issue contents

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767

October 2026 issue

Early view articles

Journal cover

research papers


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This article presents the design, installation and first experimental testing of a novel prototype target–moderator–reflector assembly for a compact accelerator-driven neutron source driven by a 35 MeV electron beam.

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EQSANS-CLI is a command-line tool for small-angle neutron scattering data reduction. It exposes the full reduction pipeline through two input surfaces, an interactive terminal that accepts both slash commands and natural language, and a headless JSON mode designed for external AI agents, both built on a shared command-handler layer.

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We present an improved numerical angle-dependent absorption correction procedure for line-collimated small- and wide-angle X-ray scattering measurements in thin-walled quartz capillaries. The procedure accounts for the constrained illuminated volume, measured primary beam profiles and capillary-wall absorption, enabling physically consistent data reduction and reliable absolute scaling when conventional experimental scalar transmission corrections become unreliable.

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Findings are presented on the impact of particle size and solidification history on defect formation in Al2024 alloy additive manufacturing powder. The results of this investigation suggest a trend of decreasing dislocation density in as-atomized samples as the particle size increases, with larger particles cooling more slowly.

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We derive a generalized Parratt method applicable to anisotropic systems, which is devoid of the numerical instabilities arising in the method of characteristic matrices. We derive formulae for both reflectivity and transmissivity.

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Modifications of the fundamental equation of X-ray stress analysis are proposed that allow correction of the hoop and longitudinal stresses obtained from sin2ψ measurements on samples featuring an inhomogeneous surface topography. The formalism is verified by angle- and energy-dispersive measurements performed on a ferritic steel sample with cylindrically shaped regions with different central angles.

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We performed grazing-incidence total X-ray scattering on an indium tin oxide thin film using a convergent incident beam. This approach enables the acquisition of total scattering profiles up to Q = 21 Å−1, demonstrating the feasibility of laboratory instruments for thin film pair distribution function analysis.

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An analytical absorption correction for powder X-ray diffraction of flat plate samples in transmission geometry is presented. Independent determination of the optical thickness enables reliable refinement of atomic displacement parameters.

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A general solution of the problem of observing isoscattering points in the form factors of quasi-spherical particles under contrast variation in a small-angle scattering experiment is presented. It uses the approach of basic functions extended to the practical area by considering experimental isopoints as caustic-type nodes.

computer programs


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DISCO is a program capable of calculating the X-ray contrast factor for single- and polycrystalline materials in real time.

laboratory notes


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We present a versatile state-of-the-art X-ray scattering laboratory within the ITACA.SB Research Infrastructure, enabling multi-scale structural characterization of complex biological specimens and advanced materials through integrated small- and wide-angle X-ray scattering (SAXS/WAXS) techniques. The platform supports simultaneous SAXS/WAXS acquisition, scanning microscopy, ultra-SAXS and size-exclusion chromatography SAXS measurements.

addenda and errata