addenda and errata\(\def\hfill{\hskip 5em}\def\hfil{\hskip 3em}\def\eqno#1{\hfil {#1}}\)

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ISSN: 1600-5775

ID23-2: an automated and high-performance microfocus beamline for macromolecular crystallography at the ESRF. Corrigendum

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aEuropean Synchrotron Radiation Facility, 71 Avenue des Martyrs, F-38000 Grenoble, France, bEuropean Molecular Biology Laboratory, 71 Avenue des Martyrs, 38042 Grenoble, France, and cARINAX, 365 Rue de Corporat, 38430 Moirans, France
*Correspondence e-mail: max.nanao@esrf.fr

A revised version of Table 2 of Nanao et al. [J. Synchrotron Rad. (2022). 29, 581–590] is provided.

Some of the values reported in Table 2[link] of Nanao et al. (2022[Nanao, M., Basu, S., Zander, U., Giraud, T., Surr, J., Guijarro, M., Lentini, M., Felisaz, F., Sinoir, J., Morawe, C., Vivo, A., Beteva, A., Oscarsson, M., Caserotto, H., Dobias, F., Flot, D., Nurizzo, D., Gigmes, J., Foos, N., Siebrecht, R., Roth, T., Theveneau, P., Svensson, O., Papp, G., Lavault, B., Cipriani, F., Barrett, R., Clavel, C. & Leonard, G. (2022). J. Synchrotron Rad. 29, 581-590.]) were found to be incorrect. The full correct table is shown below.

Table 2
Data collection and refinement statistics

Statistics for the highest-resolution shell are shown in parentheses. For the MeshAndCollect data, the average cell edge and range are provided. A refinement was not performed for these data.

  Cubic insulin helical Cubic insulin MeshAndCollect
Wavelength (Å) 0.873 0.873
No. of crystals 1 142
Resolution range (Å) 39.28–1.203 (1.246–1.203) 32.07–1.750 (1.80–1.75)
Space group I213 I213
Unit cell
a, b, c (Å) 78.50 78.47 (78.27–78.73)
α, β, γ (°) 90 90
Total reflections 2269388 (146102) 1257717 (95649)
Unique reflections 25126 (2395) 15814 (1184)
Multiplicity 90.3 (58.7) 79.53 (80.78)
Completeness (%) 99.45 (95.30) 100 (99.7)
I/σ(I)〉 30.66 (1.26) 25.48 (1.36)
Wilson B factor 17.03 13.18
Rmeas 0.106 (2.697) 0.155 (4.143)
CC1/2 1 (0.565) 1 (0.685)
Anomalous correlation (inner) 2 3
SigAno 0.816 0.842
Reflections used in refinement 23764 (1661)
Reflections used for Rfree 1264 (89)
Rwork 0.150 (0.297)
Rfree 0.164 (0.319)
CCwork 0.952
CCfree 0.948
No. of non-hydrogen atoms 457
Macromolecules 335
Solvent 122
Protein residues 50
RMS (bonds) 0.021
RMS (angles) 2.362
Ramachandran favored (%) 100.00
Ramachandran allowed (%) 0.00
Ramachandran outliers (%) 0.00
Rotamer outliers (%) 0.00
Clashscore 3.90
Average B factor 23.51
Macromolecules 20.76
Solvent 41.56

References

First citationNanao, M., Basu, S., Zander, U., Giraud, T., Surr, J., Guijarro, M., Lentini, M., Felisaz, F., Sinoir, J., Morawe, C., Vivo, A., Beteva, A., Oscarsson, M., Caserotto, H., Dobias, F., Flot, D., Nurizzo, D., Gigmes, J., Foos, N., Siebrecht, R., Roth, T., Theveneau, P., Svensson, O., Papp, G., Lavault, B., Cipriani, F., Barrett, R., Clavel, C. & Leonard, G. (2022). J. Synchrotron Rad. 29, 581–590.  Web of Science CrossRef CAS IUCr Journals Google Scholar

This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
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