Modular reactor for in situ X-ray scattering, spectroscopy and ATR-IR studies of solvothermal nanoparticle synthesis

Harouna-Mayer, S.Y.; Gumus Akcaalan, M.; Kopula Kesavan, J.; Groene, T.R.L.; Klemeyer, L.; Hussak, S.-A.; Grote, L.; Derelli, D.; Caddeo, F.; Zito, C.; Stützle, P.; Speer, D.; Dippel, A.-C.; Detlefs, B.; Appiarius, Y.; Jacobi von Wangelin, A.; Koziej, D.

doi:10.1107/S1600577525009634

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Figure 2
Thermal, pressure, and transmission characteristics of the glass inlet with 0.3 mm wall thickness. (a) Front view rendered image of the reactor. (b) Photographs showing the solution color change during Fe₃O₄ formation from Fe(acac)₃ in BnOH upon heating. (c) IR image showing uniform heat distribution of the BnOH-filled inlet at 180°C. (d) Temperature and pressure profiles during the heating of water and BnOH to 150°C and 180°C, respectively. (e) Simulated X-ray transmission of the inlet, empty and filled with the solvents water, ethanol (EtOH), and BnOH as a function of the X-ray energy.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 33| Part 1| January 2026| Pages 142-153

https://doi.org/10.1107/S1600577525009634

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