Revealing the structure of the active sites for the electrocatalytic CO2 reduction to CO over Co single atom catalysts using operando XANES and machine learning

Martini, A.; Timoshenko, J.; Rüscher, M.; Hursán, D.; Monteiro, M.C.O.; Liberra, E.; Roldan Cuenya, B.

doi:10.1107/S1600577524004739

Journal of Synchrotron Radiation Journal of
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Figure 1
Co K-edge XANES dataset (27 spectra) collected under operando conditions during the CO₂RR process. The inset shows a magnification of the pre-edge region. The arrows highlight the evolution of the XANES features with time under reaction conditions. Measurements performed at −1.2 V_RHE in 0.1 M KHCO₃ as electrolyte.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 31| Part 4| July 2024| Pages 741-750

https://doi.org/10.1107/S1600577524004739

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