[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1047
[ doi:10.1107/S160053681203067X ]

Tris[2,4-dichloro-6-(ethyliminomethyl)phenolato-[kappa]2N,O]cobalt(III)

Q. P. Huang, J. J. Guo, Y. D. Zhang and S. H. Zhang

Key indicators

checkCIF/PLATON results

No syntax errors found






Alert level B
PLAT230_ALERT_2_B Hirshfeld Test Diff for    N9     --  C80     ..        8.4 su   
PLAT601_ALERT_2_B Structure Contains Solvent Accessible VOIDS of .        118 A   3
Author Response: No significant electron density was located in these voids. NOTE from co-editor: the SQUEEZE option was not used. 

Alert level C
PLAT234_ALERT_4_C Large Hirshfeld Difference C17    --  C18     ..       0.17 Ang. 
PLAT234_ALERT_4_C Large Hirshfeld Difference C80    --  C81     ..       0.16 Ang. 
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C22     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C44     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C62     
PLAT341_ALERT_3_C Low Bond Precision on  C-C Bonds ...............     0.0072 Ang  
PLAT360_ALERT_2_C Short  C(sp3)-C(sp3) Bond  C80    -   C81    ...       1.40 Ang. 
PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ...     -0.354      
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          1      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         15      


Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large.       9.52      
PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c   .......      P21/n      
PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L=  0.600        148      


   0 ALERT level A = Most likely a serious problem - resolve or explain
   2 ALERT level B = A potentially serious problem, consider carefully
  10 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   4 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   7 ALERT type 2 Indicator that the structure model may be wrong or deficient
   4 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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