Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 58| Part 2

ISSN: 2056-9890

February 2002 issue

Highlighted illustration

Cover illustration: This triptyceno-crown ether has an unusual conformation, since the ether strand is long enough not to cause steric congestion for the triptycene unit. See Bryan, Gakh & Sachleben [Acta Cryst. E58, o129-o131].

inorganic compounds

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K₂Mo₁₅S₁₉: a novel ternary reduced molybdenum sulfide containing Mo₆ and Mo₉ clusters

S. Picard, P. Gougeon and M. Potel

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A new polymorph of 2,2,4,4,6,6-hexaisothiocyanatocyclotriphosphazene

E. Kessenich, A. Schulz and K. Polborn

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The intermetallic compound BaAuSb

E. K. Lee, G. J. Miller and S. K. Kang

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Strontium dihydrogenphosphite

R. Ouarsal, A. A. Tahiri, B. E. Bali, M. Lachkar and M. Bolte

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metal-organic compounds

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Dichlorotetrakis(4-methylimidazole)copper(II)

C. Näther, M. Wriedt and I. Jeß

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Carbonyl[hydrotris(3,5-dimethylpyrazol-1-yl)borato]copper(I) acetonitrile solvate

A. J. Blake, D. A. Carling, M. W. George, P. Hubberstey, R. Lopez Garcia and C. Wilson

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Triaqua(2,6-pyridinedicarboxylato)copper(II) at 150 K

A. J. Blake, M. Felloni, P. Hubberstey, C. Wilson and M. Schröder

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The pseudosymmetric structure of bis(diisopropylammonium) hexachloroiridate(IV) and its relationship to potassium hexachloroiridate(III)

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Chloro(1,5-cyclooctadiene)(triphenylphosphine)rhodium(I)

Q. L. Horn, D. S. Jones, R. N. Evans, C. A. Ogle and T. C. Masterman

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Bis[dicarbonyl(cyclopentadienyl)ferrio]mercury(II)

J. S. McIndoe and B. K. Nicholson

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Redetermination of bis(2-aminopyrimidine)bis(nitrato)copper(II)

G. A. Albada, I. Mutikainen, U. Turpeinen and J. Reedijk

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Diaquadichlorodiphenyltin(IV) 18-crown-6

M. M. Amini, A. Azadmeher, M. Yousefi, S. Foladi and S. W. Ng

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Tetrakis(trimethylammonioacetato-O)copper(II) bis(hexafluorophosphate)

Y.-Y. Yang, X.-M. Chen and S. W. Ng

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Dibromotetrakis(4-methylimidazole)copper(II)

C. Näther, M. Wriedt and I. Jeß

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Bis(triphenylstannyl)borate toluene solvate

S. J. Coles, D. E. Hibbs, M. B. Hursthouse, M. A. Beckett, P. Owen and K. S. Varma

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Rerefinement of (μ-1,7,11,17-tetraoxa-2,6,12,16-tetraazacycloeicosane-κ⁴N¹,N¹⁷:N⁷,N¹¹)bis[dichlorozinc(II)]

V. A. Kuksa, S. M. S. V. Wardell, P. K. T. Lin and R. A. Howie

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Tetracarbonylbis[(pentafluoroethyl)diphenylphosphine]chromium(0)

R. G. Peters, M. V. Golynskiy and R. G. Baughman

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Chlorotripyridinecopper(I)

S. Scholz, H.-W. Lerner and M. Bolte

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organic compounds

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9,10-Bis(3-hydroxy-3,3-diphenylprop-1-ynyl)anthracene N,N′-dimethylformamide solvate

R. Sugadev, D. Balasundaresan, K. K. Chacko, M. N. Ponnuswamy and M. Sureshkumar

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threo-2-(2,6-Dimethoxyphenoxy)-1-(3,4-dimethoxyphenyl)-1,3-propanediol

V. Langer, K. Lundquist, R. Stomberg and S. von Unge

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N-(tert-Butyl)-N-[2-hydroxy-3-(2-isopropyl-5-methylphenoxy)propyl]ammonium hydrogen oxalate

G. Vasuki, S. Thamotharan, V. Parthasarathi, K. Ramamurthi, S. M. Coumar and D. P. Jindal

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DL-Valinium nitrate

N. Srinivasan, B. Sridhar and R. K. Rajaram

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4-[(4-Ethoxyphenyl)aminoacetyl]-1,2,3,4-tetrahydroquinoxalin-2-one

R. Kruszynski, T. J. Bartczak and E. Mikiciuk-Olasik

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1,4-Diazabicyclo[2.2.2]octanium 2,4-dinitrophenolate

S. Chantrapromma, A. Usman, H.-K. Fun, B.-L. Poh and C. Karalai

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4-Chloro-2-methylanilinium dihydrogenphosphate

J. Fábry, R. Krupková and V. Studnička

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The 1:2 adduct N,N-dimethylethylenediamine-1,4-diium bis(2,4-dinitrophenolate)

S. Chantrapromma, A. Usman, H.-K. Fun, B.-L. Poh and C. Karalai

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Bis(phenylguanidinium) carbonate monohydrate

T. Kolev, T. Todorov and R. Petrova

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Bis(DL-serinium) oxalate dihydrate

M. Alagar, M. Subha Nandhini, R. V. Krishnakumar and S. Natarajan

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β-Alaninium oxalate hemihydrate

R. V. Krishnakumar, M. Subha Nandhini and S. Natarajan

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2,4,6,8,10,12-Hexabenzyl-5-(nitromethylene)-2,4,6,8,10,12-hexaazatricyclo[7.3.0.0^3,7]dodecane

R. D. Gilardi and R. J. Butcher

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L-Phenylalanine L-phenylalaninium dihydrogenphosphate

B. Ravikumar, B. Sridhar and R. K. Rajaram

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2-Amino-5-(4-chlorophenyl)-1-methylimidazole

V. B. Rybakov, E. V. Babaev and E. N. Belykh

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(9,10-Triptyceno)benzo-28-crown-8

J. C. Bryan, A. A. Gakh and R. A. Sachleben

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4-Phenyl-1-(2,4,5-tricyanophenyl)-1,2,3,4-tetrahydronaphthalene

M. Zhang, A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma and J.-H. Xu

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1,2-Bis(1-phenylsulfonyl-3-phenylthioindol-2-yl)ethane

K. SethuSankar, N. Suresh Babu, D. Velmurugan, S. Shanmuga Sundara Raj and H.-K. Fun

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(Benzylsulfonyl)methanol

P. C. Healy, W. A. Loughlin, B. M. Sweeney and I. D. Jenkins

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3-Amino-5,6-dicyano-1-phenylimino-1H-isoindole

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2-[(7R,9S,10R,12E)-4,9-Dihydroxy-10-methyl-5-oxo-7,8,9,10,11,14-hexahydro-5H-6-oxa-benzocyclododecen-7-yl]ethyl octanoate

L. Esser and J. K. De Brabander

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1-Acetyl-2-oxo-4′-methyl-2a′-phenylspiro[3H-indole-3,2′(2a′H,5a′H)-oxeto[3,2-d]oxazole]

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

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3(S)-Acetoxymethyl-7-chloro-1,3-dihydro-1-methyl-5-phenyl-2H-1,4-benzodiazepin-2-one

A. Višnjevac, A. Avdagić and B. Kojić-Prodić

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3-[(Diphenylmethylene)amino]phthalonitrile

J.-Z. Tian, A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

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A taxane diterpenoid from the heartwood of Taxus wallichiana

S. K. Chattopadhyay, A. Sharon, U. Yadav, S. Srivastava, V. K. Mehta and P. R. Maulik

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m-Carboxyphenylammonium nitrate

N. Benali-Cherif, A. Cherouana, L. Bendjeddou, H. Merazig, L. Bendheif and K. Bouchouit

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4,6-Dimethyl-2-(2,4-dimethylphenyliminomethyl)quinoline

M. Aygün, S. Öztürk and F. Aydog~an

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p-Carboxyphenylammonium dihydrogenmonophosphate monohydrate

N. Benali-Cherif, A. Abouimrane, K. Sbai, H. Merazig, A. Cherouana and L. Bendjeddou

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2-Methyl-3,3,10-triphenyl-3,4-dihydronaphth[2,1-c]azepine-1,5-dione

B.-G. Zhao, A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma and J.-H. Xu

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Benzyl (1R,3S)-3,6-dihydro-3-methyl-1λ⁴,2-thiazine-2-carboxylate 1-oxide

L. K. Hansen, A. Bayer and O. R. Gautun

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1,6-Bis(1-benzimidazolyl)hexane trihydrate

Y. Cai, Z. Zhou, L. Qiu, B. Kang and A. S. C. Chan

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2,5-Dibromo-6-isopropyl-3-methyl-p-benzoquinone

L. Esser, Z. Otwinowski and H. Kim

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(1S,3R,4R,4aS,8aS)-4-[(3S)-3-Hydroxy-3-methyl-4-pentenyl]-3,4a,8,8-tetramethyldecahydro-1,3-naphthalenediol

H. Kooijman and A. L. Spek

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1,2-Diethyl-3-hydroxy-6-phenylthiopyridin-4(1H)-one

W.-L. Xie, C.-H. Chen, L. Ma and L.-Q. Gu

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1,1-Dibenzyl-6-methoxy-3,4-dihydro-1H-naphthalen-2-one

C. L. Brown, S. J. Head and P. C. Healy

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N—H⋯N hydrogen bonds in trimethoprim salicylate methanol solvate [trimethoprim is 2,4-diamino-5-(3,4,5-trimethoxybenzyl)pyrimidine]

P. Panneerselvam, N. Stanley and P. T. Muthiah

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A new chiral Schiff base: (R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-5,5′,6,6′,7,7′,8,8′-octahydro-1,1′-binaphthyl-2,2′-diamine

X. Jia, X. Li and Z. Zhou

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2,6-Dibromo-4-fluorobenzonitrile

D. Britton, W. E. Noland and T. K. Henke

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Monoclinic form of 6-phenylhex-5-ene-2,4-dione

A. F. Arrieta and A. Mostad

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p-Tolylsulfonyl cyanide

D. A. Jay, A. Whiting, D. S. Yufit, J. A. K. Howard and S. Hermitage

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A 1:2 complex of pyromellitic diimide and dimethyl sulfoxide

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n-Decane

A. D. Bond and J. E. Davies

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(1R,3R,6S*)-3,6-Dihydro-3,6-dimethyl-2-(toluene-4-sulfonyl)-1λ⁴,2-thiazine 1-oxide

L. K. Hansen, A. Bayer and O. R. Gautun

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N,N-Dimethyl-N′,N′′-bis(4-methylphenyl)phosphoramidate

K. Gholivand, A. Tadjarodi and S. W. Ng

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Triisopropyl[5-(4-nitrophenyl)tetrahydrofuran-3-ylidenemethyl]silane

M. E. Light and M. B. Hursthouse

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[(2R,5R)-2,5-Bis(4-nitrophenyl)perhydrofuro[2,3-b]furan-3-yl]triisopropylsilane

S. J. Coles and M. B. Hursthouse

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Ethyl 4-methyl-9H-carbazole-3-carboxylate

T. Hökelek, S. Patır, Y. Ergün and G. Okay

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Pyridinium D(+)-10-camphorsulfonate hemihydrate

H. Fleischer and D. Schollmeyer

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Bis(L-tyrosinium) sulfate monohydrate

B. Sridhar, N. Srinivasan and R. K. Rajaram

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Research communications are designed to help authors bring out the science behind their structure determinations. Authors are encouraged to report more than one structure in the same communication and also to include the results of investigations with other techniques. The Research communications format makes Acta E the natural home for structure determinations with interesting science to report.

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