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Figure 3
Le Bail fit of the summed diffractogram of a scanned area of 400 µm × 300 µm (λ = 0.684995 Å). The calculated intensity corresponds to the known phase content of prior PXRD measurements. The observed intensities are shown in red, the refined model in black and the respective Bragg positions in green. Due to the high resolution of microXRD, peaks that do not belong to the phase content known from prior PXRD are resolved (zoom).

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 32| Part 4| July 2025| Pages 986-993
https://doi.org/10.1107/S1600577525003868
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