Acta Cryst. (2006). E62, m574-m575  [ doi:10.1107/S1600536806005630 ]

fac-Dichlorotris(trimethylphosphine)(trimethylphosphoniomethyl)rhodium(III) chloride/bromide dichloromethane benzene solvate

A. S. Batsanov, T. B. Marder and F. Seeler

Online 22 February 2006

Key indicators

• Single-crystal X-ray study
• T = 120 K
• Mean (C-C) = 0.004 Å
• Disorder in solvent or counterion
• R factor = 0.030
• wR factor = 0.074
• Data-to-parameter ratio = 44.8

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT331_ALERT_2_B Small Average Phenyl C-C Dist.   C15    -C17_a         1.36 Ang.  

Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)...          ?
PLAT077_ALERT_4_C Unitcell contains non-integer number of atoms ..          ?
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................       6.00 Perc. 

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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