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Acta Cryst. (2014). E70, o25-o26  [ doi:10.1107/S1600536813032789 ]

3-(Adamantan-1-yl)-4-ethyl-1-{[4-(2-meth­oxy­phen­yl)piperazin-1-yl]meth­yl}-1H-1,2,4-triazole-5(4H)-thione

A. A. El-Emam, H. M. Al-Tuwaijri, E. S. Al-Abdullah, C. S. Chidan Kumar and H.-K. Fun


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Alert level C THETM01_ALERT_3_C The value of sine(theta_max)/wavelength is less than 0.590 Calculated sin(theta_max)/wavelength = 0.5878 PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.966 PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd. # 1 C26 H37 N5 O S PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.139 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.588 143
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.98 mm PLAT793_ALERT_4_G The Model has Chirality at C24 (Verify) R PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 82 % PLAT960_ALERT_3_G Number of Intensities with I < - 2*sig(I) ... 3
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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