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Acta Cryst. (2014). E70, o97-o98  [ doi:10.1107/S1600536813034107 ]

10-(4-Chloro­phen­yl)-14a-hy­droxy-12-methyl-8,9,9a,10,12,13,14,14a-octa­hydro-5H-10a,14-methano­indeno­[2',1':4,5]azepino[3,4-b]pyrrolizine-5,15(7H,11H)-dione

R. A. Nagalakshmi, J. Suresh, K. Malathi, R. R. Kumar and P. L. N. Lakshman


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 3 PLAT918_ALERT_3_C Reflection(s) # with I(obs) much smaller I(calc) 1 Check
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 2 Why ? PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT431_ALERT_2_G Short Inter HL..A Contact Cl1 .. O2B .. 3.08 Ang. PLAT793_ALERT_4_G The Model has Chirality at C3A (Verify) R PLAT793_ALERT_4_G The Model has Chirality at C3B (Verify) S PLAT793_ALERT_4_G The Model has Chirality at C5A (Verify) S PLAT793_ALERT_4_G The Model has Chirality at C5B (Verify) R PLAT793_ALERT_4_G The Model has Chirality at C7A (Verify) R PLAT793_ALERT_4_G The Model has Chirality at C7B (Verify) S PLAT793_ALERT_4_G The Model has Chirality at C8A (Verify) S PLAT793_ALERT_4_G The Model has Chirality at C8B (Verify) R PLAT793_ALERT_4_G The Model has Chirality at C12A (Verify) S PLAT793_ALERT_4_G The Model has Chirality at C12B (Verify) R PLAT793_ALERT_4_G The Model has Chirality at C13A (Verify) S PLAT793_ALERT_4_G The Model has Chirality at C13B (Verify) R PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 30
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 18 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 13 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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