Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 61| Part 4

ISSN: 2056-9890

April 2005 issue

Highlighted illustration

Cover illustration: This relatively simple molecule is a rare example of a centrosymmetric molecule crystallizing in a general position in a non-centrosymmetric crystal structure. See Narasegowda, Malathy Sony, Mondal, Nagaraj, Yathirajan, Narasimhamurthy, Charles, Ponnuswamy, Nethaji & Rathore [Acta Cryst. (2005), E61, o843-o845].

inorganic compounds

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(Na_0.38,Ca_0.31)MgFe₂P₃O₁₂

M. F. Zid, A. Driss and T. Jouini

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Potassium bis(μ-sulfato-1κO:2κO′)bis[cis-dioxido-cis-bis(sulfato-κO)tungstate(VI)]

S. J. C. Schäffer and R. W. Berg

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Reinvestigation of NH₄[Co(H₂O)₆]PO₄ based on single-crystal data

B. El Bali, R. Essehli, F. Capitelli and M. Lachkar

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Dipotassium selenate tellurate

M. Dammak, A. Cousson and M. Nierlich

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Caesium thorium silicate, Cs₂ThSi₆O₁₅

J. D. Woodward, P. M. Almond and T. E. Albrecht-Schmitt

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(NH₄)₂[Co(H₂P₂O₇)₂(H₂O)₂]

R. Essehli, M. Lachkar, I. Svoboda, H. Fuess and B. El Bali

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(NH₄)₂[Ni(H₂P₂O₇)₂(H₂O)₂]

R. Essehli, M. Lachkar, I. Svoboda, H. Fuess and B. El Bali

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metal-organic compounds

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Hexakis(μ₄-2-amino-2-methylpropane-1,3-diolato)hexachloroheptairon(II,III) acetonitrile disolvate monohydrate

G. Labat, C. Boskovic and H. U. Güdel

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Dimethyl[4-methyl-2,6-bis(phenyliminomethyl)phenolato-κ²N,O]gallium(III)

W.-J. Gu, Y.-Z. Li, Y. Pan and S.-H. Liu

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Poly[zinc(II)-μ₂-azido-κ²N¹:N¹-μ₃-nicotinato-κ³N:O:O′]

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Bis(μ-4-nitropyridine N-oxide-κ²O:O)bis[dibromocopper(II)]

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Bis(1H-imidazole-κN³)bis(3-methylbenzoato-κO)copper(II)

T.-G. Xu, J.-G. Liu and D.-J. Xu

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Nonaaquaneodymium(III) trichloride bis(1,3,5,7-tetraazatricyclo[3.3.1.1^3,7]decane tetrahydrate

A. Trzesowska, R. Kruszynski, T. J. Bartczak and M. Zalewicz

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Piperazinediium hexaaquazinc(II) bis(sulfate): a structural analogue of Tutton's salts

W. Rekik, H. Naïli, T. Mhiri and T. Bataille

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Poly[[triaquacadmium(II)-μ₃-lactato] dilactatoboron(1–)]

M. Akkurt, S. Öztürk Yıldırım, J. Ramajothi, O. Büyükgüngör and S. Dhanuskodi

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catena-Poly[diaquazinc(II)-μ-(diethyl dichloromethylenebisphosphonato)-κ³O,O′:O′′-tetraaquazinc(II)-μ-(diethyl dichloromethylenebisphosphonato)-κ³O:O′,O′′]

M. Kontturi, S. Peräniemi, J. J. Vepsäläinen and M. Ahlgrén

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catena-Poly[diaquacadmium(II)-μ-(diethyl dichloromethylenebisphosphonato)-κ³O,O′:O′′-tetraaquacadmium(II)-μ-(diethyl dichloromethylenebisphosphonato)-κ³O:O′,O′′]

M. Kontturi, S. Peräniemi, J. J. Vepsäläinen and M. Ahlgrén

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Di-μ-chloro-bis{chloro[3,5-dimethyl-1-(thiocarbamoyl)pyrazole-κ²N²,S]cadmium(II)}

I. Radosavljević Evans, K. Mészáros Szécsényi and V. M. Leovac

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5-Ferrocenyl-5-methyltetrahydrofuran-2-one, the product of the Friedel–Crafts reaction of ferrocene with γ-methylenebutyrolactone

A. J. Rybarczyk-Pirek, D. Plażuk and J. Zakrzewski

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Tricarbonyl{η⁶-(S,S)-1-[2-methoxy-3,6-bis(trimethylsilyl)phenyl]-N,N-dimethylethylamine}chromium(0)

W. Braun, B. Calmuschi, D. Totev and A. Salzer

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Triphenyl[(2-oxidobenzylideneamino)acetato]antimony(V) dichloromethane solvate

G.-C. Wang, Y.-N. Lu, L. Yu, H.-B. Song and J.-S. Li

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{1,1′-[Propane-1,3-diylbis(nitrilomethylidyne)]di-2-naphtholato}iron(II)

B. Zhao and Y.-X. Sun

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Di-μ-iodo-bis[(1,10-phenanthroline-κ²N,N′)copper(I)] acetonitrile solvate

X.-P. Zhou, D. Li and S. W. Ng

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Heptaaqua(isonicotinato-κ²O,O′)lanthanum(III) 1,5-naphthalenedisulfonate

S. Gao, Z.-B. Zhu, L.-H. Huo and H. Zhao

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A co-crystal of 2-methylbenzimidazole and ammonium octamolybdate

S.-S. Feng, L.-P. Lu, H.-M. Zhang, S.-D. Qin, X.-M. Li and M.-L. Zhu

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catena-Poly[di-μ₃-benzoato-tetra-μ₂-benzoato-dipyrroletricadmium(II)]

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Octaureasamarium(III) triiodide

E. V. Savinkina, Y. F. A. Ansari, I. A. Zamilatskov, D. V. Albov and A. Y. Tsivadze

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μ-Piperidine-κ²N:N′-bis[(3-nitrobenzoato-κO)silver(I)] monohydrate

Y.-G. Li, M. Wang, L.-B. Zeng, Z.-L. You and H.-L. Zhu

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Tetraaquabis(hydrogen maleato)cadmium(II)

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1,4-Diazoniabicyclo[2.2.2]octane hexaaquacobalt(II) bis(sulfate)

Y.-J. Zhao, X.-H. Li and S. Wang

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[μ-5,11-Bis(dimethylethyleneamino)-2,8-dimethyl-1,4,5,6,7,10,11,12-octahydroimidazo[4,5-h]imidazo[4,5-c][1,6]diazecine]bis[aquasulfatocopper(II)] hexahydrate: a dinuclear copper sulfate complex based on a diazecine ligand

L. Gasque, E. Mijangos and L. Ortiz-Frade

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Bis(imidazolium) tetrachlorocobaltate(II)

H. Zhang, L. Fang and R. Yuan

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Bis[3,5-di-tert-butyl-2-hydroxybenzoato-κO]bis(dimethyl sulfoxide-κO)zinc(II)

T. Makino and J. Mizuguchi

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The first aluminium-bridged [1.1]ferrocenophane

J. A. Schachner, C. L. Lund, J. W. Quail and J. Müller

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catena-Poly[[[diaqua(imidazole)cadmium(II)]-μ-3-carboxylatophenoxyacetato] trihydrate]

S. Gao, L.-H. Huo, Z.-P. Deng and S. W. Ng

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Polymeric cobalt(II) diformate dimethylformamide 0.33-solvate

Y.-L. Fu, M. Ji, X.-L. Shen and S. W. Ng

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Bis(3-bromo-1-oxidoanthraquinone-κ²O¹,O⁹)bis(pyridine-κN)zinc(II)

H. M. Ali, S. N. Abdul Halim, S. Koushik, N. Hj. Lajis, W. J. Basirun and S. W. Ng

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[N,N-Dimethyl-N'-(2-pyridylmethylene)ethane-1,2-diamine]dithiocyanatocopper(II)

G.-R. Yue, X.-J. Xu, Y.-Z. Shi and L. Feng

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[4-Bromo-2-(pyridin-2-ylmethyliminomethyl)phenolato-κ³O,N,N′]methoxocobalt(III) perchlorate

J.-Y. Ma, T.-X. Wu, X.-G. She and X.-F. Pan

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Bis(tert-butylimido)[2-(dimethylaminomethyl)pyrrol-1-yl]tungsten(VI)-μ-oxo-bis(tert-butylimido)(η²-N,O-tert-butylnitroso)tungsten(VI)

C.-L. Uno, P.-C. Kuo, H. M. Lee and J.-H. Huang

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trans-Carbonylchlorobis(tri-m-tolylphosphino)rhodium(I) dichloromethane solvate

R. Meijboom, A. Muller and A. Roodt

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1,4-Diazoniabicyclo[2.2.2]octane diaquabis(pyrazole-3,5-dicarboxylato)zincate(II) dihydrate

X.-H. Li, X.-X. Lei, Y.-G. Tian and S. Wang

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Bis(4-carboxybenzenesulfonato)bis(1,10-phenanthroline)manganese(II)

L.-P. Zhang, L.-G. Zhu and H.-P. Xiao

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catena-Poly[[bis[4,4′-oxydibenzoato(1–)]cadmium(II)]-μ-1,2-di-4-pyridylethylene]

D.-W. Yin and H.-P. Xiao

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Tetrakis(1,4-dimethylpyridinium) dodecamolybdophosphate nitrate

X.-J. Tan, S.-X. Sun, J.-P. Ma, S.-L. Liu and D.-X. Xing

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Bis(pyrimidine-2-thiolato)bis(triphenylphosphine)ruthenium(II) chloroform solvate

Z. Li, J. Zhao, L. Liang and X. Zhou

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Bis(tetraethylammonium) bis(2-thioxo-1,3-dithiole-4,5-dithiolato)cuprate(II)

X.-Q. Wang, W.-T. Yu, D. Xu, Y.-L. Wang, T.-B. Li, G.-H. Zhang, X.-B. Sun and Q. Ren

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Bis{2-[3-(cyclohexylammonio)propyliminomethyl]phenolato}dithiocyanatocobalt(II)

G.-R. Yue, Y.-Z. Shi, M. Lin and L. Feng

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catena-Poly[[[4-bromo-2-(2-dimethylaminoethyliminomethyl)phenolato]zinc(II)]-μ-thiocyanato]

G.-R. Yue, X.-Y. Lei, X.-J. Xu and G.-Q. Xue

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catena-Poly[[diaquacadmium(II)]-μ-4-(carboxylatomethylsulfanyl)phenoxyacetato]

S. Gao, H. Su, L. H. Huo and S. W. Ng

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Hemi[4-(carboxymethoxy)phenylsulfanylacetato-κ²O,O′]hemi[4-(carboxymethylsulfanyl)phenyloxyacetato]bis(1,10-phenanthroline-κ²N,N′)cadmium(II) 4-(carboxymethoxy)phenylsulfanylacetate dihydrate

L.-H. Huo, S. Gao, H. Zhao and S. W. Ng

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(C₆H₁₆N₂)₂[Mo₈O₂₆]: a new β-octamolybdate salt

E. A. Muller, A. N. Sarjeant and A. J. Norquist

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Bis(4-amino-3-methylpyridine)diisothiocyanatozinc(II)

S. Chantrapromma, H.-K. Fun, X.-J. Feng, J.-X. Yang, J.-Y. Wu and Y.-P. Tian

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[1,2-Bis(diphenylphosphino)ethane]dichloro(methoxo)oxorhenium(V) dichloromethane solvate

A. L. Beauchamp and O. Sigouin

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(N-Hydroxy-N-phenylbenzamidato-κ²O,O′)oxo[salicylaldehyde (4-nitrobenzoyl)hydrazonato-κ³O,N,O′]vanadium(V)

S. Gao, L.-H. Huo, X.-F. Zhang and S. W. Ng

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A polymorph of cis-dichlorobis(phenanthroline-κ²N,N′)manganese(II)

T.-T. Pan and D.-J. Xu

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cis-Diaquabis(4-formyl-2-methoxyphenolato)zinc(II)

Z.-D. Lin and J.-Y. Lu

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Di-n-butyldicinnamatotin(IV)

M. Hong, H. Yin and D. Wang

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Benzamidinium tetrachlorogallate(III)

J. Barker, W. Errington and M. G. H. Wallbridge

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Tetraaquabis(1,4-di-4-pyridyl-2,3-diaza-1,3-butadiene)zinc(II) bis(perchlorate) and its supramolecular assembly

E. Tirosh, R. Maman and I. Goldberg

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Bis[2-(o-tolyliminomethyl)phenolato]copper(II)

H.-L. Zhu, K. Cheng, Z.-L. You and Y.-G. Li

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Caesium chloride 2-(N-morpholinio)ethanesulfonate

D. Milić, M. Renić and D. Matković-Čalogović

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2,2′-Bipyrimidinium hexachlororhenate(IV) dihydrate

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Poly[[bis(1H-benzimidazole-κN³)manganese(II)]-μ-aqua-μ-succinato-κ²O:O′]

H. Li, J.-G. Liu and D.-J. Xu

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Dipotassium ethane-1,1-diylbis(diazeniumdiolate) monohydrate

N. Arulsamy and D. S. Bohle

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Dichlorobis(pyridinium-2-thiolato)cadmium(II)

Y.-H. Wen and Y.-L. Feng

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Poly[[[(1,10-phenanthroline)manganese(II)]-μ₃-2-nitrobenzene-1,4-dicarboxylato] monohydrate]

L.-G. Zhu and H.-P. Xiao

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Diaqua[(1R,2R)-N,N′-bis(3,5-dibromosalicylidene)cyclohexane-1,2-diamine-κ⁴O,N,N′,O′]manganese(III) perchlorate dihydrate

T. Akitsu, Y. Takeuchi and Y. Einaga

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Diaquabis(dimethyl sulfoxide)bis(2,4-dinitrobenzoato)cobalt(II)

E. B. Miminoshvili, K. E. Miminoshvili and A. N. Sobolev

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Chlorobis[2-(2-pyridyl)phenyl-κ²N,C¹](triphenylphosphine-κP)iridium(III) dichloromethane sesquisolvate

Y. Wang, F. Teng, A. Tang, Y. Wang and X. Xu

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A 1:1 adduct of 3-(piperidin-1-yl)propionic acid with triphenyltin chloride

Y.-K. Yan and L. E. Khoo

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Bis[tris(3,5-dimethylpyrazolyl)methane]nickel(II) dibromide

A. Michaud, F.-G. Fontaine and D. Zargarian

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Chlorobis(1,10-phenanthroline-κ²N,N′)copper(II) nitrate 4-nitrobenzoic acid monohydrate

T.-G. Xu, J.-G. Liu and D.-J. Xu

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Tridecaaquadinitratohexasodium(I) bis[(trans-cyclohexane-1,2-diyldinitrilotetraacetato)nickelate(II)]

Y.-X. Long, L.-S. Long, R.-B. Huang, L.-S. Zheng and S. W. Ng

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Aquabis(2,2′-biimidazole)copper(II) dinitrate

R. Sang and L. Xu

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A cyano-bridged trimeric complex [Mn(CH₃OH)₂(H₂O)₂][Fe(bpb)(CN)₂]₂·2H₂O [bpb²⁻ is 1,2-bis(pyridine-2-carboxamido)benzenate]

Z.-H. Ni, H.-Z. Kou, L.-F. Zhang, Y.-B. Jiang and A.-L. Cui

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trans-Bis[4-(4-methoxyphenyl)-3,5-di-2-pyridyl-4H-1,2,4-triazole-κN¹]dithiocyanatocobalt(II)

S.-P. Zhang, S.-C. Shao, Z.-D. Liu and H.-L. Zhu

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organic compounds

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6,7-Dimethoxy-2-methyl-3,4-dihydroisoquinolin-1(2H)-one

I. M. Said, N. A. A. Hamid, J. Latif, L. B. Din and B. M. Yamin

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( $\pm$ )-5-Ethyl-1-methyl-5-phenylpyrimidine-2,4,6-trione at 163 K

W. Lewis, R. H. McKeown and W. T. Robinson

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2-Methoxy-5-methylphenyl phenyl ketone

S. M. Malathy Sony, P. Charles, M. N. Ponnuswamy and M. Nethaji

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8,9-Dihydro-1,6-dimethylphenanthro[1,2-b]furan-10,11-dione

J.-K. Qin, C.-Z. Liao, Y.-T. Wang, X.-Z. Bu, Z.-S. Huang and L.-Q. Gu

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5-(2-Chlorobenzamido)-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile

X.-H. Zhang, P. Zhong, Z.-P. Yang, M.-L. Hu and H.-P. Xiao

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4,4-Dinitro-5,6,7,8,9,10-hexahydro-4H-cyclonona[d]isoxazole

J. Lokaj, V. Kettmann, V. Milata and M. Marko

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2,4,6-Triamino-1,3,5-triazin-1-ium 4-methylbenzenesulfonate monohydrate

X.-M. Li, L.-P. Lu, S.-S. Feng, H.-M. Zhang, S.-D. Qin and M.-L. Zhu

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3-[(2R,3S)-3-(4-Chlorophenyl)-3-(2-methoxyanilino)-2-methylpropionyl]spiro[2H-1,3-benzoxazine-2,1′-cyclohexan]-4(3H)-one

S.-Z. Jian, J.-M. Gu and Y.-G. Wang

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tert-Butyl 1,4-dioxo-3,6-diphenyl-1,2,4,5-tetrahydropyrrolo[3,4-c]pyrrole-2-carboxylate

Y. Imura, T. Senju and J. Mizuguchi

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(E)-1-(4-Methylphenyl)-2-(4-nitrophenyl)ethene

R. De Borger, C. M. L. Vande Velde and F. Blockhuys

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2-(Methylsulfanyl)nicotinic acid

S. Basavoju, C. M. Reddy and G. R. Desiraju

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Diethyl 2-aminothiazole-4,5-dicarboxylate hemihydrate

D. E. Lynch and I. McClenaghan

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2-[Bis(4-methoxyphenyl)methyl]benzyl chloroacetate

P. G. Jones, P. Kuś and Ł. Łapok

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9-Methylene-10,10-bis(phenylethynyl)fluorene

P. G. Jones, P. Bubenitschek, H. Hopf and H. Berger

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2′-(3,4-Dimethoxybenzylidene)-2-hydroxybenzohydrazide

J.-G. Yang and F.-Y. Pan

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3-[(2-Hydroxybenzylidene)hydrazinocarbonyl]-1H-1,2,4-triazole ethanol solvate

C.-H. Ge, J.-G. Yang and F.-Y. Pan

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4-Phenyl-1-(1H-1,2,4-triazol-3-ylcarbonyl)thiosemicarbazide

D.-B. Chen, L. Huang, F.-Y. Pan and J.-G. Yang

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Bis(triphenylsilyl) phenylphosphonate

G. Ferguson, B. J. O'Leary and T. R. Spalding

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N-{3-Cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazol-5-yl}-4-nitrobenzamide ethanol solvate

P. Zhong, Z. Yang and Q. Shi

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2,2'-Diaminodibenzyl: a rare case of crystallographically non-compliant molecular symmetry

R. S. Narasegowda, S. M. Malathy Sony, S. Mondal, B. Nagaraj, H. S. Yathirajan, T. Narasimhamurthy, P. Charles, M. N. Ponnuswamy, M. Nethaji and R. S. Rathore

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5,3′-Dihydroxy-3,7,4′,5′-tetramethoxyflavone

S. Etti, G. Shanmugam, M. N. Ponnuswamy, K. Balakrishna and S. Vasanth

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4-(2-Chloroethyl)morpholinium chloride

R. S. Narasegowda, H. S. Yathirajan, P. Nagaraja and D. E. Lynch

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3-Cyano-N-methylpyridinium bromide

J. T. Mague, R. M. Ivie, R. W. Hartsock, L. V. Koplitz and M. Spulak

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A clerodane diterpenoid from Pulicaria wightiana

K. Ravikumar, B. Sridhar, B. Das and K. Venkateswarlu

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A low-temperature redetermination of metaldehyde

S. A. Barnett, A. T. Hulme and D. A. Tocher

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Amygdalin trihydrate

L. Eriksson and G. Widmalm

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3-(2,4-Dichlorophenyl)-4-[(1E)-(2,4-dichlorophenyl)methyleneamino]-4,5-dihydro-1H-1,2,4-triazole-5-thione dimethylformamide solvate

X.-N. Fang, F. Zhong, M.-Z. Dai and R.-H. Hu

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Bis[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-4H-1,2,4-triazol-3-yl] disulfide

F.-Y. Pan, J.-G. Yang, D.-B. Chen and L. Huang

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(3RS,1SR)-3-Bromo-3-(1-phenylpropyl)chroman-2,4-dione

D. Schollmeyer, B. Kammerer, C. Peifer and S. Laufer

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3-(4-Chlorobenzyl)-5-(4-oxo-4H-chromen-3-ylmethylene)-1,3-thiazolidine-2,4-dione

Ö. Özgen, M. Ceylan-Ünlüsoy, O. Bozdağ-Dündar, R. Ertan and E. Kendi

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2-(4-Bromophenyl)-5-(3,4-dimethoxyphenyl)-3,4-dimethylthiophene

Y. Lei, J. Shi, M. Yu and X. Zheng

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4-Chloro-2-(1-naphthyliminomethyl)phenol

Z.-X. Li and X.-L. Zhang

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Formation of non-centrosymmetric dimers in (1S,4aR,8aR*)-decahydronaphthalene-1-carboxylic acid

M. Davison, R. A. Lalancette and H. W. Thompson

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Benzoin thiosemicarbazone

M. Dinçer, N. Özdemir, A. Çukurovalı and İ. Yılmaz

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1-(Carbamoylmethyl)cyclohexanecarboxylic acid

B. Nagaraj, H. S. Yathirajan, P. Nagaraja and D. E. Lynch

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1,2-Bis(2-chlorophenyl)-1,2-bis(3,4-dimethylphenyl)ethane-1,2-diol

N. Sampath, S. Aravindhan, M. N. Ponnuswamy and M. Nethaji

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1-[2-(Biphenyl-4-yl)-2-oxoethyl]-4-(N,N-dimethylamino)pyridinium bromide hemihydrate

T. V. Sundar, V. Parthasarathi, K. Sarkunam, M. Nallu, B. Walfort and H. Lang

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N-(2,2-Dimethyl-4-oxo-1,3-thiazolidin-3-yl)-6-methylimidazo[2,1-b][1,3]thiazole-5-carboxamide monohydrate

S. Öztürk Yıldırım, M. Akkurt, F. Ur, Z. Cesur, N. Cesur and O. Büyükgüngör

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1-Carboxymethyl-3-iodo-1-pyridinium–iodide–(3-iodo-1-pyridinio)acetate (1/1/1)

P. G. Jones, B. Cots Carrasquer and E.-M. Zerbe

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(3S,6R)-3-Benzyloxymethyl-6-methyl-1,4-dioxane-2,5-dione

H. Kooijman, M. Leemhuis, C. F. van Nostrum, W. E. Hennink and A. L. Spek

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(3S,6S)-3-Benzyloxymethyl-6-methyl-1,4-dioxane-2,5-dione

H. Kooijman, M. Leemhuis, C. F. van Nostrum, W. E. Hennink and A. L. Spek

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2,3-Bis(5-bromo-2-thienyl)-6,7-dichloroquinoxaline

V. Stacy, G. Crundwell, J. B. Updegraff III, M. Zeller and A. D. Hunter

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Tris(triphenylsilyl)phosphate dichloromethane solvate

G. Ferguson, B. J. O'Leary and T. R. Spalding

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1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-[(4-methoxyphenyl)methyleneimino]-1H-pyrazole-3-carbonitrile

X. Zhang, Z. Yang, P. Zhong and M. Hu

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6,8′-Dimethoxy-2,2′-spirobichroman

G. R. Clark, C. L. Flowers and M. A. Brimble

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16α,17-Epoxy-11α-(p-tolylsulfonyloxy)pregn-4-ene-3,20-dione

Q. Nie, J.-K. Wang, S. Wang and M.-J. Zhang

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5-Bromo-1H-indole-3-carbaldehyde 2-thienoylhydrazone

H. M. Ali, S. N. Abdul Halim, N. H. Lajis, W. J. Basirun, S. M. Zain and S. W. Ng

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2-Oxo-2,3-dihydro-1H-indol-3-one nicotinoylhydrazone

H. M. Ali, S. N. Abdul Halim, W. J. Basirun and S. W. Ng

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Isopropyl 2,5-anhydro-4-(2,5-anhydro-4-azido-3-O-tert-butyldiphenylsilyl-4-deoxy-L-ribonylamino)-3-O-tert-butyldiphenylsilyl-4-deoxy-L-ribonate

S. Humphreys, D. J. Watkin, G. J. Sanjayan, G. E. Tranter, A. A. Edwards and G. W. J. Fleet

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(1R,2S,4S,5S)-Cyclohexane-1,2,4,5-tetrol

G. Mehta, S. Sen and S. Dey

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Methyl 3-amino-1-(2-chlorophenyl)-9-methoxy-5,6-dihydro-1H-naphtho[2,1-b]pyran-2-carboxylate

X.-S. Wang, Z.-S. Zeng, Y.-L. Li, D.-Q. Shi, X.-Y. Wei and Z.-M. Zong

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4-Acetylpyridinium chloride

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2-(3-Chloropropyl)-2,3-dihydro-1H-isoindole-1,3-dione

B. Nagaraj, H. S. Yathirajan and M. Bolte

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2-Acetamido-N-benzyl-1,4-imino-1,2,4-trideoxy-L-ribitol

C. C. Harding, D. J. Watkin, J. S. S. Rountree, T. D. Butters, M. R. Wormald, R. A. Dwek and G. W. J. Fleet

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(Z)-2-(3-Thienyl)-3-(3,4,5-trimethoxyphenyl)acrylonitrile

V. N. Sonar, S. Parkin and P. A. Crooks

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2-Benzoyl-1-tert-butyl-2-(1,2-dibenzoyl-2-tert-butylhydrazinosulfanyl)-1-(3,5-dimethylbenzoyl)hydrazine

J. Shang, Q.-M. Wang, H.-B. Song, R.-Q. Huang, L. Chen and C.-H. Mao

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4′-Methylbiphenyl-2-carboxylic acid

R. S. Narasegowda, H. S. Yathirajan and M. Bolte

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1,3-Dibromoazulene

X.-Y. Chen, J. R. Dias, D. R. Powell, J. D. Van Horn and T. C. Sandreczki

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1,3-Diiodoazulene

X.-Y. Chen, J. R. Dias, D. R. Powell, J. D. Van Horn and T. C. Sandreczki

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5-Methoxysalicylaldehyde 3-methoxybenzoylhydrazone

H. M. Ali, S. Puvaneswary, W. J. Basirun and S. W. Ng

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5-{[(4-Chlorophenyl)methylene]amino}-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile

Z. Yang, P. Zhong, Q. Shi, R. Tang and S. Li

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1,2-Bis(5-chloro-2-methyl-3-thienyl)cyclopentene

J.-T. Guan, J. Yin, G.-A. Yu and S.-H. Liu

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5-Chloromethyl-3-[4-(methylsulfonyl)phenyl]-1,2,4-oxadiazole

H.-B. Wang, J.-H. Chen, Y.-Q. Pu and J.-T. Wang

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2-(4-Bromophenyl)-1-methyl-1H-phenanthro[9,10-d]imidazole

C. B. Nielsen, M. Pittelkow and H. O. Sørensen

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9-Methylene-10,10-bis(phenylethynyl)fluorene–tetracyano-para-quinodimethane (2/3)

P. G. Jones, P. Bubenitschek, H. Hopf and H. Berger

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N-(2-Hydroxy-1-naphthylmethyl)-(S)-proline

C.-M. Dong, L.-G. Chen, X.-M. Duan, X.-G. Shu, T. Zeng and Y. Li

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N,N′-Bis(3-nitrobenzylidene)-trans-1,2-cyclohexanediamine

Z.-D. Liu, M.-Y. Tan and H.-L. Zhu

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4,4′-Bipyridinium dipicrate

L.-F. Ma, B.-T. Zhao and L.-Y. Wang

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17β-Hydroxy-28-norolean-12-ene-3,16-dione

S. Bai and L. Yang

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1-(2-Hydroxyphenyl)ethanone benzoylhydrazone

N. Ngah, N. Mohamad, M. Ahmad and B. M. Yamin

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4,5-Bis(pivaloylsulfanyl)-1,3-dithiolane-2-thione

Y. L. Wang, W. T. Yu, D. Xu, X. Q. Wang and G. H. Zhang

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17-Bromo-16-formyl-3-methoxyestra-1,3,5(10),16-tetraene

M. Watanabe, T. Matsumoto, S. Mataka and T. Thiemann

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(E)-3-(9-Ethyl-9H-carbazol-3-yl)-1-(2-hydroxyphenyl)prop-2-en-1-one

D.-X. Cao, G.-Z. Li, G. Xue, W.-T. Yu and Z.-Q. Liu

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21-Acetoxy-17α-4-pregnene-3,20-dione

R. Dey, S. Chanda, A. Pal and S. Roychowdhury

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2-Amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carbonitrile hemihydrate

S. Tu, J. Zhang, X. Zhu, J. Xu and Q. Wang

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An orthorhombic polymorph of dichlorobis[4-(dimethylamino)phenyl]tellurium

J. Beckmann, D. Dakternieks, A. Duthie and C. Mitchell

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1,3,3-Trimethyl-6′-(4-phenylpiperazin-1-yl)-2,3-dihydrospiro[1H-indole-2,3′-3H-naphth[2,1-b][1,4]oxazine]

H. Guo, Y.-B. Gao, Y.-X. Li, J. Han and J.-B. Meng

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3-[(2R,3S)-3-(2-Methoxyanilino)-2-methyl-3-phenylpropionyl]spiro[2H-1,3-benzoxazine-2,1′-cyclohexan]-4(3H)-one

S.-Z. Jian, J.-M. Gu and Y.-G. Wang

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L-Phenylalanine L-phenylalaninium malonate

M. Alagar, R. V. Krishnakumar, P. Parimala Devi and S. Natarajan

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1-Amino-N,N-dibenzyl-1,6-dideoxy-β-L-fructofuranose

C. C. Harding, D. J. Watkin, D. J. Hotchkiss, J. M. D. Cook and G. W. J. Fleet

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3-Bromo-2-(2-bromo-4,5-dimethoxybenzyl)-1-phenylsulfonyl-1H-indole

T. Ravishankar, K. Chinnakali, N. Arumugam, P. C. Srinivasan, A. Usman and H.-K. Fun

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erythro-2-(2,6-Dimethoxy-4-methylphenoxy)-1-(4-hydroxy-3,5-dimethoxyphenyl)propane-1,3-diol

V. Langer, K. Lundquist and G. E. Miksche

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5-(1-Cyclohexen-1-yl)-1,5-dimethylbarbituric acid (hexobarbitone): a low-temperature redetermination

G. S. Nichol and W. Clegg

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A quasi-planar polyaromatic compound containing an azo and a Schiff base linkage

R. J. Butcher, T. S. Basu Baul, K. S. Singh and F. E. Smith

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Methyl 3-dimethylamino-2-(2-{2-dimethylamino-1-[3-(3-pyridyl)-1,2,4-oxadiazol-5-yl]vinyloxy}phenyl)acrylate

H.-B. Wang, J.-H. Chen, Y.-Q. Pu and J.-T. Wang

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3-Hydroxysalicylaldehyde benzoylhydrazone

H. M. Ali, S. Puvaneswary, W. J. Basirun and S. W. Ng

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(E)-1-(1,3,6,8-Tetramethoxynaphthalen-2-yl)but-2-en-1-one

M. I. Choudhary, A. M. Lannang, S. Ali, S. Anjum and H.-K. Fun

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N-[3-(Hydroxymethyl)phenyl]-N′-(4-methoxybenzoyl)thiourea

N. Ngah, N. F. M. Fauzi and B. M. Yamin

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A polymorph of bavachalcone

K. Ravikumar, B. Sridhar, P. Aparna and J. M. Rao

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Redetermination of guaninium chloride dihydrate

T. C. Lewis and D. A. Tocher

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3,6-Diphenyl-1,4-bis(p-tolylsulfonyl)-1,4-dihydro-1,2,4,5-tetrazine

L. Lv, W. Hu, H.-B. Shi and G.-W. Rao

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Butane-1,4-diyl bis(bromoacetate)

M. Martínez-Palau, J. Puiggalí, X. Solans and L. Urpí

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N-(3-Methylphenyl)-N,N-bis(4-methylphenyl)amine

T. Manifar, S. Rohani and M. Jennings

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ent-(8S,10R)-15,16-Epoxy-19-norcleroda-4,11,13(16),14-tetraene-18,6(R):20,12-diolactone (isocrotocaudin)

I. M. Said, A. F. A. Noor, Y. M. Syah, J. Latif, N. Ngah and B. M. Yamin

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2-Hydroxy-2′-(4-isopropylbenzylidene)benzohydrazide

J.-G. Yang and F.-Y. Pan

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6,6,8a-Trimethyl-3a,6,7,8a-tetrahydrobenzo[b]furo[3,2-d]furan-2,4(3H,5H)-dione

B. Nagaraj, H. S. Yathirajan, P. Nagaraja and D. E. Lynch

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1-tert-Butyl-2-(4-ethylbenzoyl)-1-(2-mercapto-3,5-dimethylbenzoyl)hydrazine

J. Shang, Q.-M. Wang, R.-Q. Huang, L. Chen, H.-B. Song and C.-H. Mao

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Tricosane-1,23-dithiol

N. Nakamura, H. Shimizu and Y. Ogawa

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4-p-Tolyl-1,3,4,4a,5,6,7,8a-octahydro-2H-pyrano[2,3-d]pyrimidin-2-one

L. Yan, Y.-L. Zhu and Y.-J. Pan

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Redetermination of adeninium dichloride: the question of centrosymmetry

T. C. Lewis and D. A. Tocher

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5-Chloro-3-methyl-1-phenyl-1H-pyrazole-4-carbaldehyde: sheets built from C—H⋯O and C—H⋯π(arene) hydrogen bonds

J. Trilleras, J. Quiroga, J. Cobo, J. N. Low and C. Glidewell

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11-(4-Chlorophenyl)-10-methyl-8-phenyl-6,8-dihydro-5H-benzo[f]pyrazolo[3,4-b]quinoline

H. Serrano, J. Quiroga, J. Cobo, J. N. Low and C. Glidewell

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2,9-Dichloro-5,12-dihydroquino[2,3-b]acridine-7,14-dione

T. Senju, T. Hoki and J. Mizuguchi

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Dibenzimidazo[2,1-a:2′,1′-a′]anthra[2,1,9-def:6,5,10-d′e′f′]diisoquinoline-10,21-dione: trans form (I)

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Dibenzimidazo[2,1-a:1′,2′-b′]anthra[2,1,9-def:6,5,10-d′e′f′]diisoquinoline-6,11-dione: cis form (II)

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N-(2-Fluorobenzylidene)-2,6-diisopropylaniline

H.-Y. Gao, X.-Q. Lü, F. Bao, Q. Wu and S. W. Ng

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2-(2,6-Diisopropylphenylamino)cyclohex-1-enyl phenyl ketone

G.-Q. Gui, F. Bao, X.-Q. Lü, Q. Wu and S. W. Ng

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N,N′-Ethylenedisuccinimide

C. L. Brown, S. J. Atkinson and P. C. Healy

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(Z)-3-(4-Methoxybenzylidene)-2-methylisoindolin-1-one

K.-D. Warzecha, J. M. Neudörfl and A. G. Griesbeck

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3-(4-Bromo-1H-pyrrole-2-carboxamido)propanoic acid

X.-C. Zeng, S.-H. Xu, P.-R. Liu and J. Gu

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3-Hydroxysalicylaldehyde 2-furoylhydrazone

H. M. Ali, S. Puvaneswary, W. J. Basirun and S. W. Ng

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(5,6-Dihydroxy-2-methyl-1-benzofuran-3-yl) phenyl ketone

L.-X. Pei, X.-Z. Bu, L.-Q. Gu and S. W. Ng

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3-Hydroxysalicylaldehyde 2-thienoylhydrazone

H. M. Ali, S. Puvaneswary, W. J. Basirun and S. W. Ng

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(2R,3R)-Diacetyltartaric acid anhydride

Z.-B. Qi, M.-J. Zhang, D.-Y. Yuan, S.-S. Ma and X.-Q. Wang

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2-Iodoaniline at 100 K

A. Parkin, C. K. Spanswick, C. R. Pulham and C. C. Wilson

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4-Phenylpyridinium betaine of squaric acid

T. Kolev, R. Wortmann, M. Spiteller, W. S. Sheldrick and H. Mayer-Figge

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N-(4-Methoxybenzoyl)-N′-(4-methoxyphenyl)thiourea

H. M. Ali, S. N. Abdul Halim, W. J. Basirun and S. W. Ng

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2-(2,3-Dimethoxyphenyl)chroman-4-one

H. Wu, Z. Xu, J. Zhou and Y.-M. Liang

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2-Hydroxy-6-[(2-hydroxyphenylamino)methylene]cyclohexa-2,4-dienone

B. Koşar, C. Albayrak, M. Odabaşoğlu and O. Büyükgüngör

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4-Methyl-3,5-dinitrobenzoic acid–dimethyl sulfoxide (1/1)

A. V. Trask, M. Abthorpe and W. Jones

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1,6-Bis(pyridine-4-carboxamido)hexane

C.-F. Ding, M. Zhu, X.-M. Li, S.-S. Zhang, H. Xu and P.-K. Ouyang

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Ethyl 5-bromosalicylate

L.-F. Jin and F.-P. Xiao

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Methyl 5-nitrosalicylate

L.-F. Jin and F.-P. Xiao

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1-Acetyl-2-phenylperhydroquinolin-4-yl acetate

R. Padmavathy, K. Saminathan, D. Natarajan, N. Bhavani and K. Sivakumar

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6-tert-Butyl-4-isopropylideneamino-3-methylsulfanyl-1,2,4-triazin-5(4H)-one

D. Chopra, T. P. Mohan, K. S. Rao and T. N. Guru Row

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Ethyl 6-amino-5-cyano-2-methyl-4-phenyl-4H-pyran-3-carboxylate

Y.-L. Li, X.-S. Wang, Z.-S. Zeng, D.-Q. Shi, X.-Y. Wei and Z.-M. Zong

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Ethyl propionate at 185 K

H. A. Shallard-Brown, D. J. Watkin and A. R. Cowley

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4,5-Bis(3-methoxyphenylsulfanyl)phthalonitrile

T. Akbal, N. Akdemir, M. Özil, E. Ağar and A. Erdönmez

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5-Methoxyspiro[1-benzofuran-2(3H),2′-chroman]

G. R. Clark, K. Y. Tsang and M. A. Brimble

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(S)-2-Ammoniobutan-1-ol (2R,3R)-tartrate

G.-Y. Bai, L.-G. Chen, Y. Li, X.-L. Yan, P. Xing, C.-M. Dong, X.-M. Duan, Y.-C. Zhang and F.-Y. Ge

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Benzyltrimethylammonium dihydrogen orthophosphate monohydrate

A. Criado, M. J. Diánez, M. D. Estrada, S. Pérez-Garrido, M. Belsley and E. de Matos Gomes

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3-[(2-Hydroxyphenyl)amino]-1-phenylbut-3-en-1-one ethanol solvate

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2,4,6-Tris(pyrimidin-2-ylsulfanyl)-1,3,5-triazine

L. Zhang, X.-H. Zhao and X.-D. Wang

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(1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl (2S,3S)-3-phenyloxirane-2-carboxylate

S.-Z. Jian and Y.-G. Wang

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2-(o-Tolyliminomethyl)phenol

K. Cheng, Z.-L. You, Y.-G. Li and H.-L. Zhu

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9-Butyl-3,4,5,6,7,9-hexahydro-2H-xanthene-1,8-dione

Y.-L. Zhu, S.-L. Huang and Y.-J. Pan

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Low-temperature (110 K) single-crystal neutron diffraction study of (±)-camphoric anhydride

D. B. Kgomo, D. C. Levendis, A. Gukasov, A. Cousson, L. F. R. Schöning and A. M. Venter

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17-Oxo-5β-hydroxyandrostan-3β-yl acetate

L. C. R. Andrade, J. A. Paixão, M. J. M. de Almeida, E. J. Tavares da Silva and F. M. Fernandes Roleira

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7-Methyl-1-(β-D-erythro-pentofuranosyl)-1H-benzimidazol-2(3H)-one

Q. Ji, H. Guo, H.-B. Song, F. Huang and J.-B. Meng

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2,6-Bis(4-nitrobenzylidene)cyclohexanone

J. W. Quail, U. Das and J. R. Dimmock

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3-Methylanilinium picrate

C. Muthamizhchelvan, K. Saminathan, J. Fraanje, R. Peschar and K. Sivakumar

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1,4-Bis(4-dimethylaminobenzyl)-2,3-diaza-1,3-butadiene

Q.-H. Wang, G.-C. Guo and M.-S. Wang

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2-({4-[3-Methyl-3-(2,4,6-trimethylphenyl)cyclobutyl]-3H-thiazol-2-ylidene}hydrazonomethyl)benzene-1,4-diol ethanol solvate

C. Yüksektepe, M. S. Soylu, H. Saraçoğlu, I. Yılmaz, A. Çukurovali and N. Çalıs˛kan

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1,1′-Diphenyl-5,5′-[o-phenylenebis(methylenethio)]di-1H-tetrazole

X.-L. Luo, W. Wang, G.-C. Ma and W.-Q. Zhang

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5,5'-[(p-Phenylenedimethylene)dithio]bis(1-phenyl-1H-1,2,3,4-tetrazole)

W. Wang, B. Zhao, P.-W. Zheng and X.-M. Duan

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β-DL-Methionine at 105 K

M. Alagar, R. V. Krishnakumar, A. Mostad and S. Natarajan

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2,4-Dichloro-6-morpholino-1,3,5-triazine

C.-M. Dong, L.-G. Chen, X.-M. Duan, X.-G. Shu, T. Zeng and X.-L. Yan

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2-Bromobenzophenone

V. N. Baumer, R. V. Romashkin, M. A. Strzhemechny, A. A. Avdeenko, O. S. Pyshkin, R. I. Zubatyuk and L. M. Buravtseva

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Methyl β-N-(3-nitrophenylmethylene)dithiocarbazate

Y.-L. Zhang, S. Shan and D.-J. Xu

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3-Cyclohexyl-4-(3-methyl-3-phenylcyclobutyl)-1,3-thiazole-2(3H)-thione

C. Kırılmış, M. Koca, C. Arıcı, F. W. Heinemann and M. Ahmedzade

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Redetermination of the Diels–Alder diadduct of 1,4-benzoquinone and cyclopentadiene: 1,4:5,8-dimethano-1,1a,4,4a,5,5a,8,8a-octahydroanthracene-9,10-dione

A. A. Yakovenko and F. M. Dolgushin

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1-(4,6-Dimethylpyrimidin-2-ylsulfanyl)-3,3-dimethylbutan-2-one

L.-Z. Xu, X.-L. Ma, H.-B. Song, Q. Zhu and Y.-X. Yang

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A perchlorate salt of 1-[(2-dimethylaminoethylimino)methyl]naphthalen-2-ol

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2-(3-Bromo-1-phenylsulfonyl-1H-indol-2-ylmethylsulfanyl)-6-methyl-1H-benzimidazole

T. Ravishankar, K. Chinnakali, N. Arumugam, P. C. Srinivasan, A. Usman and H.-K. Fun

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O-(2,3,4,5,6-Pentafluorobenzyl)hydroxylaminium chloride

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(3S,4S,5S,10S,13R,14R,17R)-4α,14α-Dimethyl-3β-tosyl-5α-cholest-8-ene-7,11-dione

A. Auhmani, M. Giorgi and N. Mazoir

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4'-(2-Butyl-4-chloro-5-formylimidazol-1-ylmethyl)biphenyl-2-carbonitrile

H. S. Yathirajan, B. Nagaraj, R. S. Narasegowda, P. Nagaraja and M. Bolte

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6,6′-Dioxo-2,2-bi(7-oxatricyclo[3.2.1.1^3,8]nonane)-4,4′-dicarboxylic acid

M.-L. Hu, Y.-Q. Cheng, S. Wang, J.-X. Yuan and X.-Q. Cai

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Ethyl 5-nitrosalicylate

L.-F. Jin and F.-P. Xiao

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(E,E,E)-1,6-Bis(4-nitrophenyl)hexa-1,3,5-triene

Y. Sonoda, Y. Kawanishi and M. Goto

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Succinimido 4-(N-maleimidomethyl)cyclohexanecarboxylate

C. L. Brown, S. J. Atkinson and P. C. Healy

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1-(1-Benzofuran-2-yl)ethanone O-(2-chlorobenzoyl)oxime

N. Ocak Ískeleli, C. Kazak, C. Kırılmış and M. Koca

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Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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Acta E is now included in the Thomson Reuters Emerging Sources Citation Index.

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