[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o691-o692
[ doi:10.1107/S1600536813008544 ]

N-{1,2-Bis(pyridin-3-yl)-2-[(E)-(pyridin-3-yl)methylideneamino]ethyl}nicotinamide

C. M. Quiroa-Montalván, D. Chávez, R. Reyes-Martínez, D. Morales-Morales and M. Parra-Hake


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for N12 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C27 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C3 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C7 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C14 PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0051 Ang PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond C20 - C21 ... 1.35 Ang. PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond C21 - C22 ... 1.38 Ang. PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond C26 - C27 ... 1.35 Ang. PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond C27 - C28 ... 1.38 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 15.245 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.199 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 11
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 9 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 6 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 10 Perc. PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 48 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 5
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 13 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 11 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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