Methodological insights into the dip-and-pull X-ray photoelectron spectroscopy technique: analysing electrochemical interfaces under in situ/operando conditions

Rotonnelli, B.; Brige, A.; Oshchepkov, A.G.; Gallet, J.-J.; Bournel, F.; Bonnefont, A.; Yaroslavtsev, A.; Shavorskiy, A.; Temperton, R.; Savinova, E.R.; Asset, T.

doi:10.1107/S1600577525008811

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Figure 1
(a) Example of XPS in situ/operando setup for the `transparent-window cell' design; (b) D&P spectroelectrochemical cell representation, belonging to the `meniscus cell' type; (c) zoomed-in view of the analysed interface; (d) and (e) correspond to illustration of the XPS signal of dissolved species (e.g. cations) in the electrolyte at point of zero charge (PZC) (d) and at potential different from the PZC (e).

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 33| Part 1| January 2026| Pages 130-141

https://doi.org/10.1107/S1600577525008811

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