Orchestrating agentic systems at ALS beamline 5.3.1 with Osprey and Bluesky

Chan, K.H.; Ha, Y.; Islegen-Wojdyla, A.; Leon, S.D.; Garces, M.; McReynolds, D.; Chong, X.; Sriramoju, R.V.; Mahl, J.; Guenzing, D.; Koepp, W.; Hexemer, A.; Hellert, T.; Chavez, T.

doi:10.1107/S1600577526007836

Figure 4
AI-assisted beamline operation at ALS beamline 5.3.1 combining multi-edge fluorescence spectroscopy and tender GISAXS. (a) Representative GISAXS detector image acquired during GISAXS scan. (b) Corresponding horizontal line cut showing integrated intensity versus momentum transfer q. (c) Sequential fluorescence scans across Mn, Co, Ni, Cu, and Zn K-edges, demonstrating automated edge selection and parameter configuration. All measurements were executed through validated plan templates via the Bluesky Queue Server, illustrating coordinated multi-step alignment and spectroscopy within a deterministic control framework.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 33| Part 5| September 2026|

https://doi.org/10.1107/S1600577526007836

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