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Acta Cryst. (2012). E68, o2017  [ doi:10.1107/S1600536812022143 ]

2-{[3-Methyl-4-(2,2,2-trifluoroethoxy)pyridin-2-yl]methylsulfanyl}-1H-benzimidazole propan-2-ol monosolvate: a second monoclinic polymorph

J.-J. Ma, M.-H. Qi, M.-H. Hong, J. Lu and G.-B. Ren


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Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.970 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C15 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 4 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.597 100
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 2 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C16 PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 7 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 89 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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