Acta Cryst. (2011). E67, m1392  [ doi:10.1107/S1600536811037214 ]

Dichlorido{2-[(thiophen-2-ylmethyl)iminomethyl]pyridine-²N,N'}palladium(II)

M. O. Onani and W. M. Motswainyana

Online 17 September 2011

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.007 Å
• Disorder in main residue
• R factor = 0.042
• wR factor = 0.144
• Data-to-parameter ratio = 17.8

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...        3.4 Ratio
PLAT245_ALERT_2_C U(iso) H6A     Smaller than U(eq) C7B     by ...      0.016 AngSq
PLAT420_ALERT_2_C D-H Without Acceptor      *S8B    -  *H5A    ...          ?      
PLAT420_ALERT_2_C D-H Without Acceptor      *S8A    -  *H5B    ...          ?      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         17      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600        240      

Alert level G
PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite         11      
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?
PLAT301_ALERT_3_G Note: Main Residue  Disorder ...................         29 Perc.
PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms ....          !
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......         26      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   6 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   5 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   5 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   2 ALERT type 5 Informative message, check

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