into a 0.2 mm diameter Lindeman glass capillary. (b) Rietveld refinements of the NIST CeO2 powder data obtained in the single-step scan mode. The markers and line show the measured (Iobs.) and calculated (Icalc.) data, respectively. The intensity difference curves (Iobs. − Icalc.) are offset for clarity. All data were measured using an X-ray energy of 35 keV.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 31| Part 4| July 2024| Pages 955-967
https://doi.org/10.1107/S1600577524003539
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