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Figure 2
(a) Photograph of the setup on the MAX IV beamline DanMAX. The ARΩS furnace (center, with orange polyimide windows) is on a hexapod stage in front of the PILATUS4 CdTe detector prototype (left: black with blue frame and reflective entrance window), with the X-ray beam coming from the right. (b) Heat map of the integrated diffraction data as a function of time, background corrected. (c) Estimated sample temperature and heat rate determined from refined alumina lattice parameters. (d) Selected Rietveld refined patterns at room temperature and 2000 K. (e) Evolution of relative masses determined from the refined scale factors. |