Acta Crystallographica Section C
Acta Crystallographica
Section C STRUCTURAL CHEMISTRY

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STRUCTURAL
CHEMISTRY

Volume 40| Part 1

ISSN: 2053-2296

January 1984 issue

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inorganic compounds

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The charge-density study of the Laves phases, MgZn₂ and MgCu₂

T. Ohba, Y. Kitano and Y. Komura

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The structure of hexapotassium disodium hexatungstoplatinate(IV) dodecahydrate, K₆Na₂[PtW₆O₂₄].12H₂O

U. Lee, H. Ichida, A. Kobayashi and Y. Sasaki

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Uranyl hydroxide sulphamate trihydrate, UO₂(OH)(NH₂SO₃).3H₂O

J. Toivonen and R. Laitinen

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Synthèse et structure d'un nouveau titanoniobate: le trititanotétraniobate de dibaryum, Ba₂Ti₃Nb₄O₁₈

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Cobalt(III) lithium oxide, CoLiO₂: structure refinement by powder neutron diffraction

H. J. Orman and P. J. Wiseman

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Dicesium magnesium bis(chromate) hexahydrate, Cs₂Mg(CrO₄)₂.6H₂O

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Barium aquacobalto(III)undecatungstoborate(6–) 26-water, Ba₃[BCo(H₂O)W₁₁O₃₉].26H₂O

T. J. R. Weakley

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Structure of strontium selenate, SrSeO₄

H. Prévost-Czeskleba and H. Endres

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metal-organic compounds

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Structure of (bicyclo[2.2.1]hepta-2,5-diene)[(−)-(R,R)-2-exo,3-endo-bis(diphenylphosphino)bicyclo[2.2.1]heptane]rhodium(I) perchlorate tetrahydrofuran solvate, C₃₈H₃₈P₂Rh⁺.ClO₄⁻.C₄H₈O, the penultimate catalyst precursor in asymmetric reductions using the norphos ligand

R. E. Davis, B. B. Meyer, K. L. Hassett, P. N. Juri and E. P. Kyba

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Structure de l'aqua(aza-4 azonia-1 bicyclo[2.2.2]octane)trinitratocadmium(II), Cd(C₆H₁₃N₂)(H₂O)(NO₃)₃

B. Viossat, P. Khodadad and N. Rodier

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Structure of a nine-membered palladacycloalkane, bis[dimethyl(phenyl)phosphine]-3,3,6,6,9,9,13,13-octamethyl-anti,syn,anti,syn-11-palladapentacyclo[10.1.0.0²,⁴.0⁵,⁷.0⁸,¹⁰]tridecane, C₃₆H₅₄P₂Pd

H. M. Büch and C. Krüger

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Structure of lithium diisopropyldithiocarbamate trihydrate, Li⁺.C₇H₁₄NS₂⁻.3H₂O

Å. Oskarsson and I. Ymén

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Structure of lithium dimethyldithiocarbamate tetrahydrate, Li[C₃H₆NS₂].4H₂O

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The structure of hexakis(tetramethylammonium) dihydrogendodecatungstate enneahydrate, [(CH₃)₄N]₆[H₂W₁₂O₄₀].9H₂O

M. Asami, H. Ichida and Y. Sasaki

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Structure of cis-[3,4-bis(trifluoromethyl)-2,5-dithiahexane]dichloroplatinum(II), cis-[Pt{CH₃SCH(CF₃)CH(CF₃)SCH₃}Cl₂]

W. N. Hunter, K. W. Muir and D. W. A. Sharp

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Structure of carbonyldichloro(cyclopropyl)bis(methyldiphenylphosphine)iridium(III), [IrCl₂(C₃H₅)(CO){P(CH₃)(C₆H₅)₂}₂]

P. N. Swepston, N. L. Jones, J. A. Ibers, M.-Y. Shang, J.-L. Huang and J.-X.(C.-S.) Lu

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The structure of tetrakis(acetato)bis(4-pyridinecarbonitrile)dirhodium(II) acetonitrile solvate, [Rh₂(O₂CCH₃)₄(C₆H₄N₂)₂].CH₃CN

F. A. Cotton and T. R. Felthouse

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Structure of a novel one-dimensional chlorpromazine–copper(II) complex salt, [C₁₇H₂₀ClN₂S]₂[CuCl₄]₂

A. Obata, H. Kawazura and H. Miyamae

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Structure of oxonium tris(triethylammonium) octamolybdate(4–) dihydrate, (C₆H₁₆N)₃(H₃O)[Mo₈O₂₆].2H₂O

P. K. Bharadwaj, Y. Ohashi, Y. Sasada, Y. Sasaki and T. Yamase

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Structure of calcium acetate monohydrate, Ca(C₂H₃O₂)₂.H₂O

E. A. Klop, A. Schouten, P. van der Sluis and A. L. Spek

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Structure of 1,3-(1,1'-ruthenocenediyl)propane, C₁₃H₁₄Ru, and 1,4-(1,1'-ruthenocenediyl)butane, C₁₄H₁₆Ru

S. Ohba, Y. Saito, S. Kamiyama and A. Kasahara

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Hexaaquanickel(II) dipotassium tetrahydrogen tetra-o-phthalate tetrahydrate, K₂[Ni(H₂O)₆][C₈H₅O₄]₄.4H₂O

M. Biagini Cingi, A. M. Manotti Lanfredi and A. Tiripicchio

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Calcium naphthionate octahydrate, Ca²⁺.2C₁₀H₈NO₃S⁻.8H₂O

C. J. Brown, M. Ehrenberg and H. R. Yadav

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The structure of (2,2'-bipyridine)dichlorozinc(II), Zn(C₁₀H₈N₂)Cl₂

M. A. Khan and D. G. Tuck

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The structure of the lead salt of 2,4,6-trinitro-1,3-benzenediol monohydrate (α polymorph), α-Pb²⁺.C₆HN₃O₈²⁻.H₂O

M. A. Pierce-Butler

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Structure of tribromobis(pyridine)thallium(III), TlBr₃(C₅H₅N)₂

S. E. Jeffs, R. W. H. Small and I. J. Worrall

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The structure of bis[2-amino-2-hydroxymethyl-1,3-propanediolato(1–)-O,N]copper(II)–sodium perchlorate monohydrate, [Cu(C₄H₁₀NO₃)₂].NaClO₄.H₂O

G. J. M. Ivarsson

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X-ray molecular structure of the orange isomer of (5,7,7,12,14,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene)copper(II) perchlorate, [Cu(C₁₆H₃₂N₄)](ClO₄)₂

T.-J. Lee, T.-H. Lu, C.-S. Chung and T.-Y. Lee

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Structures of three polymeric complexes [silver(I) nitrate]_x–1,4-oxathiane, (AgNO₃)_x.C₄H₈OS [x = 1 (I), 2 (II), 6 (III)]

J. C. Barnes and J. D. Paton

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Dichloro[phenyldi(2-pyridyl)phosphine-N,N']cobalt(II) hemiethanolate, [Co(C₁₆H₁₃N₂P)Cl₂].1/2C₂H₆O

M. G. Ehrlich, F. R. Fronczek, S. F. Watkins, G. R. Newkome and D. C. Hager

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Monopotassium salt of 4-methyl[1,2,5]thiadiazolo[3,4-c][1,2,6]thiadiazine-7(6H)-one 5,5-dioxide, C₄H₃N₄O₃S₂⁻.K⁺

C. Esteban-Calderón, M. Martínez-Ripoll and S. García-Blanco

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Structure of (L-alanyl-L-histidinato)copper(II) 3.5-hydrate, [Cu(C₉H₁₂N₄O₃)].3.5H₂O

Y. Mauguen, E. Vilkas and C. Amar

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Structure of cis-bis(2,2'-bipyridine)bis(benzenethiolato)nickel(II) dideuteriohydrate, [Ni(C₁₀H₈N₂)₂(C₆H₅S)₂].D₂O

K. Osakada, T. Yamamoto, A. Yamamoto, A. Takenaka and Y. Sasada

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organic compounds

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Structures of (Z)-3,4-diethyl-5-(phenylmethylene)-3-pyrrolin-2-one, C₁₅H₁₇NO (I), and (Z)(syn)-3,4-dimethyl-5-(2-pyridylmethylene)-3-pyrrolin-2-one, C₁₂H₁₂N₂O (II)

J. K. Dattagupta, E. F. Meyer Jnr, D. L. Cullen, D. A. Lightner, H. Falk, K. Grubmayr and I. Bernal

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Third (γ) polymorph of tri-tert-butylmethyl p-nitrobenzoate, C₂₀H₃₁NO₄

W. Wong-Ng, P.-T. Cheng and S. C. Nyburg

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α-(4-Methyl-2-nitrophenylhydrazono)acetanilide, C₁₅H₁₄N₄O₃

C. J. Brown and H. R. Yadav

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5-Deoxy-5-hydroperoxytelekin O-methyl derivative and its pyrazoline adduct, C₁₆H₂₂O₄ and C₁₇H₂₄N₂O₄

G. Appendino, M. Calleri, G. Chiari and D. Viterbo

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4aβ,5,8,8aβ-Tetrahydronaphthoquin-1α,4α-diol, C₁₀H₁₄O₂

S. Ariel and J. Trotter

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Structures of thianthrene (I), C₁₂H₈S₂, (redeterminations at 163 K and 295 K) and 1-azathianthrene (II), C₁₁H₇NS₂, (at 163 K)

S. B. Larson, S. H. Simonsen, G. E. Martin, K. Smith and S. Puig-Torres

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Structure of diphenylthiophosphinic acid, (C₆H₅)₂P(=S)OH, at 140 K

R. Mattes and D. Rühl

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Structure of 5-amino-4-phenyl-3,4-dihydro-2H-pyrrol-2-one, C₁₀H₁₀N₂O

P. Gluziński, J. Rajewski, J. Lange, G. D. Andreetti and G. Bocelli

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Structure of cyclo(-L-Pro-L-Val-L-Pro-L-Val-) dimethyl sulfoxide solvate, C₂₀H₃₂N₄O₄.C₂H₆OS

I. Ueda, T. Ueda, I. Sada, T. Kato, M. Mikuriya, S. Kida and N. Izumiya

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Structure of the 1:1 complex of 1,4-dithiintetracarboxylic N,N'-dimethyldiimide and acridine, [C₁₀H₆N₂O₄S₂][C₁₃H₉N]

Y. Yamaguchi and I. Ueda

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Structure of 1-(p-dimethylaminophenyl)-3-(mercaptoacetyl)urea, C₁₁H₁₅N₃O₂S

A. Uchida, Y. Ohashi, Y. Sasada, Y. Kaneko and T. Endo

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Structure of 1-(p-dimethylaminophenyl)-3-(phenylacetyl)urea, C₁₇H₁₉N₃O₂

Y. Ohashi, A. Uchida, Y. Sasada, K. Kinoshita and T. Endo

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Structure of the 1:1 complex of 1-(p-dimethylaminophenyl)-3-(phenylacetyl)urea and 1-isobutyl-3-(p-nitrobenzoyl)urea, C₁₇H₁₉N₃O₂.C₁₂H₁₅N₃O₄

A. Uchida, Y. Ohashi, Y. Sasada, M. Moriya and T. Endo

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Structure of 11,12-dichloro-9,10-ethano-9,10-dihydro-1-anthroic acid methyl ester, C₁₈H₁₄Cl₂O₂

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cis-3,6-Diethoxy-1,2,4,5-tetraaza-3,6-diphosphacyclohexan-3,6-disulfid, C₄H₁₄N₄O₂P₂S₂

H. Viertel and U. Engelhardt

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Structure of 5-cinnamoyl-1,3-dimethyl-6-[(2-morpholinoethyl)amino]uracil hydrochloride, C₂₁H₂₇N₄O₄⁺.Cl⁻

V. Warin, F. Baert, J. L. Bernier and J. P. Henichart

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Structure of 2,2,6,6-tetramethylpiperidinium bromide, C₉H₂₀N⁺.Br⁻

M. D. Walkinshaw, A. H. Cowley and S. K. Mehrotra

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The structure of N-[3-(3-ammoniopropylammonio)propyl]succinamic acid sulfate, C₁₀H₂₃N₃O₃²⁺.SO₄²⁻

J. S. Suh, Z. B. Xu, K. Hofmann, C. S. Yoo and M. Sax

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The structure of 4-hydroxy-2,3,4-triphenyl-2-cyclopenten-1-one benzene solvate C₂₃H₁₈O₂.1/2C₆H₆

K. Vyas and H. Manohar

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A 1:2 host–guest complex between 1,4,7,10,13,16-hexaoxacyclooctadecane (18-crown-6) and N,N'-diformohydrazide, C₁₂H₂₄O₆.2C₂H₄N₂O₂

M. R. Caira, W. H. Watson, F. Vögtle and W. Müller

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Refined structure of phenazine–iodine molecular complex, C₁₂H₈N₂.I₂

T. Uchida and K. Kimura

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Methyl (diphenylmethylimino)acetate N-oxide, C₁₆H₁₅NO₃

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Acetyltriphenylmethane, C₂₁H₁₈O

M. N. Ponnuswamy and J. Trotter

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Structure of 5-benzoyl-4-(p-chlorophenyl)-2,2,5-triphenyl-Δ³-1,3-oxazoline, C₃₄H₂₄ClNO₂

C. Ruiz-Valero, E. Gutiérrez-Puebla and A. Monge

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The structure of phyllanthocindiol methyl ester, C₂₅H₃₂O₈

L. R. Nassimbeni, M. L. Niven, G. M. Cragg and G. R. Pettit

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Structure of N-(3-dimethylaminopropyl)dithiocarbamic acid, C₆H₁₄N₂S₂

V. Schramm, S. C. Kokkou and P. Karagiannidis

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Structure de la raubasine hydratée, C₂₁H₂₄N₂O₃.H₂O

J.-P. Dubost, J.-M. Léger, M. Goursolle, J.-C. Colleter and A. Carpy

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Structure of 3,4-dihydro-2-[(p-hydroxyphenethyl)aminomethyl]-1(2H)-naphthalenone hydrochloride, BE-2254, C₁₉H₂₁NO₂.HCl

A. Carpy, J.-M. Léger and J.-C. Colleter

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Hemanthamine, C₁₇H₁₉NO₄

W. H. Watson, J. Galloy and M. Silva

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Structure of 3α,7α-bis(2-hydroxy-2-propyl)bicyclo[3.3.1]nonane, C₁₅H₂₈O₂

H. van Koningsveld, J. A. Peters and J. C. Jansen

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Bis[2-(o-methoxyphenoxy)ethyl] ether–urea (1:1) complex, C₁₈H₂₂O₅.CH₄N₂O

K. K. Chacko, P. Narasimhan and W. Saenger

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Structure and absolute configuration of (+)-doronine–benzene (1:1), C₂₁H₃₀ClNO₈.C₆H₆

R. Y. Wong and J. N. Roitman

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Structure of N-acetyl DL-phenylalanine p-nitroanilide, C₁₇H₁₇N₃O₄

B. K. Sinha, V. Pattabhi, S. Raghunathan and E. J. Gabe

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L-Tyrosyl-L-glutamic acid monohydrate, C₁₄H₁₈N₂O₆.H₂O

J. Pandit, T. P. Seshadri and M. A. Viswamitra

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Structure of cyclo(-L-Pro-L-Pro-Gly-L-Pro-L-Leu-Gly-) methanol solvate monohydrate, C₂₅H₃₈N₆O₆.CH₃OH.H₂O

T. Nakashima, T. Yamane, I. Tanaka and T. Ashida

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Structure of guanidinomethylphosphonic acid monohydrate, C₂H₈N₃O₃P.H₂O

W. Sawka-Dobrowolska, T. Głowiak and R. Tyka

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Structure of cataline, C₂₁H₂₅NO₅, a non-phenolic aporphine alkaloid

I. Fonseca and S. García-Blanco

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Structures of trans-6,7-dibromo-8-oxabicyclo[3.2.1]octan-3-one, C₇H₈Br₂O₂, and 6-bromo-8-oxabicyclo[3.2.1]oct-6-en-3-one, C₇H₇BrO₂

M. M. Olmstead, H. Hope, V. Sampath and N. E. Schore

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Structure of telluric acid–glycine (1:2) monohydrate, Te(OH)₆.2C₂H₅NO₂.H₂O, at 120 K and determination of hydrogen positions

D. Tran Qui, J. Vicat and A. Durif

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(1R,1'R,2S,2'S,3R,3'R,5R,5'R,6S,6'S)-3-Hydroxy-3'-trimethylsilyloxy[3,3'-bitricyclo[4.2.1.0²,⁵]non-7-enyl]-4,4'-dione, C₂₁H₂₆O₄Si

J. W. Bats, O. Bellinger and W. Ried

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Structure of 5,2'-anhydro-5-(p-toluenesulfonamido)-1-(3'-O-tosyl-β-D-arabinofuranosyl)imidazole-4-carbonitrile, C₂₃H₂₂N₄O₇S₂

S. Sugio, H. Mizuno, K. Kitamura, M. Ikehara and K.-i. Tomita

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Structure of 1-(p-ethoxyphenyl)-1,3-dihydro-3-phenyl-2H-benzimidazole-2-thione, C₂₁H₁₈N₂OS

A. Criado, A. Conde and R. Márquez

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2-(1,3-Dithiol-2-ylidene)-4-cyclopentene-1,3-dione, C₈H₄O₂S₂, and 2-(1,3-benzodithiol-2-ylidene)cyclohexanone, C₁₃H₁₂OS₂

W. H. Watson, J. Galloy, D. A. Grossie and J. Nakayama

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Structure of 9-annulene derivatives. 3. 7H-Benzocyclononen-7-ol, C₁₃H₁₂O

Mazhar-ul-Haque, J. Ahmed and W. Horne

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The structure of monacolin K, C₂₄H₂₆O₅

S. Sato, T. Hata, Y. Tsujita, A. Terahara and C. Tamura

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Structure and absolute configuration of (8R)-8-benzyloxy-6-(1,3-dioxan-2-yl)-1,4-dithiaspiro[4.4]non-6-ene, C₁₈H₂₂O₃S₂

J. C. Barrière, A. Chiaroni, J. Cléophax, S. D. Géro and C. Riche

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A 1:1 complex of 2,9-dimethyl-1,10-phenanthroline and resorcinol, C₁₄H₁₂N₂.C₆H₆O₂

W. H. Watson, J. Galloy, F. Vögtle and W. M. Müller

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Molecular compounds and complexes. XV. Pyrene–1,4,5,8-naphthalenetetrone (1:1), C₁₆H₁₀.C₁₀H₄O₄

F. H. Herbstein and G. M. Reisner

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The structure of p-iodobenzoic acid, C₇H₅IO₂

R. G. Baughman and J. E. Nelson

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