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Acta Cryst. (2014). E70, i4  [ doi:10.1107/S1600536813033680 ]

Nickel(II) uranium(IV) tris­ulfide

M. D. Ward and J. A. Ibers


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Alert level B Crystal system given = orthorhombic PLAT971_ALERT_2_B Large Calcd. Non-Metal Positive Residual Density 2.90 eA-3
Alert level C PLAT019_ALERT_1_C Check _diffrn_measured_fraction_theta_full/_max 0.996 PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.43 PLAT922_ALERT_1_C wR2 in the CIF and FCF Differ by ............... 0.0041 Check PLAT923_ALERT_1_C S values in the CIF and FCF Differ by ....... -0.196 Check PLAT927_ALERT_1_C Reported and Calculated wR2 Differ by ......... 0.0040 Check PLAT928_ALERT_1_C Reported and Calculated S value Differ by . -0.196
Alert level G PLAT004_ALERT_5_G Polymeric Structure Found with Dimension ....... 3 Info PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT793_ALERT_4_G The Model has Chirality at S2 (Verify) R
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 3 ALERT level G = General information/check it is not something unexpected 5 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 0 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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