Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 61| Part 2

ISSN: 2056-9890

February 2005 issue

Highlighted illustration

Cover illustration: Sildenafil citrate is better known as the anti-impotence drug Viagra. The crystal structure has not been reported previously, but a monohydrate has now been characterized crystallographically. See Yathirajan, Nagaraj, Nagaraja & Bolte [Acta Cryst. (2005), E61, o489-o491].

inorganic compounds

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Reinvestigation of Hg₂GeSe₄ based on single-crystal data

Y. Dong, S. Kim and H. Yun

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CeRu₂Al₁₀ with the YbFe₂Al₁₀ structure type

A. I. Tursina, S. N. Nesterenko, E. V. Murashova, I. V. Chernyshev, H. Noël and Y. D. Seropegin

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CsYbSe₂

B. Deng and J. A. Ibers

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Tetratellurium bis[heptachlorodigallate(III)], Te₄[Ga₂Cl₇]₂

M. Lindsjö and L. Kloo

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metal-organic compounds

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Methyl 2-[(ferrocenylcarbonyl)amino]thiophene-3-carboxylate

S. Alley, J. F. Gallagher, P. T. M. Kenny and A. J. Lough

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Tetraaquadithiocyanatonickel(II) tetrakis(2-amino-4,6-dimethylpyrimidine) dihydrate

M. Hemamalini, P. T. Muthiah and R. J. Butcher

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[1-(3-Aminopropyl)-4,7-dithia-1-azacyclononane-κ⁴N,N′,S,S′]bis(dimethylformamide-κO)nickel(II) bis(tetraphenylborate) acetonitrile disolvate

A. J. Blake and V. Lippolis

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Aqua{2-[(E)-3,5-dibromo-2-oxidobenzylideneamino]ethanesulfonato}(1,10-phenanthroline)zinc(II) ethanol solvate

S.-H. Zhang, Y.-M. Jiang and K.-B. Yu

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(2,2′-Bipyridine N,N′-dioxide-κ²O,O′)dibromomercury(II)

O. M. Tedmann, P. Y. Zavalij, S. K. Madan and S. R. J. Oliver

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(2,2′-Bipyridine N,N′-dioxide-κ²O,O′)diiodomercury(II)

O. M. Tedmann, P. Y. Zavalij, S. K. Madan and S. R. J. Oliver

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Azidobis(2,2′-bipyridine)cadmium(II)

F.-F. Jian, C.-L. Li, H.-L. Xiao and P.-P. Sun

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Poly[disilver(I)(Ag—Ag)-μ-4-chlorobenzoato-μ-piperazine]

S. Yang, Y. Zou and H.- Zhu

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A dimeric alkyl complex supported by an O,S,S,O-tetradentate diphenolate ligand

H. Ma, G. Melillo, L. Oliva, T. P. Spaniol and J. Okuda

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Tetrakis(μ-N-acetyl-N-phenylglycinato-κ²O,O′)bis[(N-acetyl-N-phenylglycinato-κ³O,O,O)(1,10-phenanthroline-κ²N,N′)cerium(III)] dihydrate

A.-Y. Fu, S.-Z. Fu and T. Yu

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{N-[Bis(2-pyridyl)methyl]-N,N-bis(2-pyridylmethyl)amine-κ⁵N}chlororuthenium(II) perchlorate methanol solvate

T. Kojima, D. M. Weber and C. T. Choma

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Bis(di-2-pyridylmethanediol-κ³N,O,N′)nickel(II) dilactate

C.-J. Li, W. Li, M.-L. Tong and S. W. Ng

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A C-centered monoclinic modification of bis(di-2-pyridylmethanediol-κ³N,O,N′)copper(II) diacetate tetrahydrate

C.-J. Li, W. Li, M.-L. Tong and S. W. Ng

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Diaquabis(5-nitro-1H-benzimidazole-κN³)copper(II) dinitrate

C.-F. Ding, S.-S. Zhang, B.-Q. Tian, X.-M. Li, H. Xu and P.-K. Ouyang

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A dinuclear copper complex with a p-aminobenzoate anion

J. Yang, L. Li, J.-F. Ma and Y.-Y. Liu

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(2-Phenylethyl)ammonium tetrabromothallate(III)

M. Abdi, F. Zouari, N. Chniba-Boudjada, P. Bordet and A. B. Salah

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(Tetrahydroborato)bis(triphenylphosphine)copper(I): a redetermination at 90 K

J. Moncol, M. Gembicky and P. Coppens

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Bis(1H-benzimidazole-κN³)bis(4-hydroxybenzoato-κ²O,O′)copper(II)

J.-R. Su, J.-M. Gu and D.-J. Xu

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Nitrato[1-(2-pyridylmethyliminomethyl)naphthalen-2-olato]zinc(II)

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Bis[4-bromo-2-(cyclohexyliminomethyl)phenolato]copper(II)

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catena-Poly[[bis(μ₄-hexafluoroglutarato)bis(tetrahydrofuran)tetrasilver(I)]-μ₂-4,4′-biphenyldicarbonitrile]

S.-Q. Liu, H. Konaka, T. Kuroda-Sowa and M. Munakata

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catena-Poly[[[(4′-phenyl-2,2′:6′,2′′-terpyridine-κ³N,N′,N′′)zinc(II)]-μ-terephthalato-κ²O:O′] monohydrate]

Q.-D. Tu, Y.-G. Yin, J. He, J. Xiang, D. Li and S. W. Ng

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catena-Poly[[[(1,10-phenanthroline)nickel(II)]-μ-4,4′-oxydibenzoato] 0.25-hydrate]

H.-P. Xiao, J.-G. Wang, X.-H. Li, M.-L. Hu and W.-B. Zhang

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catena-Poly[[[bis(1H-imidazole-κN³)zinc(II)]-μ-terephthalato-κ²O:O′] trihydrate]

D.-D. Lin, K.-L. Yin and D.-J. Xu

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catena-Poly[[tetraaquacadmium(II)-μ-hexane-1,6-diamine-κ²N:N′] terephthalate dihydrate]

X.-G. Meng and Z.-D. Lin

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Bis[μ-3,5-bis(2-pyridyl)-4-(4-isopropylphenyl)-4H-1,2,4-triazole]disilver(I) diperchlorate acetonitrile solvate

S.-C. Shao, Z.-L. You, S.-P. Zhang, H.-L. Zhu and S. W. Ng

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Tetraaquatetrakis(dimethylacetamide-κO)neodymium(III) hexacyanoferrate(III) trihydrate

J. Overgaard, H. Svendsen, M. A. Chevalier and B. B. Iversen

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Aqua(bromomaleato-κO)bis(phenanthroline-κ²N,N′)manganese(II) monohydrate

D.-X. Li, D.-J. Xu and Y.-Z. Xu

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[μ-2,8-Dimethyl-5,11-bis(dimethylaminoethyl)-1,4,5,6,7,10,11,12-octahydrodiimidazo[4,5-h;4,5-c][1,6]diazecine]bis[aquacopper(II)] diacetate hexahydrate

L. Gasque, J. Olguín and S. Bernès

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Hexaaquamagnesium(II) benzene-1,4-dioxyacetate

Q. Yang, S. Gao and L.-H. Huo

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Poly[[triaquabis(μ₄-3-carboxy-4-hydroxybenzenesulfonato)disilver(I)] monohydrate]

S. Gao, Z.-B. Zhu, L.-H. Huo and S. W. Ng

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Poly[di-μ-aqua-bis(μ₈-3-carboxylato-4-hydroxybenzenesulfonato)tetrasilver(I)]

S. Gao, Z.-B. Zhu, L.-H. Huo and S. W. Ng

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Dipyridinium diaquatetrachlorotin(IV) 1,5-naphthalenedisulfonate

S. Gao, L.-H. Huo, H. Zhao and S. W. Ng

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Poly[bis[aquamercury(I)]-di-μ-aqua-μ-1,5-naphthalenedisulfonato]

Z.-B. Zhu, S. Gao, L.-H. Huo and S. W. Ng

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Bis(2,2′-bipyridine)(3-carboxy-4-hydroxybenzenesulfonato)copper(II) 3-carboxy-4-hydroxybenzenesulfonate

S. Gao, L.-H. Huo, H. Zhao and S. W. Ng

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(18-Crown-6)potassium chlorochromate

S. A. Kotlyar, R. I. Zubatyuk, O. V. Shishkin, G. N. Chuprin, A. V. Kiriyak and G. L. Kamalov

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1,1,3,3-Tetraphenyl-1,2,3-triphosphenium tetrachloroaluminate dichloromethane solvate

R. M. K. Deng, K. B. Dillon, A. E. Goeta and A. L. Thompson

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catena-Poly[bis[aqua(1,10-phenanthroline)zinc(II)]-μ₄-benzene-1,2,4,5-tetracarboxylato]

X.-L. Wang, F.-C. Liu, J.-R. Li and S. W. Ng

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(η⁶-N,N-Diethylaniline)(η⁴-1,2,3,4-tetramethylcyclobutadiene)cobalt(I) hexafluorophosphate

A. R. Kennedy and P. L. Pauson

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Bis(p-toluidinium) tetrachlorozincate(II)

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1′-(1-Hydroxyethyl)-N,N-diphenylferrocene-1-carboxamide

M. Cetina, S. Đaković, A. Hergold-Brundić and V. Rapić

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catena-Poly[[[bis(μ-4-cyanobenzoato-κ²O:O)bis[(4-cyanobenzoato-κ²O,O′)cobalt(II)]]-di-μ-4,4′-bipyridine-κ⁴N:N′] dihydrate dimethylformamide tetrasolvate]

H.-Y. He, L.-G. Zhu and S. W. Ng

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Poly[di-μ₄-acetato-di-μ₂-azido-copper(II)disodium(I)] at 150 K

C. Näther, J. Greve and I. Jeß

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Poly[tetra-μ₂-azido-di-μ₂-4,4′-bipyridine-sodium(I)iron(III)]

C. Näther, J. Greve and I. Jeß

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Lithium hydrogen (RS)-phenylsuccinate

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Bis(5-bromo-N-cyclohexylsalicylideneaminato-κ²N,O)nickel(II)

Y.-X. Sun and S. W. Ng

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(Benzoylacetone 4-methoxybenzoylhydrazonato-κ³O,N,O′)(N-benzoylhydroxylaminato-κ²O,O′)oxovanadium(IV)

S. Gao, L.-H. Huo, H. Zhao and S. W. Ng

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Hexaaquazinc(II) bis(perchlorate) bis(2,5-dimethylpyrazine 1,4-dioxide)

J. J. Lu and J. M. Shi

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Poly[[(2-iodopyrazine-κN⁴)copper(I)]-μ₃-thiocyanato-κ³N:S:S]

C. Näther, M. Wriedt and I. Jeß

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Aqua[bis(5-bromosalicylidene)ethylenediaminato]chloromanganese(III)

L.-L. Dang, Y.-Q. Huo, W. Wang and J. Li

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Bis[4-bromo-2-(pyridin-2-ylmethyliminomethyl)phenolato-κ³N,N′,O]cobalt(III) nitrate

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[4-Bromo-2-(pyridin-2-ylmethyliminomethyl)phenolato](methanol)copper(II) perchlorate

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cis-(2,2′-Bipyridyl-κ²N,N′)carbonyl(η³-1-methylene-2,2′:6′,2′′-terpyridyl-κ³C¹,N,N′)ruthenium(II) bis(hexafluorophosphate) acetone disolvate

D. H. Gibson, M. S. Mashuta and J. G. Andino

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catena-Poly[bis[aqua(1,10-phenanthroline-κ²N,N′)cobalt(II)]-di-μ-4,4′-oxydibenzoato-1:2κ⁴O:O′]

H.-P. Xiao, X.-H. Li and S. W. Ng

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A redetermination of [N,N-bis(3,5-dimethyl-1H-pyrazol-1-ylmethyl-κN²)-2-hydroxyethylamine-κN](3,5-dimethyl-1H-pyrazole-κN²)nitratocopper(II) nitrate

A. Ramdani, M. El Kodadi, M. Fouad, D. Eddike, M. Tillard and C. Belin

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Tris(1,10-phenanthroline-κN,N′)manganese(II) bis(perchlorate) chloroform disolvate

G.-H. Cui and J.-R. Li

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A redetermination of lithium chloride dioxane

J. J. Morris, B. C. Noll and K. W. Henderson

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Retracted: Bis(4-bromo-2-formylphenolato-κ²O,O′)copper(II)

Y.-X. Sun and G.-Z. Gao

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μ-Terephthalato-bis[bis(2,2′-bipyridine)copper(II)] bis(perchlorate) dihydrate

S.-Z. Yang and X.-H. Li

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β-Methyl-γ,γ-bis(8-quinolinoxy)germa-γ-lactone

S. Mahboob, M. Parvez, M. Mazhar and S. Ali

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Hexaaquamanganese(II) 5,5′-(1,4-phenylene)ditetrazolate

Z.-J. Ma, J. Tao, R.-B. Huang and L.-S. Zheng

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Bis(2-oxopyridinato N-oxide-κ²O,O′)copper(II)

L. Xu, Y.-Z. Li, S.-H. Liu, X.-T. Chen and J.-H. Zhou

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3,3′-(p-Phenylenedimethylene)bis(1-methylimidazolium)–tetrachloroargentate(I) (3/2)

J.-W. Wang, F.-B. Xu, Q.-S. Li, H.-B. Song and Z.-Z. Zhang

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Aqua[4-bromo-2-(pyridin-2-ylmethyliminomethyl)phenolato]copper(II) nitrate monohydrate

Y.-X. Sun, G.-Z. Gao, H.-X. Pei and R. Zhang

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Dichloro[N,N-dimethyl-N'-(pyridin-2-ylmethylidene)ethane-1,2-diamine]zinc(II)

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Methylchlorosila[1]ferrocenophane

W. Y. Chan, A. J. Lough and I. Manners

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Aquabis(2,2′-bipyridine)(3-carboxylato-4-hydroxybenzenesulfonato)manganese(II) dihydrate

S.-R. Fan, L.-G. Zhu, H.-P. Xiao and S. W. Ng

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Bis(4-hydroxybenzoato-κ²O,O′)(1,10-phenanthroline-κ²N,N′)copper(II)

J.-R. Su, J.-M. Gu and D.-J. Xu

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Diaquabis(μ-4-hydroxybenzenecarboxylato-κ²O,O′)disilver(I)(Ag—Ag) tetrahydrate

Y. Wang and N. Okabe

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[N,N′-Ethylenebis(salicylideneiminato)]nickel(II) chloroform solvate

X.-L. Cheng, S. Gao, L.-H. Huo and S. W. Ng

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Bis[di-2-pyridyl(hydroxy)methanolato-κ³O,N,N′]iron(III) tetrafluoroborate trihydrate

D. Onggo, A. Mimin, B. M. Yamin and S. W. Ng

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Tetrakis(μ₂-4-tolylthioacetato-κ²O:O′)bis[(pyridine-κN)copper(II)]

S. Gao, L.-H. Huo, H. Shu and S. W. Ng

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Aquabis(3,5-dicarboxybenzoato-κO)bis(hexamethylenetetramine-κN)nickel(II)

S. Gao, L.-H. Huo, H. Zhao and S. W. Ng

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An X-ray powder diffraction study of catena-poly[[bis(1-methyl-1H-tetrazole-κN⁴)copper(II)]-di-μ-bromo]

L. S. Ivashkevich, A. S. Lyakhov, M. M. Degtyarik and P. N. Gaponik

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Azido[1-(isobutylaminomethyliminomethyl)-2-naphtholato]nickel(II)

Y.-X. Sun, G.-Z. Gao, R. Zhang and H.-X. Pei

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Chloro(2,3,7,8,12,13,17,18-octaethylporphyrinato)iron(III)

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Ethylenediammonium diaquabis(ethylenediamine-κ²N,N′)zinc(II) bis(pyridine-2,6-dicarboxylato-κ³,O,N,O′)zincate(II) dihydrate

A.-Y. Fu, D.-Q. Wang and D.-Z. Sun

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Bis[μ-4′-(2-pyridyl)-2,2′:6′,2′′-terpyridine]disilver(I) bis(hexafluorophosphate)

L. Hou, D. Li and S. W. Ng

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Twinned poly[[diaquacalcium(II)]-μ₄-benzene-1,3-dioxyacetato]

S. Gao, L.-H. Huo, J.-W. Liu and S. W. Ng

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trans-Bis[(2E)-3-(N,N-dimethylamino)-1-(2-pyridyl)prop-2-en-1-one]diisothiocyanatonickel(II)

G.-X. Li, J.-Q. Li and X.-Z. Kang

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organic compounds

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N-Chloromethyl-4-(dimethylamino)-N,N-dimethylanilinium chloride

A. S. Batsanov, J. C. Collings and T. B. Marder

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DL-Phenylalaninium trichloroacetate

K. Rajagopal, R. V. Krishnakumar and S. Natarajan

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1,4-Bis(1-phenyl-1H-tetrazol-5-ylsulfanyl)butane

W. Wang, H.-M. Liu and W.-Q. Zhang

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2-(Benzotriazol-1-yl)-2-(α-hydroxybenzyl)-N-phenylthioacrylamide

F.-Q. Liu, W.-H. Li, L.-D. Lu, X.-J. Yang, X. Wang and B.-R. Hou

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Hydrogen bonding in creatininium nitrate

F. Berrah, H. Lamraoui and N. Benali-Cherif

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n-Octanol

H. A. Shallard-Brown, D. J. Watkin and A. R. Cowley

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2-Oxo-2-phenylethyl morpholine-4-carbodithioate

L.-Z. Xu, K. Li, G.-P. Yu, G.-D. Si and C.-L. Yu

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(8E)-8-Benzylidene-3,4,5,6,7,8-hexahydro-4-phenylquinazoline-2(1H)-thione

X.-L. Zhang and Z.-P. Liang

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(2Z)-2-(Anthracen-9-ylmethylene)-5,6-dihydroimidazo[2,1-b]thiazol-3(2H)-one

Z.-P. Liang and J. Li

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Melamine (1,3,5-triazine-2,4,6-triamine): a neutron diffraction study at 14 K

A. Cousson, B. Nicolaï and F. Fillaux

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3-(4-Chlorophenyl)-3-hydroxy-1-phenylpropan-1-one

Z.-F. Yu, X.-Y. Gu, B. Zhao and Z.-Z. Tian

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Brooker's di-tert-butylmerocyanine

N. Masciocchi, P. Scuderi and A. Maspero

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10,11-Dihydrocinchonan-9-ol

X.-X. Lei, X. Jing, A.-J. Zhang and S. W. Ng

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1-(4-Decylphenyl)pyridin-4(1H)-one

C. Li, J. R. Wolf, D. J. Dyer and P. D. Robinson

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2-[(E)-Benzylideneamino]-N-(2-fluorophenyl)-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide

Vasu, K. A. Nirmala, D. Chopra, S. Mohan and J. Saravanan

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2-Methylphenyl 4-toluenesulfonate: supramolecular aggregation through weak C—H⋯O, C—H⋯π and π–π interactions

V. Manivannan, N. Vembu, M. Nallu, K. Sivakumar and F. R. Fronczek

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4-Methylphenyl 4-toluenesulfonate: supramolecular aggregation through weak C—H⋯O and C—H⋯π interactions

V. Manivannan, N. Vembu, M. Nallu, K. Sivakumar and F. R. Fronczek

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3-(p-Nitrobenzyl)-1,3-thiazolidine-2,4-dione

H. S. Yathirajan, K. M. L. Rai, S. L. Gaonkar, R. S. Narasegowda, B. Prabhuswamy and M. Bolte

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1-(4-Methoxyphenyl)-2-(6-methyl-2-nitro-3-pyridyloxy)propan-1-one

I. Vencato, P. H. Ferri, S. C. Santos, M. Pereira, C. Lariucci, L. I. B. Homar and H. B. Napolitano

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2,2′:5,6-Di-O-isopropylidene-2-C-hydroxymethyl-D-talono-1,4-lactone

C. C. Harding, D. J. Watkin, A. R. Cowley, R. Soengas, U. P. Skytte and G. W. J. Fleet

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A cation–anion complex: 1,10-phenanthrolin-1-ium 5-sulfonatosalicylic acid

S.-R. Fan, H.-P. Xiao and L.-G. Zhu

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4-Benzoyl-1,5-diphenyl-1H-pyrazole-3-carboxylic acid methanol solvate

I. Yıldırım, N. Özdemir, Y. Akçamur, M. Dinçer and O. Andaç

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2-(1H-Benzotriazol-1-yl)-3-(4-chlorophenyl)-3-hydroxy-N-phenylprop-2-enethioamide

L.-Z. Xu, S.-H. Yang, C.-Y. Zhu, K. Li and F.-Q. Liu

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(3S,8S)-3,8-Dimethyl-1,6-dioxa-4,9-diaza-5λ⁵-phosphaspiro[4.4]nonane-2,7-dione

L. Yu, Z. Liu, H. Fang and Y.-F. Zhao

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(±)-(1SR,8RS,10RS)-9,9,10-Tribromotricyclo[6.2.1.0^2,7]undeca-2,4,6-triene

C. C. Ersanlı, U. Çoruh, T. Hökelek, E. M. Vázquez-López and A. Daştan

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4-[(4-Hydroxybenzylidene)amino]-1,5-dimethyl-2-phenyl-2,3-dihydro-1H-pyrazol-3-one methanol solvate

X.-L. Zhang and Z.-X. Li

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(1R,2R)-Ethyl 1-azido-2-hydroxy-2,3-dihydro-1H-pyrrolo[1,2-a]indole-9-carboxylate

M. A. Fernandes, C. B. de Koning, J. P. Michael and R. L. Petersen

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Tetra-n-butylammonium hexafluorophosphate at 110 K

Z. Stein and I. Goldberg

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Ethyl 3-hydroxy-2-naphthoate

C.-Z. Jin and L.-F. Jin

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3,4-(Methylenedioxy)benzaldehyde benzoylhydrazone ethanol solvate

A.-X. Li and L.-L. Liu

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(Z)-Ethyl 3-phenyl-2-[(triphenylphosphoranylidene)amino]prop-2-enoate

X.-B. Huang, M.-C. Liu, H.-Y. Wu, J.-C. Ding and M.-L. Hu

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1-(2,6-Dihydroxyphenyl)butanone

H.-R. Huang, X.-L. Feng, Z.-G. She, Y.-C. Lin, L. L. P. Vrijmoed and E. B. G. Jones

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4,4'-(2-Methyl-1H-imidazole-4,5-diyl)bis[2(S)-methyl-3-azoniabutanoate] acetic acid monohydrate

L. Gasque, E. Mijangos and S. Bernès

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Melaminium benzoate dihydrate

G. J. Perpétuo and J. Janczak

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(–)-(3a′S,4′S,9b′S,1R,2S,5R)-4′-Ethyl-3a′,4′,5′,7′,8′,9b′-hexahydro-2-isopropyl-5-methyl-2′-phenylspiro[cyclohexane-1,7′-dioxino[3,2-e]isoindole]-1′,3′,9′-trione

D. Schollmeyer, R. Hoffmann and J. Mattay

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1-tert-Butyl-3-(α-hydroxy-4-isopropylbenzylidene)pyrrolidine-2,4-dione

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4-(Benzoylthiocarbonyl)morpholine

W.-W. Liu, Y.-Z. Li, L.-D. Kong and H.-W. Hu

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Ethyl 2-methoxycarbonylamino-3-phenylpropionate

B. Tan, H. Fang, Z.-B. Wei and L.-R. Jin

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3-Ethyl-1-[2-(1-ethylmorpholinium-1-yl)ethyl]benzimidazolium diiodide monohydrate

M. Akkurt, S. O. Yıldırım, H. Küçükbay, U. Yılmaz and O. Büyükgüngör

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2-Acetamido-N-(2-chlorophenyl)-4,5,6,7-tetrahydrobenzothiophene-3-carboxamide

K. Chandra Kumar, M. K. Kokila, Puttaraja, S. Mohan, K. S. Manjunath Shetty and M. V. Kulkarni

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1-(4-Methoxyphenyl)-3-(1H-1,2,4-triazol-1-yl)propan-1-one

J. Wan, C.-L. Li, X.-M. Li and S.-S. Zhang

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Candesartan cilexetil, an antihypertensive agent containing an extended double ester chain

D. Fernández, D. Vega and J. A. Ellena

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The 1:1 proton-transfer compound of 5-sulfosalicylic acid with 4-aminobenzoic acid

G. Smith, U. D. Wermuth and J. M. White

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2,2′-Bipyridinium 5-nitroisophthalate 5-nitroisophthalic acid dihydrate

D.-M. Chen, X.-H. Li, H.-P. Xiao and M.-L. Hu

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[(1-Methylcytosine)₂H]I, an asymmetric base pair

J. Müller and E. Freisinger

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N-(2-Nitrophenylsulfonyl)glycine methyl ester

L. F. Bornaghi, S.-A. Poulsen, P. C. Healy and A. R. White

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2C-Methyl-D-arabinono-1,4-lactone monohydrate

F. Punzo, D. J. Watkin, S. F. Jenkinson and G. W. J. Fleet

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2-Hydroxy-1-phenylethanone

P. Zhao, Q. Shao, W. Zhou, J. Li, M. Lu and C. Li

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1,4,7-Triazacyclononane hemihydrate

A. R. Battle, D. L. Johnson and L. L. Martin

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4-Aminopyridinium isonicotinate monohydrate

A. R. Kennedy and M. Kittner

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4-(2,6-Dimethylphenoxy)phthalonitrile

O. Büyükgüngör, B. Koşar, N. Akdemir, E. Ağar and I. Gümrükçüoğlu

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Hydrogen-bonded networks in 1H-indazoles: the case of 7-methyl-1H-indazole

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4-Chlorophenyl thiobenzoate

T. B. Ganesh, A. Dhakshinamoorthy, K. Pitchumani, S. Athimoolam, B. Sridhar and R. K. Rajaram

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5-Amino-3H-isobenzofuran-1-one (5-aminophthalide)

H. S. Yathirajan, B. Nagaraj, S. L. Gaonkar, R. S. Narasegowda, B. Prabhuswamy and M. Bolte

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5-Bromo-3H-isobenzofuran-1-one (5-bromophthalide)

H. S. Yathirajan, B. Nagaraj, S. L. Gaonkar, R. S. Narasegowda, P. Nagaraja and M. Bolte

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N,N′-Diphenyl-2,2′-(1,3,4-thiadiazolyl-2,5-dithio)diacetamide

Y.-H. Wen, S.-S. Zhang, B.-H. Yu, X.-M. Li and Q. Liu

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(4S)-4-(Methoxycarbonylmethylaminocarbonyl)-4-(3,4,5-trimethoxybenzamido)butanoic acid

X. Li, W.-F. Xu, J.-F. Wu, J.-L. Wang and Y.-M. Yuan

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2′-(2-Thienylmethylidene)-2-hydroxybenzohydrazide

F.-Y. Pan and J.-G. Yang

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N′-(2-Chlorobenzylidene)-2-hydroxybenzohydrazide

F.-Y. Pan and J.-G. Yang

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N—H⁺⋯Cl⁻ and C—H⋯O interactions in 6-fluoro-3-(4-piperidinio)benz[d]isoxazole chloride

H. S. Yathirajan, T. Narasimhamurthy, B. Nagaraj, P. Nagaraja, R. S. Narasegowda and R. S. Rathore

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2,6-Bis(4-methoxyphenyl)-1-nitroso-3,5-diphenylpiperidin-4-one

S. Natarajan, R. V. Krishnakumar, M. Subha Nandhini, V. P. Alex Raja, S. Perumal and K. Ravikumar

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4-Bromophenylboronic acid ethanol 0.04-solvate

N. S. P. Bhuvanesh and J. H. Reibenspies

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5-Acetyl-4,6-dimethyl-1,2,3,4-tetrahydropyrimidin-2-one

V. E. Zavodnik, A. D. Shutalev, G. V. Gurskaya, A. I. Stash and V. G. Tsirelson

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2,6-Bis[2,4-bis(heptyloxy)phenyl]pyridine

N. W. Alcock and J. P. Rourke

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2-Cyano-3-(4-hydroxyphenyl)propenoic acid

H.-F. Qian, W. Huang and C. Yao

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Ethyl 2-acetyl-3-[2-(1H-indol-3-yl)ethylamino]propenoate

N.-J. Fan, D.-H. Li, X.-M. Jiang, Y.-B. Zhang, W. Guo and C.-Z. Xia

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1,5-Dimethyl-2-phenyl-4-[(E,E)-3-phenylprop-2-enylideneamino]-1H-pyrazol-3(2H)-one

Z.-X. Li and X.-L. Zhang

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2-Methyl-6-(1,7,7-trimethylbicyclo[2.2.1]hept-2-yl)phenol

O. Y. Borbulevych

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Bharangin triacetate

K. Ravikumar, B. Sridhar and M. M. Murthy

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2-Cyano-3-(4-hydroxyphenyl)acrylic acid

M. Karas, I. Fournier and M. Bolte

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N,N-Bis(anthracen-9-ylmethyl)propylamine

Q.-X. Liu, H.-B. Song and Z.-M. Li

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7-Amino-1H-3,1-benzothiazine-2,4-dithione

Y. Yu, H.-P. Zhong, K.-B. Yang, R.-B. Huang and L.-S. Zheng

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2-Acetyl-3′-chloroacetanilide

X.-S. Tai, W.-Y. Liu, Y.-Z. Liu and Y.-Z. Li

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4,5,9,14-Tetramethyl-19-norcholest-24-en-3-one

K.-Y. Liu, W.-Y. Gao, T.-J. Zhang, H.-X. Chen and B. Zhou

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4-Phenyl-3-[(1H-1,2,4-triazol-1-yl)methyl]-1H-1,2,4-triazole-5-thione

F.-F. Jian, Z.-S. Bai, K. Li and H.-L. Xiao

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N,N′-(o-Phenylene)dibenzenesulfonamide

J. C. Bryan, J. M. Rosenberg and K. Kavallieratos

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16α,17-Epoxypregn-4-ene-3,11,20-trione

Q. Nie, J. Wang, S. Wang and M. Zhang

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1-(4-Hydroxyphenyl)-3-(1H-1,2,4-triazol-1-yl)propan-1-one

F.-Q. Liu, W.-H. Li, H.-B. Song, L.-D. Lu, X.-J. Yang and X. Wang

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8-Hydroxyquinolinium–dibromosuccinate–dibromosuccinic acid (2/1/2)

D.-X. Li, D.-J. Xu and Y.-Z. Xu

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1-(4-Chlorophenyl)-3-(4-hydroxyphenyl)prop-2-en-1-one

T. Ravishankar, K. Chinnakali, S. Nanjundan, P. Selvam, H.-K. Fun and X.-L. Yu

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Dimethyl [phenyl(pyridine-4-carboxamido)methyl]phosphonate

H. Fang, M.-J. Fang, X.-X. Liu, J.-J. Lin and Y.-F. Zhao

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3-(3,7-Dimethylocta-2,6-dienyloxy)-1,8-dihydroxy-6-methyl-9,10-anthraquinone

N. Boonnak, S. Chantrapromma, H.-K. Fun, S. Anjum, S. Ali, Atta-ur-Rahman and C. Karalai

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N-(Dicyclopropylmethylamino)-4,5-dihydro-1,3-oxazolium dihydrogenphosphate

H.-J. Hu, C.-R. Sun, H. Zhang and Y.-J. Pan

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(±)-(3aRS,4SR)-9-Chloro-2-(2-chloro-4-nitrophenyl)-4-(4-chlorophenyl)-3a,4-diethoxy-6,8-dimethoxychromano[4,3-d]-Δ^1,9^b-1,2,3-thiadiazoline

Y.-Z. Hu and H.-Z. Ying

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2,3,5,6-Tetramethylpyrazinium–trichloroacetate–trichloroacetic acid (1/1/1)

D.-M. Chen, F.-Y. Xia, M.-L. Hu, L. Li and Z.-M. Jin

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4-Methyl-2-thioxo-2,3-dihydrothiazol-3-yl 4-methylphenyl carbonate

J. Hartung, N. Schneiders and U. Bergsträsser

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2-(3-Methoxysalicylideneamino)-1H-benzimidazole monohydrate

Ç. Albayrak, M. Odabąsogˇlu and O. Büyükgüngör

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2-(3-Methoxysalicylideneamino)-1H-benzimidazole

M. Odabąsogˇlu, C. Albayrak and O. Büyükgüngör

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12,13-Dihydro-12-oxo-13-phenylbenzo[b]naphth[f][1,4]oxazepine-2,3-dicarbonitrile

Ş. Işik, M. Yavuz, N. Akdemir, E. Ağar and M. Özil

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4,5-Methylenedithio-1,3-dithiol-2-one

G. Xue, W. Yu and Q. Fang

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1,10-Phenanthrolin-1-ium 2-carboxy-4-nitrobenzoate

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N,N′-Di-3-pyridylperylene-3,4:9,10-bis(dicarboximide)

J. Mizuguchi, K. Hino, K. Sato, H. Takahashi and S. Suzuki

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N,N′-Di-2-pyridylperylene-3,4:9,10-bis(dicarboximide)

J. Mizuguchi, K. Hino, K. Sato, H. Takahashi and S. Suzuki

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N,N′-Di-4-pyridylperylene-3,4:9,10-bis(dicarboximide)

K. Hino, K. Sato, H. Takahashi, S. Suzuki and J. Mizuguchi

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Guanidinium 4-hydroxypyridinium-2,6-dicarboxylate

A. Moghimi, H. Aghabozorg, J. Soleimannejad and F. Ramezanipour

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(Z)-2,3-Bis(2-phenylindolizin-3-yl)-2-butenedinitrile

W.-W. Liu, Y.-Z. Li, R.-K. Sun, H.-W. Hu, Q.-J. Wu and Z.-X. Huang

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Diphenylphosphenium bromide

F. Dornhaus, H.-W. Lerner and M. Bolte

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Henicosane-1,21-dithiol

N. Nakamura, H. Shimizu and Y. Ogawa

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2-Phenylselanyl-3,5-methano-2H-cyclopenta[b]furan-2-one

T. Francis, D. A. R. Happer and W. T. Robinson

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3-{[(1Z)-(3-Methyl-5-oxo-1-phenyl-1,5-dihydropyrazol-4-ylidene)(phenyl)methyl]amino}propionic acid

H.-Z. Xu, X. Zhang and G.-S. Yu

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(Z)-1-Phenyl-2-(3-phenylthiazolidin-2-ylidene)ethanone

L.Z.- Xu, H.-Z. Xu, H.-B. Song, G.-D. Si, Y.-Q. Qin and K. Zhou

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A diastereoisomer of pyrano[3,2-c]quinoline

K. Ravikumar, B. Sridhar, M. Mahesh and V. V. N. Reddy

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trans-4-[(4-Dimethylaminophenyl)ethenyl]-N-methylquinolinium p-toluenesulfonate monohydrate

B. J. Coe, J. J. Hall, J. A. Harris, B. S. Brunschwig, S. J. Coles and M. B. Hursthouse

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Ethyl 4,6-dimethyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

V. E. Zavodnik, A. D. Shutalev, G. V. Gurskaya, A. I. Stash and V. G. Tsirelson

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p-Phenylene diacetate

J. Men, F. Gu and H. Sun

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2,5-Dimethoxybenzene-1,4-dicarbaldehyde

C. B. Nielsen, M. Pittelkow and H. O. Sørensen

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(1RS,2SR)-1,2,4,5,7-Pentabromo-5-methoxyindane

M. Akkurt, İ. Çelik, K. Berkil, A. Tutar, C. C. Ersanlı, O. Çakmak and O. Büyükgüngör

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Ethyl 1,3-dibromoazulene-6-carboxylate

Z. Hussain, T. Oeser and H. Hopf

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1-(4-Hydroxyphenyl)-3-(4-methoxyphenyl)prop-2-en-1-one

S. Sathiya Moorthi, K. Chinnakali, S. Nanjundan, R. Radhika, H.-K. Fun and X.-L. Yu

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1-(4-Bromophenyl)-3-(3-hydroxyphenyl)prop-2-en-1-one

S. S. Moorthi, K. Chinnakali, S. Nanjundan, C. S. Unnithan, H.-K. Fun and X.-L. Yu

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Benzyl 2-amino-6-chloro-9H-purine-9-carboxylate

K. F. Adebambo, N. M. Howarth and G. M. Rosair

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Sildenafil citrate monohydrate

H. S. Yathirajan, B. Nagaraj, P. Nagaraja and M. Bolte

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2-(5-Ethylpyridin-2-yl)ethanol

H. S. Yathirajan, S. L. Gaonkar and M. Bolte

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The natural naphthoquinone sterekunthal-B

K. Ravikumar, B. Sridhar, S. V. Reddy, U. S. Kumar and J. M. Rao

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(Z)-5-Benzylidene-3-phenethyl-2-thioxoimidazolidin-4-one

H.-Y. Wu, X.-B. Huang, J.-C. Ding, M.-C. Liu and M.-L. Hu

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3,6-Di-4-pyridylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

J. Mizuguchi, T. Imoda and H. Takahashi

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3-[N′-(4-Hydroxy-3-methoxybenzylidene)hydrazinocarbonyl]-1H-1,2,4-triazole

F.-Y. Pan and J.-G. Yang

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Dibenzyl 5-(2-chloroethyl)-3,7-diethyl-2,8-dimethyldipyrromethane-1,9-dicarboxylate

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1-(6-Bromopyridin-2-yl)-3-methyl-3H-imidazol-1-ium bromide monohydrate

B. Y. Cheng, J. Y. Zeng, P. L. Chiu and H. M. Lee

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2-Azido-2-deoxy-3,4-O-isopropylidene-2-C-methyl-D-ribono-1,5-lactone

F. Punzo, D. J. Watkin, S. F. Jenkinson, F. P. Cruz and G. W. J. Fleet

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(3R,4R,5S)-5-(Acetamidomethyl)-N-benzyl-3,4-dihydroxytetrahydrofuran-3-carboxamide

F. Punzo, D. J. Watkin, M. Iezzi Simone and G. W. J. Fleet

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Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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Acta E is now included in the Thomson Reuters Emerging Sources Citation Index.

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S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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