(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2008). E64, i5 [ doi:10.1107/S1600536807066354 ]

Dicaesium tetrachloridodioxidoplutonate(VI)

M. P. Wilkerson and B. L. Scott

Online 18 December 2007

Key indicators

Single-crystal X-ray study
T = 141 K
Mean (Pu-O) = 0.004 Å
R factor = 0.015
wR factor = 0.037
Data-to-parameter ratio = 26.3

checkCIF/PLATON results

No syntax errors found




Alert level B
ABSTM02_ALERT_3_B  The ratio of expected to reported Tmax/Tmin(RR) is > 1.50
            Tmin and Tmax reported:      0.150     0.286
            Tmin and Tmax expected:      0.062     0.188
            RR =      1.588
            Please check that your absorption correction is appropriate.
PLAT060_ALERT_3_B Ratio Tmax/Tmin (Exp-to-Rep) (too) Large .......       1.59      

Alert level C
CRYSC01_ALERT_1_C The word below has not been recognised as a standard
            identifier.
            golden
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       0.66      
PLAT194_ALERT_1_C Missing _cell_measurement_reflns_used datum ....          ?

Alert level G
ABSTM02_ALERT_3_G  When printed, the submitted absorption T values will be
            replaced by the scaled T values. Since the ratio of scaled T's
            is identical to the ratio of reported T values, the scaling
            does not imply a change to the absorption corrections used in
            the study.
            Ratio of Tmax expected/reported      0.658
            Tmax scaled      0.188 Tmin scaled      0.099

   0 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check