[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o771
[ doi:10.1107/S1600536813010349 ]

9H-Carbazole-9-carbothioic dithioperoxyanhydride

N. Uludag, M. Ates, N. Çaylak Delibas, Ö. Çelik and T. Hökelek


Key indicators

checkCIF/PLATON results

No syntax errors found



Alert level A PLAT029_ALERT_3_A _diffrn_measured_fraction_theta_full Low ....... 0.928
Author Response: Quality of the crystal was highly poor. The recrystallization studies made to get a better quality crystal were not succesful.

Alert level B PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 25 PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 19
Alert level C PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0066 Ang PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 9.337 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.006 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 7 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1 PLAT915_ALERT_3_C Low Friedel Pair Coverage ...................... 79 Perc.
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT128_ALERT_4_G Alternate Setting of Space-group P21212 ....... P22121 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 145 PLAT952_ALERT_5_G Reported and Calculated Lmax Values Differ by .. 2
1 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 9 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster