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Figure 1
The asymmetric unit of (3), with displacement ellipsoids drawn at the 50% probability level. H-atom radii are arbitrary. The difference density synthesis suggested the presence of two H atoms bonded to O8 on one mol­ecule and O108 on the other, each with 50% site occupancy. Atoms O37 and O38 carry three H atoms with 33% site occupancy. Atom O39 carries four H atoms with 25% site occupancy. This abnormal water molecule geometry is needed to explain the complex hydrogen-bond network (see Comment).

Journal logoCRYSTALLOGRAPHIC
COMMUNICATIONS
ISSN: 2056-9890
Volume 61| Part 7| July 2005| Pages o2155-o2157
https://doi.org/10.1107/S1600536805018489
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