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Acta Cryst. (2014). E70, m21-m22  [ doi:10.1107/S1600536813033357 ]

Bis([mu]2-benzoato-[kappa]2O:O')bis­[(benzoato-[kappa]2O,O')bis(4,4'-bi­pyridine-[kappa]N)cobalt(II)]-benzoic acid (1/6)

R. Peña-Rodríguez, J. M. Rivera, R. Colorado-Peralta, A. M. Duarte-Hernández and A. Flores-Parra


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Alert level C PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low .... 46 % PLAT230_ALERT_2_C Hirshfeld Test Diff for O2 -- C21 .. 5.3 su PLAT234_ALERT_4_C Large Hirshfeld Difference C19 -- C20 .. 0.17 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C42 -- C43 .. 0.16 Ang. PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... O3 Check PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... C15 Check PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... C26 Check PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... N1 Check PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... C11 Check PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... C12 Check PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C43 Check PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C36 Check PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.1 Note PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C43 -C48 1.37 Ang. PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C36 -C41 1.36 Ang. PLAT341_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0073 Ang. PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 41 Ang3 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 10.945 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.603 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 43 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 7
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 3 Why ? PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00300 Deg. PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Co1 -- O2 .. 6.4 su PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 4 Why ? PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 80
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 21 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 12 ALERT type 2 Indicator that the structure model may be wrong or deficient 7 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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