[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o40-o41
[ doi:10.1107/S1600536812047976 ]

Ethyl 2,7,7-trimethyl-4-(1-methyl-1H-indol-3-yl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

S. Öztürk Yildirim, R. J. Butcher, M. G. Gündüz, A. El-Khouly, R. Simsek and C. Safak

Key indicators

checkCIF/PLATON results

No syntax errors found

Alert level C PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT793_ALERT_4_G The Model has Chirality at C7 (Verify) .... S PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 131
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 1 ALERT level C = Check. Ensure it is not caused by an omission or oversight 3 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check
checkCIF publication errors
Alert level A PUBL024_ALERT_1_A The number of authors is greater than 5. Please specify the role of each of the co-authors for your paper.
Author Response: As the reported work is a part of collaboration between three Universities. Hence the number of authors are greater than 5. Synthesis has been carried out by M. G. G\"und\"uz, A. El-Khouly, C. \,Safak and R. \,Simsek while S. \"Ozt\"urk Yildirim and R. J. Butcher are responsible for the single crystal growth, X-ray data collection, refinement of the structure, structure completion in the form of paper.

1 ALERT level A = Data missing that is essential or data in wrong format 0 ALERT level G = General alerts. Data that may be required is missing

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