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Figure 6
In situ Fe K-edge HERFD-XANES analysis of the reaction to Fe3O4. (a) In situ HERFD-XANES data. (b) Concentration profiles of three distinct Fe species extracted via MCR-ALS. (c) MCR-ALS recovered spectra. (d) FEFF simulations based on structures determined from in situ PDF analysis, confirming the initial species as Fe(acac)3, the intermediate as [Fe3(μ3-O)(AcOR)6(ROH)3]+ and Fe3O4 as the final product.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 33| Part 1| January 2026| Pages 142-153
https://doi.org/10.1107/S1600577525009634
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