Modular reactor for in situ X-ray scattering, spectroscopy and ATR-IR studies of solvothermal nanoparticle synthesis

Harouna-Mayer, S.Y.; Gumus Akcaalan, M.; Kopula Kesavan, J.; Groene, T.R.L.; Klemeyer, L.; Hussak, S.-A.; Grote, L.; Derelli, D.; Caddeo, F.; Zito, C.; Stützle, P.; Speer, D.; Dippel, A.-C.; Detlefs, B.; Appiarius, Y.; Jacobi von Wangelin, A.; Koziej, D.

doi:10.1107/S1600577525009634

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Figure 5
In situ ATR-FTIR analysis of the reaction of Fe(acac)₃ to Fe₃O₄ in BnOH, compared with reference spectra of acetone and benzyl acetate, Fe(acac)₃ dissolved in BnOH at room temperature, and BnOH at 180°C.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 33| Part 1| January 2026| Pages 142-153

https://doi.org/10.1107/S1600577525009634

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