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Figure 1
Design and integration of the in situ furnace for synchrotron experiments. (a) CAD rendering showing a side and bottom view of the furnace, with the laboratory coordinate system overlaid in black: x is along the incident X-ray beam direction and z is vertical. Key components such as the sample holder slots, X-ray beam aperture and water-cooling channels are visible. The bottom view shows the placement of the thermocouple and resistive heaters, between which the sample is inserted. (b) Photograph of the furnace mounted on the beamline goniometer. A circular heat shield is inserted on the bottom part to protect the goniometer. The angles μ, χ and ω represent goniometer rotations about the laboratory coordinate axes.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 33| Part 1| January 2026| Pages 115-122
https://doi.org/10.1107/S1600577525010288
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