Acta Cryst. (2005). E61, m1326-m1328  [ doi:10.1107/S1600536805018441 ]

The polymorph of racemic tris(2,4-pentanedionato-²O,O')vanadium(III), redetermined at 120 K

S. J. Kavitha, K. Panchanatheswaran, J. N. Low and C. Glidewell

Online 17 June 2005

Key indicators

• Single-crystal X-ray study
• T = 120 K
• Mean (Wave) = 0.000 Å
• R factor = 0.058
• wR factor = 0.135
• Data-to-parameter ratio = 18.7

checkCIF/PLATON results

No syntax errors found




Alert level B
RINTA01_ALERT_3_B  The value of Rint is greater than 0.15
            Rint given   0.174

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   0 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

Copyright © International Union of Crystallography
IUCr Webmaster