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Acta Cryst. (2013). E69, o1021  [ doi:10.1107/S1600536813014931 ]

(E)-1-(3-Chlorophenyl)-2-(2-oxidonaphthalen-1-yl)diazen-1-ium

A. Benosmane, A. Mili, H. Bouguerria and A. Bouchoul


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Alert level C PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0052 Ang PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.565 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 4 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 16 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 2 PLAT921_ALERT_1_C R1 in the CIF and FCF Differ by ............... 0.0016 PLAT922_ALERT_1_C wR2 in the CIF and FCF Differ by ............... 0.0044 PLAT923_ALERT_1_C S values in the CIF and FCF Differ by ....... 0.024 PLAT926_ALERT_1_C Reported and Calculated R1 Differ by ......... 0.0016 PLAT927_ALERT_1_C Reported and Calculated wR2 Differ by ......... 0.0043
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 1 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT333_ALERT_2_G Check Large Av C6-Ring C-C Dist. C7 -C12 1.43 Ang. PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 4
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 10 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 7 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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