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![[Figure 2]](mad5003fig2mag.jpg)
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Figure 2
(a) Experimental setup: a 0.7 mm × 0.9 mm 35 keV X-ray beam hits the rotating sample capillary (2 mm) with the scattered X-rays detected by a vertically offset area detector at a sample–detector distance of 1240 mm. Sample temperature is controlled by a heat gun. (b) Azimuthally integrated X-ray scattering signals from a water-filled capillary, S(Q)Meas. (dark grey) at 300 K, an empty capillary S(Q)Bg. (light grey), and the background-corrected scattering signal  (black) from water. |
![[Figure 2]](mad5003fig2.jpg)
 | JOURNAL OF SYNCHROTRON RADIATION |
ISSN: 1600-5775
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