A comparison of the X-ray single-crystal structure of Li₃SbO₄ with the Rietveld refinement

A comparison between the Rietveld and single-crystal X-ray structures of trilithium antimony tetraoxide, Li₃SbO₄, shows that the first method can yield a poor description of the structure, while the second gives more accurate geometric parameters.

Na₃Co(NO₂)₆ at 293 and 10 K

Precise X-ray structural determinations of Na₃Co(NO₂)₆ at 293 and at 10 K have been performed. The CoN₆ core is quite close to octahedral in stereochemistry. The accurate and extensive data sets collected should be suitable for charge–density analysis studies.

Di-μ-phenyl­thio-bis­[bis­(η⁵-methyl­cyclo­penta­dienyl)(tetra­hydro­furan)lanthanum(III)] bis­(tetra­hydro­furan) solvate

catena-Poly[aquacopper(II)-μ-[N-(1-oxido-2-naphthylmethylene)glycinato-O,N,O′:O′]]

[H₃N(CH₂)₂NH₃]_0.5[BePO₄], a beryllophosphate analogue of aluminosilicate zeolite gismondine

[H₃N(CH₂)₂NH₃]_0.5[BePO₄] is the first organically templated beryl­lophosphate to crystallize with an aluminosilicate zeolite topology. A three-dimensional network of BeO₄ and PO₄ tetrahedra corresponding to the gismondine (GIS) framework encapsulates disordered ethyl­enedi­ammonium cations.

Bis{μ-2-[(1,5-di­aza-1-cyclooctyl)methyl]phenolato-N,N′,O:O}bis­[chlorozinc(II)] diacetone solvate: design of a square-pyramidal ZnN₂O₂Cl complex

(Nitro-κN)[2-(phenyldiazenyl-κN²)pyridine-κN](2,2′:6′,2′′-terpyridine-κ³N)ruthenium(II) tetra­fluoroborate

Three mono­alk­oxy-substituted nido-platinaboranes: [(PPh₃)₂PtB₁₀H₁₁-8-(OCH₃)], [(PPh₃)₂PtB₁₀H₁₁-8-{OCH(CH₃)₂}] and [(PPh₃)₂PtB₁₀H₁₀-9-{OCH(CH₃)₂}]

η⁵-(3)-1-Methyl-1,2-dicarbollyl-η⁵-2′,5′-di­methylpyrrolylcobalt(III)

Tetra­kis­(di­methyl­amido)­vanadium(IV)

Comparative X-ray study of three nickel(II)–thio­cyanate compounds

A low-temperature neutron diffraction study of Mn₁₂-acetate

The low-temperature structure of the title dodecanuclear mixed-valence manganese carboxyl­ate, [Mn₁₂O₁₂(CD₃COO)₁₆(H₂O)₄]·2CD₃COOH·4H₂O, is similar to the room-temperature structure, differing by a small change in the configuration of one of the coordinated acetate groups, related to additional hydrogen bonding.

A mixed-valence manganese(III)–manganese(IV) di-μ-oxo complex, [(cyclam)MnO]₂(ClO₄)₂(NO₃)

Hydrogen-bonded adducts of ferrocene-1,1′-diyl­bis­(di­phenyl­methanol): monomeric and dimeric 1:1 adducts with 1,2-bis­(4-pyridyl)­ethane and 1,2-di­amino­ethane

[6-Amino-3-methyl-5-nitro­sopyrimidine-2,4(1H,3H)-dionato]­sodium dihydrate at 150 K: coordination-polymer ladders linked by hydrogen bonds

Sodium 2-nitro­ethanaloximate forms a layered-framework structure

Iodo­(phthalocyaninato)­chromium(III)

5,6-Di­phenyl­[1,3]­dithiolo­[4,5-b]di­thiine-2-thione

Investigations on benz­[1,2]­oxaphos­phinane derivatives

Di­methyl N,N′-ox­alamido­diethano­ate

Di­ethyl 4-(2,5-di­meth­oxy­phenyl)-2,6-di­methyl-1,4-di­hydro­pyridine-3,5-di­carboxyl­ate, conformational change with solvent of crystallization

The lock-in phase in the urotropine–sebacic acid system

Polymorphism in pentacene

Triclinic and orthorhombic polymorphs of 2-iodo-4-nitro­aniline: interplay of hydrogen bonds, nitro⋯I interactions and aromatic π–π-stacking interactions

Hydrogen-bonded chains in N-(2-nitro­phenyl)phenylamine

N,N′-Bis­[tris­(hy­droxy­methyl)­methyl]­ethanedi­amide: six O—H⋯O hydrogen bonds generate only a two-dimensional structure

N,N′-Di­methyl­piperazinium(2+) phos­phono­acetate: hydrogen-bonded anion sheets containing cation-templated R₆⁶(28) rings

Hydrogen-bonded bilayers in piperazinium(2+) bis­(mandelate) bis­(methanol) solvate

Hamigerin A and a hamigerin D decomposition product

Differently coloured polymorphs of 4-[(2-nitro­phenyl)azo]phenol

Zwitterionic 4-piperidine­carboxylic acid monohydrate

trans-1,2,3-Tris(1-hydroxycyclo­propyl)cyclo­propane

1,2-Bis(N-fluoro-p-toluene­sulfon­amido)­ethane chloroform solvate

Di­methyl 2-{[2-(meth­oxy­carbonyl)-1-(meth­oxy­carbonyl­methyl)pyrrol-4-yl]­methyl­ene}propane­dioate

N-Z-Pro–D-Leu using synchrotron radiation data from a very small crystal

Meth­oxy-ether and crown-ether derivatives of tetrahomodioxa- and octahomo­tetraoxacalix­[4]­arenes

Thermal isomerization pathway of 1-(4-nitro­phenyl)-2-phenyl­imino-2,5-di­hydro-1H-pyrido­[3,2-b]­indole-3-carbo­nitrile discovered by laboratory powder data

2-(N,N-Di­phenylamino)benzoic acid

1H-Pyrrole-2-carbo­thio­amide

N-tert-Butyl-N′-(5,7-di­methyl-1,8-naphthyridin-2-yl)­urea

MEM(TCNQ)₂ at room temperature and 10 K, and the absence of a spin-Peierls transition

Diiso­propyl­ammonium hydrogen difluoride

Conformational polymorphs of 22-cyano-N-methyl-5-phenylpent-2-en-4-ynamide