Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 59| Part 1

ISSN: 2056-9890

January 2003 issue

Highlighted illustration

Cover illustration: The tridentate Schiff base ligand derived from the condensation of salicylaldehyde and DL-tyrosine, in the presence of pyridine, forms this square-pyramidal five-coordinate Cu complex, with a water molecule occupying the apical site. See Butcher, Mockler & McKern [Acta Cryst. E59, m20-m22].

editorial

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Structure Reports Online: from infancy to maturity

W. Clegg and D. G. Watson

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Some guidelines for publishing SHELXL-generated CIF results in Acta Crystallographica

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international union of crystallography

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Notes for authors 2003

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metal-organic compounds

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Nitratotris(2,2,6,6-tetramethyl-3,5-heptadionato)hafnium(IV)

U. K. Urs, M. S. Dharmaprakash, S. A. Shivashankar and T. N. Guru Row

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1-Methyl-N-(4-nitrobenzyl)pyridinium bis(2-thioxo-1,3-dithiole-4,5-dithiolato)nickelate(III)

W.-J. Tong, L. Liu, Q.-J. Meng, Y.-Z. Li and Y.-G. Yao

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[(R)-(+)-1,1-Binaphthyl-2,2′-diamine](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate diethyl ether disolvate

M. D. Jones, F. A. Almeida Paz, J. E. Davies and B. F. G. Johnson

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Bis(4,4′-bipyridine)tetraaquacobalt(II) 2,6-naphathalenedicarboxylate dihydrate

F. A. Almeida Paz, Y. Z. Khimyak and J. Klinowski

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Tetramethyllead(IV) at 150 K

H. Fleischer, S. Parsons and C. R. Pulham

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Chain structure of catena-poly[[bis[cis-1-(2,4,6-trimethylphenyl)tetrazole-κN⁴]copper(II)]-di-μ-chloro]

D. O. Ivashkevich, A. S. Lyakhov, M. M. Degtyarik and P. N. Gaponik

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Aquadichloro(2,9-dimethyl-1,10-phenanthroline-κ²N,N′)copper(II)

P. Lemoine, B. Viossat and J.-C. Daran

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Aqua(pyridine-κN)(N-salicylidenetyrosinato-κ³O,N,O′)copper(II)

R. J. Butcher, G. M. Mockler and O. McKern

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[1-(Benzimidazol-2-ylmethyl)-1,4,7-triazacyclononane]chlorocopper(II) perchlorate

Q.-X. Li, Y.-Z. Li and Q.-H. Luo

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A one-dimensional Cl-bridged Pt^II/IV mixed-valence complex, catena-poly[[bis(ethylenediamine)platinum(II)-μ-chloro-bis(ethylenediamine)platinum(IV)-μ-chloro] tetrakis(hydrogensulfate)]

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Anhydrous tris(dibenzoylmethanido)(o-phenanthroline)europium(III), [Eu(DBM)₃(Phen)]

M. O. Ahmed, J.-L. Liao, X. Chen, S.-A. Chen and J. H. Kaldis

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Redetermination of the structure of diferrocenyl ketone at low temperature

N. Bratych, K. Hassall and J. White

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μ-Succinato-bis(aquatriphenyltin)bis(o-phenanthroline)

C. F. Chee, K. M. Lo and S. W. Ng

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The chain structure of catena-poly[[(2-tert-butyltetrazole-κN⁴)copper(II)]-di-μ-chloro]

A. S. Lyakhov, P. N. Gaponik, M. M. Degtyarik and L. S. Ivashkevich

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Diacetatobis(2-aminobenzothiazole)zinc(II)

A. Usman, H.-K. Fun, S. Chantrapromma, M. Zhang, Z.-F. Chen, Y.-Z. Tang, S.-M. Shi and H. Liang

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trans-Dichlorobis(cyclohexyldiphenylphosphine)palladium(II)

A. M. M. Meij, A. Muller and A. Roodt

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The interplay of coordination, π–π stacking and hydrogen bonding in the supramolecular self-assembly of bis(μ-7-iodo-8-hydroxyquinoline-5-sulfonato-κ³N,O:O′)bis[triaquanickel(II)] tetrahydrate

S. B. Raj, P. T. Muthiah, U. Rychlewska, B. Warżajtis, G. Bocelli and R. O'lla

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organic compounds

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Strong symmetrical intramolecular hydrogen bonds in diprotonated piperazinium bis(hydrogenmaleate)

Z. M. Jin, M. L. Hu, K. W. Wang, L. Shen and M. C. Li

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[2-(tert-Butylcarbonylmethylamino)phenyl]acetic acid

N. Raynal, M. Amblard, J. Martinez and M. Rolland

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Dimethyl iminiodiacetate chloride

M. Ramos Silva, J. A. Paixão, A. Matos Beja, A. J. F. N. Sobral, S. H. Lopes, N. G. C. L. Rebanda and A. M. d'A. Rocha Gonsalves

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Tetraphenylphosphonium chloride dihydrate

A. J. Blake, C. D. Garner and J. M. Tunney

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5-Methoxy-4-(4-methoxyphenyl)isochroman-3-ol

M. Palusiak, M. Małecka, A. Rybarczyk-Pirek, J. Epsztajn, A. Bieniek and J. A. Kowalska

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Hydrogen-bonded supramolecular motifs in trimethoprim–terephthalate–terephthalic acid (2/1/1)

M. Hemamalini, P. T. Muthiah, G. Bocelli and A. Cantoni

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5-(Benzo[1,3]dioxol-5-yl)-7-(4-chlorophenyl)-3-methyl-1-phenyl-1,6,7,8-tetrahydropyrazolo[3,4-b][1,4]diazepine

J. N. Low, J. Cobo, M. Nogueras, A. Sánchez, B. Insuasty and M. Mosquera

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3α,4β-Dihydroxy-5β-androstan-17-one

L. C. R. Andrade, J. A. Paixão, M. J. M. de Almeida, F. M. Fernandes Roleira, M. L. Sá e Melo, A. S. Campos Neves and E. J. Tavares da Silva

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(S)-4,16-Dihydroxymethyl-[2.2]paracyclophane bis-(1S)-camphanoate

P. G. Jones, J. Hillmer and H. Hopf

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2,2′-[1,4-Phenylenebis(methylenethio)]dithiazole

W. Zhang, H.-M. Liu, C.-B. Li and W.-Q. Zhang

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DL-Valinium perchlorate

B. Sridhar, N. Srinivasan, B. Dalhus and R. K. Rajaram

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DL-Methioninium trichloroacetate at 123 K

K. Rajagopal, R. V. Krishnakumar, A. Mostad and S. Natarajan

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2,2′-[1,2-Phenylenebis(methylenethio)]bis(5-methyl-1,3,4-thiadiazole)

Y. Zheng and H.-B. Liu

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3-Methoxy-1-(4-methoxyphenyl)-4,4-bis(methylsulfoxy)azetidin-2-one

J. R. Deschamps, M. McCain and M. Konaklieva

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Cilansetron hydrochloride monohydrate, modification A (monoclinic)

P. G. Jones, H. Möller and E. Finner

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Cilansetron hydrochloride monohydrate, modification B (orthorhombic)

P. G. Jones, H. Möller and E. Finner

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Dimethyl 1-(3-chloro-4-methylphenyl)pyrazole-3,4-dicarboxylate

S. Thamotharan, V. Parthasarathi, R. Sanyal, V. Badami Bharati and A. Linden

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An anomalous racemate of naringenin at 120 K

P. J. Cox, M. Jaspars, Y. Kumarasamy, L. Nahar and S. D. Sarker

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8-Chloro-4-[1-(phenylsulfonyl)indol-3-yl]-3a,4,5,9b-tetrahydro-3H-cyclopenta[c]quinoline

R. Sankaranarayanan, M. Yogavel, D. Velmurugan, K. Sekar, G. Babu, P. T. Perumal, S. Shanmuga Sundara Raj and H.-K. Fun

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2-Naphthalenol

B. Marciniak, E. Rozycka-Sokolowska and V. Pavlyuk

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2-Amino-7-methoxy-3-(1-methyl-1H-benzimidazol-2-yl)chromenium perchlorate

V. N. Baumer, A. A. Karasev and Z. A. Sizova

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2-Ethyl-3-hydroxy-1-morpholinopyridin-4(1H)-one

A. Decken, D. C. Sample, B. A. Noseworthy, C. M. Vogels and S. A. Westcott

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3-Chlorobenzoxazolo[3,2-b]isoquinolin-6-one

A. Usman, L. Wang, H.-K. Fun, K.-Q. Ling and J.-H. Xu

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5-Cyano-7-methoxy-2,2-dimethyl-4-oxochroman-6-yl acetate

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(5S,6R,7R,9R)-1-Benzyl-7,9-dimethyl-8-oxo-1-azaspiro[4.4]nonane-6-carbonitrile

D. Gravestock and J. M. McKenzie

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2-(Benzotriazol-1-ylmethyl)-1-phenyl-3-pyrazolidinone: two weak hydrogen bonds combine to form molecular ladders

J. N. Low, A. Quesada, J. Cobo, M. Nogueras, A. Sánchez, R. Abonia and H. Meier

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1,5-Bis(ethylsulfonyl)pentane

J.-R. Li, Y. Zheng, Y.-B. Xie, R.-Q. Zou, R.-H. Zhang and X.-H. Bu

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2-Cyclopentyl-2-hydroxy-2-phenylacetic acid, a pseudosymmetric crystal structure with space group Pna2₁ and Z′ = 2

J. W. Bats, M. Walter and C. R. Noe

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2-(4-Chlorophenyl)-4-(2-hydroxyethyl)-5-methyl-2,4-dihydro-3H-1,2,4-triazol-3-one

S. Thamotharan, V. Parthasarathi, V. Sunagar, B. Badami and A. Linden

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N-Methyl-4-piperidyl p-nitrobenzoate at 130 K

L. Andrau and J. White

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Succinimido 2-acetoxybenzoate

W. Zou, Y. Gao, T. Sugiyama, T. Matsuura and J. Meng

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1,4-Bis{2-hydroxy-3-[N-(2-hydroxyethyl)imino]-5-methylbenzyl}piperazine

M. Yogavel, S. Selvanayagam, D. Velmurugan, S. Shanmuga Sundara Raj, H.-K. Fun, M. Marappan and M. Kandaswamy

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Benzyl (2S)-2-tert-butoxycarbonylamino-5-(2-furyl)-5-oxopentanoate

W. Clegg, R. F. W. Jackson and N. Wishart

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9-Pentafluorophenylmethylene-9H-fluorene

M. J. Plater, R. A. Howie and D. M. Schmidt

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(Z)-3-[(1-Methylethyl)thiomethylene]-4-phenyl-1,4-pentadiene-1,1,2-tricarbonitrile

P. G. Jones, P. Bubenitschek, H. Hopf and M. Kreutzer

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Ethyl 4-acetyl-3,5-dimethyl-1H-pyrrole-2-carboxylate

J. A. Paixão, M. Ramos Silva, A. Matos Beja, A. J. F. N. Sobral, S. H. Lopes and A. M. d'A. Rocha Gonsalves

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Agatholic acid

R. B. Bates, S. Cai, R. S. Cantor, M. D. Carducci, A. K. Irvine, B. V. Jiorle, P. Nakkiew, W. N. Setzer and L. N. Trinh

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1,2-Bis[1-phenylsulfonyl-3-(phenylthio)indol-2-yl]ethene

R. Sankaranarayanan, M. Yogavel, D. Velmurugan, K. Sekar, P. C. Srinivasan, S. Shanmuga Sundara Raj and H.-K. Fun

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N-(4-Methoxyphenyl)quinoline-2-carboxamide

J. Y. Qi, L. Q. Qiu, Q. Y. Yang, Z. Y. Zhou and A. S. C. Chan

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N-(4-Iodophenyl)quinoline-2-carboxamide

J. Y. Qi, L. Q. Qiu, Q. Y. Yang, Z. Y. Zhou and A. S. C. Chan

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Research communications are designed to help authors bring out the science behind their structure determinations. Authors are encouraged to report more than one structure in the same communication and also to include the results of investigations with other techniques. The Research communications format makes Acta E the natural home for structure determinations with interesting science to report.

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Editorial Advisory Board

S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardA. LindenS. ParsonsM. RossiI. D. WilliamsM. Zema

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