Acta Cryst. (2013). E69, m58
[ doi:10.1107/S1600536812050234 ]

Tris(2,2'-bipyridine-²N,N')cobalt(II) bis(hexafluoridophosphate)

A. Mentes and K. Singh

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.008 Å
• R factor = 0.049
• wR factor = 0.088
• Data-to-parameter ratio = 13.6

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT214_ALERT_2_C Atom F2      (Anion/Solvent) ADP max/min Ratio          4.2 prola
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of          P1     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of          P2     
PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor ....        2.6      
PLAT341_ALERT_3_C Low Bond Precision on  C-C Bonds ...............     0.0078 Ang  

Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details  in the CIF          ?
PLAT152_ALERT_1_G The Supplied and Calc. Volume s.1. Differ by ...          4 Units
PLAT870_ALERT_4_G ALERTS Related to Twinning Effects Suppressed ..          !
PLAT931_ALERT_5_G Check Twin Law ( 1 1  0)[       ] Estimated BASF       0.18      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   5 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   4 ALERT level G = General information/check it is not something unexpected

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   2 ALERT type 5 Informative message, check

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