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Figure 3
S3DXRD configuration and reconstructed maps of the α-Fe wire. (a) Experimental setup at EH1 for S3DXRD. A rotation stage (ω) is mounted on the X–Z translation stage, allowing the lateral shift of the rotation axis with the X stage. Above the rotation stage, a pair of xs–ys alignment stages supports the positioning of the α-Fe specimen. (b) Reconstructed IPF-xs and (c) IPF-ys maps show a seemingly random arrangement of grain orientations, whereas (d) IPF-zs map displays a grain texture with a preferred orientation. (e) Completeness map clearly highlights the grain boundaries in the polycrystalline α-Fe wire.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 33| Part 5| September 2026|
https://doi.org/10.1107/S1600577526006387
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