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Acta Cryst. (2014). E70, o43-o44  [ doi:10.1107/S1600536813033096 ]

5-Chloro-5''-(4-chloro­benzyl­idene)-4'-(4-chloro­phen­yl)-1''-ethyl-1'-methyl­dispiro­[indoline-3,2'-pyrrolidine-3',3''-piperidine]-2,4''-dione

I. S. A. Farag, A. S. Girgis, A. A. Ramadan, A. M. Moustafa and E. R. T. Tiekink


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Alert level B CRYSS02_ALERT_3_B The value of _exptl_crystal_size_max is > 1.0 Maximum crystal size given = 1.020
Author Response: The dimensions are confirmed and a large collimator was employed for the data collection. The refinement was smooth with no untoward errors.

Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.977 PLAT230_ALERT_2_C Hirshfeld Test Diff for C9 -- C10 .. 5.5 su PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... C23 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.633 Check PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 10 Why ? PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 41 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 9
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 1 Why ? PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 1.02 mm PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT793_ALERT_4_G The Model has Chirality at C1 (Verify) S PLAT793_ALERT_4_G The Model has Chirality at C6 (Verify) R PLAT793_ALERT_4_G The Model has Chirality at C8 (Verify) R PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 100
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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