Acta Cryst. (2010). E66, m229-m230  [ doi:10.1107/S1600536810003259 ]

Di--chlorido-bis{[2-({[2-(2-pyridyl)ethyl](2-pyridylmethyl)amino}methyl)phenol]zinc(II)} bis(perchlorate) dihydrate

S. E. Coelho, G. G. Terra and A. J. Bortoluzzi

Online 30 January 2010

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT214_ALERT_2_B Atom O4P     (Anion/Solvent) ADP max/min Ratio         5.20 prola

Alert level C
PLAT214_ALERT_2_C Atom O3P     (Anion/Solvent) ADP max/min Ratio         4.40 oblat
PLAT221_ALERT_2_C Large Solvent/Anion  O     Ueq(max)/Ueq(min) ...       3.94 Ratio
PLAT230_ALERT_2_C Hirshfeld Test Diff for    N32    --  C31     ..       5.02 su   
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C35     
PLAT341_ALERT_3_C Low Bond Precision on  C-C Bonds (x 1000) Ang ..          8      
PLAT417_ALERT_2_C Short Inter D-H..H-D       H1WA   ..  H10     ..       2.10 Ang. 
PLAT417_ALERT_2_C Short Inter D-H..H-D       H1WB   ..  H10     ..       2.11 Ang. 
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.596          5      
PLAT234_ALERT_4_C Large Hirshfeld Difference C34    --  C35     ..       0.15 Ang. 
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of         Cl2     

Alert level G
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......        124      
PLAT128_ALERT_4_G Non-standard setting of Space-group P21/c   ....      P21/n      
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported   _diffrn_ambient_temperature        293 K    
PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ...................      40.00 Perc.
PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels ..........          6      
PLAT793_ALERT_4_G The Model has Chirality at N1      (Verify) ....          R      

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
  10 ALERT level C = Check and explain
   7 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   7 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   6 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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