Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 62| Part 3

ISSN: 2056-9890

March 2006 issue

Highlighted illustration

Cover illustration: Surprisingly, the single-crystal structure of ammonium hydrogenselenate(IV) has not hitherto been determined. It is isostructural with KHSeO₃ and contains tetrahedral ammonium cations and trigonal-pyramidal HSeO₃^- anions. The structure is held together by an intricate network of weak hydrogen bonds. See Weil [Acta Cryst. (2006), E62, i38-i40].

editorial

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Structure Reports Online: further growth leads to major changes

W. Clegg and D. G. Watson

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international union of crystallography

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Notes for authors 2006

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inorganic compounds

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Ammonium hydrogenselenate(IV)

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Tetracaesium octaselenidotetraarsenate(III)

T. Van Almsick and W. S. Sheldrick

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Sodium peroxodisulfate

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Cobalt mercury tetraselenocyanate, CoHg(SeCN)₄

S.-L. Li, H.-K. Fun, S. Chantrapromma, J.-Y. Wu and Y.-P. Tian

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Garnet-type Li_2.44K_0.56Cr₂(AsO₄)₃

S. Kouass, B. Bouzemi and H. Boughzala

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Trisodium dihydroxotetraoxoosmate(VII), Na₃[OsO₄(OH)₂]

K. M. Mogare, W. Klein and M. Jansen

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Dy₂AlGe₂

G. Demchenko, J. Kończyk, P. Demchenko, V. Kuprysyuk and R. Gladyshevskii

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Rietveld refinement of the Tutton salt K₂[Fe(H₂O)₆](SO₄)₂

P. Ballirano and G. Belardi

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Praseodymium dodecaiodo-ferro-octahedro-hexapraseodymium, Pr₇I₁₂Fe

A. Palasyuk, I. Pantenburg and G. Meyer

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Partial Pd occupancy in uranium palladium diantimonide, UPd_0.603(6)Sb₂

S. Bobev, D. J. Mixson, E. D. Bauer and J. L. Sarrao

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Uranium copper diantimonide, UCu_0.44(1)Sb₂ with a large Cu deficiency

S. Bobev, D. J. Mixson, E. D. Bauer and J. L. Sarrao

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Ta_1.40(1)Mn_4.60(1)Si₅: distribution of the Ta and Mn atoms

S. Bobev, E. D. Bauer and J. L. Sarrao

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Redetermination of di-μ-bromo-bis[tetracarbonylmanganese(I)] at low temperature

A. Haghiri, H.-W. Lerner and M. Bolte

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Rb₂Cd₃(SO₄)₃(OH)₂·2H₂O: structural stability at 500 K

D. Swain and T. N. Guru Row

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metal-organic compounds

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catena-Poly[[diaquabarium(II)]-di-μ-2-formylbenzoato]

M. Odabaşoǧlu and O. Büyükgüngör

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[μ-1κC¹:2(C²,C³-η)-Allyl]tetracarbonyl-1κ²C,2κ²C-(1η⁵-cyclopentadienyl)(2η⁵-pentamethylcyclopentadienyl)rutheniumiron hexafluorophosphate

H. B. Friedrich, E. O. Changamu and M. Rademeyer

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Di-μ-bromo-bis[bis(1,2-diaminoethane-κ²N,N)nickel(II)] dibromide

M. Xie and R. E. Norman

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Layered triaqua(phenylselenonato)lithium(I)

A. Machado and R. A. Burrow

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(2,2′-Bipyridine-5,5′-dicarboxylic acid)tetrachloroplatinum(IV) monohydrate

J. Hafizovic, U. Olsbye and K. P. Lillerud

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(4-Acetylpyridine)(tetraphenylporphyrinato)zinc(II)

S. Lipstman, S. George and I. Goldberg

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Tetrakis(μ₂-2,2-dimethylpropanoato-κ²O,O′)bis[(pyridine-κN)copper(II)]

G. Blewett, C. Esterhuysen, M. W. Bredenkamp and K. R. Koch

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Bis{2-[3-(cyclohexylamino)propyliminomethyl]-4-nitrophenolato}copper(II) diperchlorate

Y.-X. Sun, M. Qin, K.-Q. Gu, G. Yang and F. Xie

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[1,1′-Bis(diphenylphosphino)cobaltocenium-κ²P,P′]chloro(η⁵-pentamethylcyclopentadienyl)ruthenium(II) hexafluorophosphate dichloromethane hemisolvate

X.-H. Wu, Y. Ren, G.-A. Yu and S.-H. Liu

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Di-μ-bromo-2κ²Br:2′κ²Br-bis[bis(μ-acetylacetonato-1κO:2κO′)bromo-2κBr-bis(tetrahydrofuran-1κO)cadmium(II)nickel(II)]

M. Döring, G. Hahn and W. Imhof

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Pentacarbonyl[N,N-dimethyl-N′-(5-{2-[5-(4-pyridylethynyl)thiophen-2-yl]vinyl}thiophen-2-ylmethylene)benzene-1,4-diamine]tungsten(0)

P.-H. Huang, T.-H. Huang, J.-Y. Shen and Y.-S. Wen

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Tris(tert-butyl 3-oxobutanoato-κ²O¹,O³)aluminium(III) at 153 K

M. S. Dharmaprakash, S. Thamotharan, G. M. Neelgund and S. A. Shivashankar

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Di-μ-iodo-1:2κ⁴I:I-diiodo-2κ²I-tris(1,10-phenanthroline)-1κ²N,N′;2κ²N,N′-bismuth(III)sodium(I)

F. Li, H. Yin and D. Wang

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[μ-1,2-Bis(phenylsulfanyl)ethane-κ²S:S′]bis[dibromomercury(II)]

J.-B. Gong, L.-N. Zhou and W. Chen

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[μ-1κC¹:2(C²,C³-η)-Allyl]tetracarbonyl-1κ²C,2κ²C-(1η⁵-cyclopentadienyl)(2η⁵-pentamethylcyclopentadienyl)diiron(II) hexafluorophosphate

E. O. Changamu, H. B. Friedrich and M. Rademeyer

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Hexakis(1-methyl-1H-imidazole-κN³)nickel(II) dichloride dihydrate

W.-H. Wang, X.-Y. Su, Z.-H. Mao, J.-S. You and R.-G. Xie

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An enriched hydrogen-bond system in trans-diaquabis(N,N-diethylnicotinamide-κN)bis(3-methoxysalicylato-κO)copper(II) dihydrate

J. Moncol, Z. Púčeková, T. Lis and D. Valigura

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{4-[1-(4-Hydroxyphenyl)-1-methylethyl]phenoxy}trimethyltin(IV)

Aziz-ur-Rehman, S. Ali, M. Najam-ul-Haq, S. Shahzadi and K. Wurst

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Tetraethylammonium dichlorotris(2,6-dimethylphenylsulfanyl-κS)ruthenium dichloromethane solvate

Y.-W. Song, Z. Yu and Q.-F. Zhang

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Bis(tetra-n-butylammonium) tetrabromocadmate(II) toluene disolvate

A. Kropidłowska, J. Chojnacki and B. Becker

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μ-Isophthalato-bis[triphenyltin(IV)]

W.-L. Zhang, J.-F. Ma and H. Jiang

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fac-Tris(tert-butyl isocyanide)tricarbonylmolybdenum(0)

W. Imhof, K. Halbauer, D. Dönnecke and H. Görls

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Di-μ-hydroxo-κ⁴O:O-bis[aquatris(triphenylsilanolato-κO)zirconium(IV)] toluene solvate

B. Schweder, D. Walther and W. Imhof

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catena-Poly[tributyltin(IV)-μ-acetato]

M. A. Saeed, A. Badshah, M. K. Rauf, D. C. Craig and S. Ali

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Lithiation of the diaminopyridine protio-ligand MeC(2-C₅H₄N){CH₂N(H)Mes}₂ (Mes = 2,4,6-C₆H₂Me₃)

B. D. Ward, L. H. Gade and P. Mountford

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tert-Butyl isocyanide-1κC-di-μ-carbonyl-2:3κ⁴C-nonacarbonyl-1κ³C,2κ³C,3κ³C-triangulo-diironosmium

C. Evans, L. J. Farrugia and M. Tegel

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Bis(tert-butyl isocyanide)-1κ²C-di-μ-carbonyl-2:3κ⁴C-octacarbonyl-1κ²C,2κ³C,3κ³C-triangulo-diironosmium

C. Evans, L. J. Farrugia and M. Tegel

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Poly[[aqua(μ₄-1,4-cyclohexanedicarboxylato)praseodymium(III)] hemihydrate]

G.-B. Che, C.-B. Liu, H. Liu and B. Liu

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Bis[(4-bromobenzyl)triphenylphosphonium] bis(1,2-dicyanoethane-1,2-dithiolato-κ²S,S′)nickel(II) monohydrate

S.-B. Yang and C.-L. Ni

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Dicyanatobis(1,10-phenanthroline)manganese(II)

Z.-X. Li, M.-M. Yu, Z.-H. Ni, H.-Z. Kou and W.-F. Fu

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Tris(2-methyl-2-phenylpropyl)(2-phthalimidoacetato-κO)tin(IV)

L.-J. Tian, F.-Y. Yu, Y.-X. Sun and X.-C. Liu

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Bis[η³-2-tert-butyl-1,3-bis(trimethylsilyl)-1-azaallyl]cobalt(II)

Y. Zhang, H.-B. Tong, D.-S. Liu, M.-S. Zhou and S.-P. Huang

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μ-Oxo-bis[(diethyl 6,17-dimethyldibenzo[a,h]-5,9,14,18-tetraaza[14]annulene-7,16-dicarboxylato)iron(III)] sesquihydrate

E.-G. Jäger, J. Knaudt and W. Imhof

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Potassium 3,5-dinitrobenzoate

Y.-P. Du and M.-C. Hu

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{Tris[2-(2-pyridylmethyleneimino)ethyl]amine}manganese(II) bis(perchlorate)

S.-N. Li, Y.-W. Ren, J. Li, F.-X. Zhang and M.-C. Hu

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Chloro[(4R,9R,14R,19R)-24-chloro-2,21-dimethyl-3,10,13,20,26-pentaazatetracyclo[20.3.1.0^4,9.0^14,19]hexacosa-1(26),2(3),20(21),22(23),24-pentaene](methoxo)manganese(II) chloride monohydrate

H.-Y. Tu, C.-J. Wang, X.-G. Meng and A.-D. Zhang

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trans-Dichlorobis[(S)-(–)-1-(1-naphthyl)ethylamine]palladium(II)

J. Vázquez, S. Bernès, G. Hernández, H. Aguilar and R. Gutiérrez

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Hexakis(N,N-dimethylacetamide)nickel(II) bis(tetrafluoroborate) 0.17-hydrate

H. Suzuki and S. Ishiguro

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cis-Diaqua(1,10-phenanthroline-κ²N,N′)(pyridine-2,5-dicarboxylato-κ²N,O)manganese(II) monohydrate

S.-M. Zhao and T.-X. Wu

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N-(1-Ferrocenylethyl)-N-(1-phenylethyl)methylamine

Z.-G. Yin, H.-Y. Qian, J. Jia and C.-X. Zhang

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Aqua(dipicolinato-κ³O,N,O′)(1,10-phenanthroline-κ²N,N′)zinc(II) monohydrate

W. T. A. Harrison, P. Ramadevi and S. Kumaresan

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Bis[2,4,6-triisopropyl-N-(quinolin-8-yl)benzenesulfonamidato-κ²N,N′]zinc(II)

L. E. da Silva, A. C. Joussef, S. Foro and B. Schmidt

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Bis[4-nitro-N-(quinolin-8-yl)benzenesulfonamidato-κ²N,N′]copper(II)

L. E. da Silva, A. C. Joussef, S. Foro and B. Schmidt

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Dichloro(4,4′-di-tert-butyl-2,2′-bipyridine-κ²N,N)bis(triphenylphosphine-κP)ruthenium(II) dichloromethane solvate

Y.-W. Song, Z. Yu and Q.-F. Zhang

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catena-Poly[[bis(isothiocyanato-κN)copper(II)]bis(μ-1,1′-methylenedi-1H-imidazole-κN³:κN^3′)]

G.-H. Cui, G.-Y. Dong and J. Ribas

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μ-Hexatriacontaoxophosphatododecamolybdato-bis[bis(1,10-phenanthroline)copper(II)]

Y.-P. Bai and E. Wang

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(2,2′-Bipyridyl)bis(pentane-2,4-dionato)vanadium(III) perchlorate dichloromethane solvate

S. J. Kavitha, K. Panchanatheswaran, J. N. Low and C. Glidewell

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Tris(ethylenediamine)nickel(II) tetraoxomolybdate(VI)

B.-Z. Lin, G.-H. Han, F. Geng and C. Ding

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trans-Dichlorobis(10-dodecyl-9-phospha-10-silatriptycene-κP)palladium(II)

H. Tsuji, T. Inoue, S. Sase and K. Tamao

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Bis(ethylenediammonium) diaquabis[hydrogendiphosphato(3–)]nickelate(II): structure and vibrational spectroscopy

R. Essehli, B. El Bali, M. Lachkar, I. Svoboda and H. Fuess

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A coordination polymer of thallium(III) nitrate with 4,4′-bipyridine N,N′-dioxide

L. J. Moitsheki, S. A. Bourne and L. R. Nassimbeni

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Poly[diaquadi-μ₅-succinato-μ₆-succinato-didysprosium(III)]

C.-X. Wang, Y. Li, Q.-H. Zhang, D.-J. Cai and X.-B. Xie

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catena-Poly[[[cis-diaqua(2,2′-bipyridine)cadmium(II)]-μ-3-sulfonatobenzoato] monohydrate]

X.-H. Miao and L.-G. Zhu

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catena-Poly[[[(3,5-dimethyl-1H-pyrazole-κN²) copper(II)]-μ-[(3,5-dimethyl-1H-pyrazol-1-yl)methylamino]acetato] nitrate monohydrate]

E. F. Abdeljalil, B. L. Najib, K. Abdelali, B. El Bali and M. Bolte

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Di-μ-chloro-μ-(dimethyl sulfide)-bis[dichloro(dimethyl sulfide)niobium(III)]

M. Kakeya, T. Fujihara and A. Nagasawa

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Bis(tetraethylammonium) bis[N-(2-mercaptobenzoyl)-1,3-benzothiazole-2-carboxamidato]cobaltate(III) chloride

M. J. Frome, L. E. Cooper, B. J. Lewis, M. J. Ferguson and C. J. A. Daley

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Bis{5-methyl-2-phenyl-4-[(3-tolylamino-κN)phenylmethylene]-1H-pyrazol-3(4H)-onato-κO}cobalt(II)

F. Bao, Y.-H. Jiao and S. W. Ng

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Potassium (4-methyl-2-oxo-2H-chromen-7-yloxy)sulfate

K. Sierosławski, K. Ślepokura and T. Lis

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Di-μ-acetato-bis[μ-2-hydroxy-N,N′-bis(2-oxidobenzyl)propane-1,3-diamine]bis(N,N′-dimethylformamide)trinickel(II) N,N′-dimethylformamide disolvate

M. Sarı, O. Atakol, I. Svoboda and H. Fuess

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Bis(morpholinium) tetraiodo(morpholine-4-carbodithioato-κ²S,S′)bismuth(III)

F. Li, H. Yin and D. Wang

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Bis[N,N′-bis(trimethylsilyl)benzamidinato]diethylhafnium(IV)

R. Fischer, D. Walther and W. Imhof

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trans-Bis(acetylacetonato-κ²O,O′)mesityl(tetrahydrofuran-κO)vanadium(III)

W. Imhof and W. Seidel

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fac-Dichlorotris(trimethylphosphine)(trimethylphosphoniomethyl)rhodium(III) chloride/bromide dichloromethane benzene solvate

A. S. Batsanov, T. B. Marder and F. Seeler

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N,N-Dimethylacetamide complex of aluminium(III) perchlorate

H. Suzuki and S. Ishiguro

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Tris(1H-benzimidazole-κN³)(thiodiacetato-κ³O,S,O′)cobalt(II) dihydrate

L. Cao, J.-G. Liu and D.-J. Xu

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Poly[diaquadi-μ-malonato-manganese(II)disodium(I)]

Y.-T. Wang, G.-M. Tang and X.-Y. Qin

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Bis(2,2′-bipyridine)[2-(2-pyridyl)-1H-benzimidazol-1-yl]ruthenium(II) perchlorate acetonitrile solvate monohydrate

Y.-J. Liu, H. Chao, H.-J. Yu, Y.-X. Yuan and L.-N. Ji

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Cocrystallization of dichloro(N,N-dimethylformamide)[hydrotris(pyrazol-1-yl)borato]vanadium(III) with its partially oxidized analog chloro(N,N-dimethylformamide)[hydrotris(pyrazol-1-yl)borato]oxovanadium(IV)

C. C. McLauchlan and K. J. McDonald

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Bis[4-(4-methoxyphenyl)-3-methyl-5-(2-pyridyl)-4H-1,2,4-triazole-κN¹]bis(salicylato-κO)copper(II) methanol disolvate

A.-Y. Zhou, Z.-X. Wang, Y. Lan, L.-T. Yuan and C.-Y. Liu

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Diammine[pyridine-2,6-dicarboxylato-κ³O²,N,O⁶]zinc(II)

J. Xiang and X.-C. Lin

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catena-Poly[[bis(tetrafluoroborato)copper(II)]bis[μ-1,3-bis(ethylsulfinyl)propane-κ²O:O′]]

Y. Tao, Q. Yu and J.-R. Li

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μ-Oxalato-bis[chlorotripyridinecobalt(II)] pyridine disolvate

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Azido{2,4-dichloro-6-[2-(diethylamino)ethyliminomethyl]phenolato}nickel(II)

F.-W. Wang and Y.-J. Wei

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Di-μ-hydroxo-bis[(2,2′-bipyridine)palladium(II)] trifluoromethanesulfonate

R. A. Adrian, R. E. Benson, L. M. Daniels, E. R. T. Tiekink and J. A. Walmsley

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Aquadichloro(2,9-dimethyl-1,10-phenanthroline-κ²N,N)copper(II)

C.-F. Ding, X.-M. Li, M. Zhu, H. Xu and S.-S. Zhang

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μ-1,1′-Methylenedi-1H-imidazole-κ²N³:N^3′-bis[aqua(pyridine-2,6-dicarboxylato)copper(II)] tetrahydrate

G.-Y. Dong, G.-H. Cui and S.-C. Wang

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Bis(ethylenediamine-κ²N,N′)(2-oxido-5-sulfonatobenzoato-κ²O¹,O²)chromium(III) dihydrate

B. Liu, Z.-J. Wang, S.-P. Huang and B.-S. Yang

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Bis{2-[1-(adamantan-1-yl)ethyliminomethyl]phenolato-κO}dichloromanganese(II)

J.-L. Huang and Y.-H. Wen

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catena-Poly[[dibromomercury(II)]-μ-1,5-bis(benzylsulfanyl)pentane-κ²S:S′]

Q. Yu, Y. Tao and J.-R. Li

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Bis(thiocyanato-κN)bis(2,2′-thiodipyridine-κ²N,N′)nickel(II) monohydrate

Q.-H. Zhao, X.-M. Mu, M.-S. Zhang and R.-B. Fang

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Tetra-μ-1,1′-dimethyl-2,2′-bi-1H-imidazole-bis[aquacopper(II)] tetranitrate hexahydrate

L. M. Gruia, F. D. Rochon and A. L. Beauchamp

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Bis(2,2′-bipyridine-κ²N,N′)copper(I) trifluoromethanesulfonate

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Bis(N-ethylpyridinium) bis(2-thioxo-1,3-dithiole-4,5-dithiolato)zincate(II)

Y.-L. Wang, W.-T. Yu, H.-Y. Chen, D. Xu and W.-F. Guo

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trans-Bis(4-aminopyridine-κN)bis(succinimidato-κN)copper(II) dihydrate

T. Akitsu and Y. Einaga

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catena-Poly[[aqua(4,4′-dimethyl-2,2′-bipyridine)copper(II)]-μ-fumarato-κ²O,O′:κ²O′′,O′′′-[aqua(4,4′-dimethyl-2,2′-bipyridine)copper(II)]-μ-fumarato-κO:κO′]

G.-Y. Dong, G.-H. Cui and J. Lin

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Bis(1,10-phenanthroline-κ²N,N′)(sulfato-κ²O,O′)cobalt(II) 1,2-ethanediol solvate

K.-L. Zhong, Y.-M. Zhu and W.-J. Lu

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μ-Oxalato-bis[chlorotripyridinemanganese(II)] pyridine disolvate

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(3,5-Dimethylpyridine)bis(tri-tert-butoxysilanethiolato)cadmium(II)

A. Dołęga, J. Chojnacki, A. Konitz, W. Komuda and W. Wojnowski

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[2,6-Bis(8-quinolyloxymethyl)pyridine]dinitratocadmium(II)

C.-J. Li, J.-M. Dou, D.-C. Li and D.-Q. Wang

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Pentacarbonyl-1κ²C,2κ³C-(μ-ethyl 3-mercaptopropionato-1κS:2κS)(μ-4-methylbenzoyl-1κO:2κC)(triphenylphosphine-1κP)diiron(Fe—Fe)

J.-T. Liu, Y.-C. Du, Y.-J. Mao, L. Zhang and Y.-L. Wu

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Tri-n-butyl(5-chloro-6-hydroxypyridine-3-carboxylato)tin(IV)

F.-H. Li, H.-D. Yin, G. Li and D.-Q. Wang

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[3,5-Dibromosalicylaldehyde (2-hydroxybenzoyl)hydrazonato-κ³O,N,O′]bis(pyridine-κN)zinc(II)

Y. Wu, S.-M. Shi, B. Jia and Z.-Q. Hu

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(Tricyclohexylphosphine)bis(tropolonato)palladium(II)

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Aquadibenzoato(2,2′-bipyridine)cadmium(II) monohydrate

L.-G. Zhu and M.-L. Hu

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Dimethyl[2-oxido-1-benzaldehyde (2-thienylcarbonyl)hydrazonato]tin(IV)

S.-W. Chen and H.-D. Yin

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Hexaimidazolium tetrachloromanganate(II) hexachloromanganate(II)

H. Zhang, P. Chen and L. Fang

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organic compounds

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4-Methyl-N-(4-oxo-2-thioxoimidazolidin-3-yl)-1,2,3-thiadiazole-5-carboxamide

I. Wawrzycka-Gorczyca, A. Siwek and M. Dobosz

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3-Phenoxy-1,4-diphenylazetidin-2-one

M. Akkurt, S. Karaca, A. A. Jarrahpour, D. Khalili and O. Büyükgüngör

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3-(Hydroxydiphenylmethyl)-2-(methoxymethoxy)benzaldehyde

W.-Z. Chen, Q.-L. Zeng, H. Fang, Y.-X. Gao and Y.-F. Zhao

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(E)-4-(4-Hydroxy-3-methoxyphenyl)but-3-en-2-one

S.-F. Wang, L.-J. Zhou and X. Yang

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(Z)-4-Anilinopent-3-en-2-one

F. Shaheen, L. Marchio, A. Badshah and M. K. Khosa

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2-(4-Hydroxystyryl)-1-methylpyridinium p-toluenesulfonate

S. Chantrapromma, P. Ruanwas, B. Jindawong, I. A. Razak and H.-K. Fun

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Bis[2-(4-phenyl-1H-1,2,3-triazol-1-yl)ethyl] benzene-2,4-dicarboxylate

X.-R. Zhang, S.-S. Zhang, M.-H. Xu and X.-M. Li

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2-(1,3-Benzothiazol-2-yl)quinolin-8-ol

L. E. da Silva, A. C. Joussef, S. Foro and B. Schmidt

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L-Tyrosine n-butyl ester

S.-S. Qian, H.-L. Zhu and E. R. T. Tiekink

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Ethyl 9-dicyanomethylene-2,5,7-trinitrofluorene-4-carboxylate

A. S. Batsanov and I. F. Perepichka

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(3S,4S)-4-(Cyclopropylcarbonyl)-3-[(1R)-1-hydroxyethyl]azetidin-2-one

L.-J. Wang, Z.-D. Zhang, J.-F. Zheng, H. Fang and L.-R. Jin

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1-Phenyl-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

J.B.-J. Teh, P. S. Patil, H.-K. Fun, I. A. Razak and S. M. Dharmaprakash

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3-(3-Bromophenyl)-1-phenylprop-2-en-1-one

S.-L. Ng, P. S. Patil, I. A. Razak, H.-K. Fun and S. M. Dharmaprakash

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3-(4-Methoxyphenyl)-1-(4-nitrophenyl)prop-2-en-1-one

P. S. Patil, J.B.-J. Teh, H.-K. Fun, I. A. Razak and S. M. Dharmaprakash

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(E)-2-Benzoyl-4-[(4-methylphenyl)diazenyl]phenol

O. Gonca, I. Şamil, C. Albayrak and A. Erbil

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Bis(2,6-dimethylpyridyl)iodonium dibromoiodate

A. S. Batsanov, A. P. Lightfoot, S. J. R. Twiddle and A. Whiting

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5-Mesylmethoxy-1-(4-nitrophenyl)tetrazole

A. S. Lyakhov, N. G. Egorova, T. V. Artamonova, P. N. Gaponik and G. I. Koldobskii

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2-(Carboxymethyl)-4,6-dimethoxybenzoic acid

G. Qadeer, N. H. Rama and Q.-S. Li

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2,2-Dimethyl-1,4-dihydro-2H-3,1-benzoxazine

M. Odabaşoğlu, O. Özdamar and O. Büyükgüngör

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cis-anti-cis-Dicyclohexyl-18-crown-6–thiacetazone–methanol (1/2/2)

M. S. Fonari, E. V. Ganin, Y. A. Simonov and W.-J. Wang

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N,N-Dibenzyl-3-nitrobenzenesulfenamide

I. Brito, M. López-Rodríguez, D. Vargas and Y. León

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1-Acetyl-3,3-bis[3-(2-methylphenyl)-1,2,4-oxadiazol-5-yl]-1H-indolin-2(3H)-one

X.-C. Yan, H.-B. Wang and Z.-Q. Liu

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(17S)-2α,3α,18β,23,24-Pentahydroxy-19(18→17)-abeo-28-norolean-12-en-21-one from the rhizome of Phlomis umbrosa

P. Liu, W. Qiao, W. Jia, J. Teng and H.-Q. Duan

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5-Nitro-1-(2-piperidinoethyl)-1H-benzimidazole

M. Akkurt, S. O. Yıldırım, H. Küçükbay, N. Şireci and H.-K. Fun

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tert-Butyl (S)-N-[(S)-1-(oxiranyl)ethyl]carbamate

R. A. Toscano, B. Ortiz, R. Sánchez-Obregón, F. Walls and F. Yuste

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3,7,7a-Tri-epi-casuarine pentaacetate

F. Punzo, D. J. Watkin, J. Van Ameijde, G. Horne, G. W. J. Fleet, M. R. Wormald and R. J. Nash

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4-[(1,3-Dioxo-2-azaspiro[4.5]decan-2-yl)amino]benzoic acid

A. Dzierżawska-Majewska, J. Karolak-Wojciechowska and J. Obniska

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(1,3-Dioxan-2-ylmethyl)triphenylphosphonium bromide monohydrate

Y.-Z. Wu, H.-Y. Li and W.-T. Yu

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2-(2,4-Dichlorophenyl)-5-methyl-4-(2-nitrophenylsulfonyl)-2H-1,2,4-triazol-3(4H)-one

L. Wang, B.-L. Wang, Z.-M. Li and H.-B. Song

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(Z)-5-Amino-2-dibenzylamino-1-phenyl-6-(2-pyridyl)hex-4-en-3-one

J. Meng, J.-F. Zheng, H. Fang and L.-R. Jin

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1-Benzoyl-3-(4-cyano-5-methylsulfanyl-1H-pyrazol-3-yl)thiourea

L.-R. Wen, M. Li, J.-X. Zhou and P. Liu

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(E)-1-Ethoxycarbonyl-2-[(2-hydroxy-1-naphthyl)(phenyl)methyliminio]propan-1-ide

J.-H. Li and C.-P. Lin

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12-Methoxy-15-(1-pyrrolidino)podocarpa-8,11,13-triene-15-one

R. J. Butcher, O. Bakare and N. J. John

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The second orthorhombic polymorph of zwitterionic metanilic acid at 130 K

G. Smith, U. D. Wermuth, D. J. Young and J. M. White

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6-Methyl-2-[2,2,6,6-tetramethyl-5-(2-pyridyl)hepta-3,4-dien-3-yl]pyridine

J. Averbeck, M. Schürmann, H. Preut and N. Krause

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1-(1-Hydroxy-2-naphthyl)ethanone

O. Büyükgüngör and M. Odabaşoğlu

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Surprising orientation in ring synthesis of 3,5-dimethylpyrazin-2(1H)-one

M. Helliwell, Y. Yun and J. A. Joule

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A monoclinic polymorph of 25,27-bis(benzyloxy)-26,28-dihydroxycalix[4]arene

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Triamcinolone acetonide methanol 0.67-solvate at 170 K

I. Jeß and C. Näther

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4-Benzoyl-5-(4-chlorophenyl)-2-(methylsulfanyl)-1H-imidazole

D. V. Albov, V. B. Rybakov, E. V. Babaev and A. A. Tsisevich

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A pentacycloundecane dimer

H. G. Kruger, M. Rademeyer and R. Ramdhani

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4-N-Acetylamino-5-[N-acetyl-N-(tetra-O-acetyl-β-D-glucopyranosyl)amino]-1,3-dimethyluracil

A. Sánchez Rodrigo, M. Nogueras Montiel, J. Cobo, J. N. Low and C. Glidewell

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2-(p-Tolyl)-1,3,2-benzodioxaborole

G. Bramham, A. S. Batsanov, T. B. Marder and N. C. Norman

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Verticillin chloroform solvate

F. Liu, S. Wu, Y. Chen, L. Yang and P. Wu

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2,5-Di-O-acetyl-3-C-methyl-D-lyxono-1,4-lactone

R. Bream, D. Watkin, R. Soengas, V. Eastwick-Field and G. W. J. Fleet

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N,N-Dimethyl-1-phenylsulfonyl-1H-pyrrole-3-sulfonamide

D. A. Grossie, D. J. Malwitz and D. M. Ketcha

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ortho-Bis(dimethylsilyl)hexamethyldecasilasesquioxane

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Cyclopent-3-ene-1,1-dicarboxylic acid

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4-Ethoxycarbonyl-3-furoic acid

A. Parkin, M. Adam, S. M. Harte, J. L. Kennedy and C. C. Wilson

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Ethyl (3,4,5-tribromo-1H-pyrrole-2-carboxamido)acetate

X.-C. Zeng and J.-X. Meng

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1,2-Difluorophenyl 4-vinylphenyl sulfone

A. P. Purdy, S. K. Jarchow-Choy, R. D. Gilardi and R. J. Butcher

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(3,6-Dibromo-9H-carbazol-9-yl)(phenyl)methanone

X.-M. Duan, W.-S. Xie, P.-M. Huang, J.-S. Li and P.-W. Zheng

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3-Methyl-1-(3-methylpyridinium-4-yl)pyridinium dichloride monohydrate

N. F. Sciortino and C. J. Kepert

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4-(2-Naphthoxy)phthalonitrile

R. Ustabaş, U. Çoruh, N. Akdemir, E. A~gar and H. Kalkan

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Cocrystallized 1,2-dibromo-4,5-dimethyl-3-nitrobenzene and 1,2-dibromo-4,5,6-trimethyl-3-nitrobenzene

J. M. S. Skakle, B. Gojdka and J. L. Wardell

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[2-(3-Fluoropyridinium-1-yl)-1-hydroxy-1-phosphonoethyl]phosphonate

R. Cao, M. P. Hudock, Y. Zhang, S. R. Wilson and E. Oldfield

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[2-(Dimethylsulfonio)-1-hydroxy-1-phosphonoethyl]phosphonate monohydrate

Y. Zhang, R. Cao, M. P. Hudock, S. R. Wilson and E. Oldfield

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2′-Acetyl-2-hydroxynaphthohydrazide

M.-L. Liu, J.-M. Dou, D.-C. Li and D.-Q. Wang

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10-(4-Bromostyryl)anthracene

J.-Y. Wu, L. Li and L. Tian

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Bis(9-ethylcarbazol-3-yl)methane

E. Asker and J. Masnovi

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N,N′,N′′-Tribenzyloxydicarbonimidic diamide

I. Đilović, D. Matković-Čalogović, I. Kos, M. Biruš and M. Jadrijević Mladar-Takač

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16-Cyano-13α-(5-methyl-1,3,4-oxadiazol-2-yl)-13,16-seco-17-norandrost-4-en-3-one

T. V. Sundar, V. Parthasarathi, R. Bansal, K. Ravikumar and B. Sridhar

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2-(4-Methoxyphenoxy)-1,9-diphenyl-1,9-dihydropurin-6-one

N.-Y. Huang, M.-W. Ding, Z.-G. Luo, N. Zuo, X.-H. Zeng and H.-W. He

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3-(1H-Indol-3-yl)-2-[3-(4-methoxybenzoyl)thioureido]propionic acid

N. Ngah, N. Dariman and B. M. Yamin

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2-(2,4-Dichlorophenoxy)-N-(4,6-dimethoxypyrimidin-2-yl)propionamide

G.-H. Liu, Y.-N. Xue, L.-Z. Yang, M. Yao and S.-J. Xue

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2-(1-Phenylsulfonyl-1H-indol-3-yl)-1,2-dihydronaphthalen-1-ol

C. Dockendorff, M. Lautens and A. J. Lough

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3-(1,3-Benzodioxol-5-yl)-1-(4-methoxyphenyl)prop-2-enone

I. Vencato, C. K. Z. Andrade, W. A. Silva and C. Lariucci

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Diaminopyrimidinium squarate 1.394-hydrate

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2-(1H-1,2,3-Benzotriazol-1-yl)-1-benzoylethyl 2-chlorobenzoate

J. Wan, Z.-Z. Peng, X.-M. Li and S.-S. Zhang

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Bis(2-azidoethyl) isophthalate

X.-R. Zhang, S.-S. Zhang, M.-H. Xu and X.-M. Li

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[4-(2,3-Dichlorophenyl)piperazin-1-yl][2-(2-methoxyphenylsulfanyl)phenyl]methanone

J.-C. Chu, Z.-H. Shang, X.-Q. Zhou and D.-Z. Liu

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6,6-Dithiobis(6,7-dihydro-5H-pyrazolo[1,2-a][1,2,4]triazolium) dichloride methanol solvate dihydrate

B.-Z. Song, J. Song, G.-C. Wang and W.-D. Wang

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Glycyl-L-proline hemihydrate at 298 K

S. A. Moggach, S. Parsons and L. Sawyer

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Redetermination of 5-fluorocytosine monohydrate

G. Portalone and M. Colapietro

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1,5-Bis[(1E)-(2-methoxyphenyl)methylene]thiocarbonohydrazide ethanol solvate

X.-N. Fang, Y.-P. Xu, X.-F. Guo and X.-R. Zeng

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[1-Hydroxy-1-phosphono-2-(trimethylphosphonium-1-yl)ethyl]phosphonate monohydrate

R. Cao, M. P. Hudock, Y. Zhang, S. R. Wilson and E. Oldfield

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Ethylenediammonium disaccharinate

Z.-L. Wang, L.-H. Wei, M.-X. Li and J.-Y. Niu

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1-Benzoyl-3-(3-chlorophenyl)thiourea

M. K. Rauf, A. Badshah, U. Flörke and A. Saeed

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5-(5-Bromothiazol-2-ylaminomethylene)-2,2-dimethyl-1,3-dioxane-4,6-dione

L. E. da Silva, A. C. Joussef, C. R. Andrighetti-Fröhner, R. J. Nunes and A. J. Bortoluzzi

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Cylopentylamine monohydrate

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N,N′-Diphenylguanidinium phthalate

P. S. Pereira Silva, M. Ramos Silva, A. Matos Beja and J. A. Paixão

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2,6-Dichlorobenzamide

M. K. Rauf, A. Badshah, M. Bolte and A. Saeed

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4-(4-Methoxybenzoyl)-2,2-dimethyl-5-phenylamino-2,3-dihydro-1,3,4-thiadiazole

M. S. M. Yusof, N. A. Tajuddin, A. S. Mardi and B. M. Yamin

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8′-Methoxy-3H-spiro[1-naphthofuran-2,2′-chroman]

G. R. Clark, K. Y. Tsang and M. A. Brimble

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Methyl (E)-2-cyano-3-(1H-indol-3-yl)acrylate

V. N. Sonar, S. Parkin and P. A. Crooks

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Bis(2-azidoethyl) terephthalate

X.-R. Zhang, S.-S. Zhang, M.-H. Xu and X.-M. Li

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1-(4-Chlorobenzoyl)-2-(1H-1,2,4-triazol-1-yl)ethyl morpholine-4-carbodithioate

Z.-Y. Wang, J. Wan, X.-M. Li, C.-L. Li and S.-S. Zhang

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2′,7′-Bis(4-methoxyphenyl)spiro[cyclopropane-1,9′-9H-fluorene]

Z.-X. Wang, H.-Y. Lin and P. Lu

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Sumatriptan, an antimigraine drug

K. Ravikumar, B. Sridhar and H. Krishnan

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Methyl 1,6-dimethyl-4-(3-nitrophenyl)-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

J.-J. Li, L. Jiang, X.-P. Wu and W.-K. Su

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Ethyl 2-(5,1′,5′-trimethyl-3,3′-bi-1H-pyrazol-1-yl)acetate

A. Attayibat, S. Radi, A. Ramdani, D. Eddike, M. Tillard and C. Belin

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(Z)-6-[(2-Methoxyphenylamino)methylene]-4-methylcyclohexa-2,4-dien-1(2H)-one monohydrate

M. Odabaşoğlu, C. Albayrak and O. Büyükgüngör

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N,N′-Bis(3-nitrophenyl)isophthalamide tetrabutylammonium chloride

M. E. Light, P. A. Gale and K. Navakhun

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2-(1H-1,2,3-Benzotriazol-1-yl)-1-benzoylethyl 2,4-dichlorobenzoate

J. Wan, X.-M. Li, Z.-Z. Peng and S.-S. Zhang

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4′-(4-Methoxyphenyl)-3′-phenylspiro[1H-isothiachroman-3,5′-isoxazolidin]-4(2H)-one

B. Brahim, K. Abdelali, B. L. Najib, B. El Bali and M. Bolte

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N,N′-Bis(3,5-dimethyl-1H-pyrazol-1-ylmethyl)piperazine

E. F. Abdeljalil, B. L. Najib, K. Abdelali, B. El Bali and M. Bolte

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9,9-Bis(ethoxycarbonylethyl)-9H-fluorene

W.-B. Hu, H.-X. Liu, D.-T. Tian, C.-M. Liu and Z.-L. Liu

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5-Hydroxy-4′,6,7-trimethoxyflavone

M. S. Ali, S. Ali, S. Anjum and W. Ahmad

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11-Phenyl-7,8,9,10,10a,11,12,13,14,15-decahydro-5H-3,1-benzoxazino[2,1-e]acridine

V. A. Kaminskiia, O. Yu. Slabkoa, A. V. Kachanova, A. V. Gerasimenko and S. W. Ng

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Butyl 3-(3,4-dihydroxyphenyl)prop-2-enoate

C.-N. Xia, W.-X. Hu and W. Zhou

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Cimicidol-3-one: a cycloartenol triterpenoid from the rhizomes of Cimicifuga racemosa

C. Dan, K. Yu, S. Peng, Y. Zhou and L. Ding

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A naphthalene–thiophene–naphthalene diazomethine triad solvated with dichloromethane

W. G. Skene and S. Dufresne

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4-Amino-1-(4-nitrobenzyl)pyridinium bromide

T. V. Sundar, V. Parthasarathi, K. Ravikumar, P. Venkatesan and M. Nallu

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(E,E)-1,8-Dioxacyclotetradeca-3,10-diene-2,9-dione

B. Samas, D. A. Pflum and R. W. Coscia

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3-Chloroacetophenone 2,4,6-trinitrophenylhydrazone

S. Shan, Z. Fan and D.-J. Xu

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4-Methylacetophenone [(2-methyl-4-nitro-1H-imidazol-1-yl)acetyl]hydrazone

S. Balamurugan, A. Thiruvalluvar and B. Kalluraya

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3-Benzotriazol-1-yl 5-methyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

L.-Q. Jiang and F.-X. Sun

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Methyl {2-[3-(4-bromophenyl)-1,2,4-oxadiazol-5-ylmethoxy]phenyl}acetate

Z.-Q. Liu, H.-B. Wang, Y.-Q. Pu and X.-C. Yan

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9,9′-Diethyl-3,3′-di-9H-carbazolyl

E. Asker and J. Masnovi

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1,2-Bis(2-ethyl-5-hydroxymethyl-3-thienyl)-3,3,4,4,5,5-hexafluorocyclopent-1-ene, a new photochromic diarylethene compound

T.-S. Yang, S.-Z. Pu, F.-S. Luo and J.-K. Xu

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Adamantane-1,2-diol

M. A. Myint, J. R. Price and E. W. Tan

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2-(3-Bromo-4-methoxyphenyl)imidazo[1,2-a]pyridine

G.-Y. Duan, C.-B. Tu, Y.-W. Sun, D.-T. Zhang and J.-W. Wang

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A proton transfer compound: propane-1,3-diaminium–pyridine-2,6-dicarboxylate–pyridine-2,6-dicarboxylic acid–water (2/2/2/5)

H. Aghabozorg, M. Ghadermazi and F. Ramezanipour

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3,4,4-Trichloro-1-[4-(2-fluorophenyl)piperazinyl]-1-(n-hexadecylsulfanyl)-2-nitrobuta-1,3-diene

C. Ibis, M. C. Sayil and F. Ozkok

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(2RS,3SR,5RS,6SR)-Bicyclo[2.2.1]heptane-2,3,5,6-tetryl tetraacetate

R. Ustabaş, U. Çoruh, M. Yavuz, E. Salamci and E. M. Vázquez-López

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6-Acetyl-2-(N-methylamido)pyridine

B.-Y. Su, J.-S. Zhao and S. W. Ng

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3,6-Dibromo-9-(4-pyridylmethyl)-9H-carbazole

X.-M. Duan, P.-M. Huang, J.-S. Li, P.-W. Zheng and X.-J. Wang

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2-Methyl-6-nitroaniline

Z.-L. Jing, Q.-Z. Zhang, J. Jia and M. Yu

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6-(Acetoxymethyl)-5-chloro-2-[(2R,3R,4R,5S)-3,4-diacetoxy-2,5-bis(chloromethyl)-2,3,4,5-tetrahydrofuran-2-yloxy]-3,4,5,6-tetrahydro-2H-pyran-3,4-diyl diacetate toluene solvate

H.-L. Wen, Z.-J. Fang, Z.-S. Wu and M.-Y. Xie

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Bis(3-ammoniopropyl)ethylenediaminium bis(squarate)

H. Paşaoğlu and O. O. Yilan

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2,2-Dimethyl-5-[(4-methylthiazol-2-ylamino)methylene]-1,3-dioxane-4,6-dione

L. E. da Silva, A. C. Joussef, C. R. Andrighetti-Fröhner, C. M. O. Simões and A. J. Bortoluzzi

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(E)-4,4′-Diazastilbene–4,4′-oxydibenzoic acid (1/1)

Z.-C. Ma, A.-Q. Ma and G.-P. Wang

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6-Chloro-3-chloromethylene-7-methyl-1,2,4-triazolo[4,3-b]pyridazine

Anna Katrusiak and Andrzej Katrusiak

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Pamoic acid determined from powder diffraction data

D. A. Haynes, J. Van de Streek, J. C. Burley, W. Jones and W. D. S. Motherwell

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2-Aminopyridinium 5-formylsalicylate

S.-L. Li, J.-F. Ma and G.-J. Ping

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2-(2-Methoxyphenylsulfanyl)benzoic acid

A.-J. Li, M.-L. Tao, J. Ma, X.-Q. Zhou and D.-Z. Liu

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L-Histidinium tetrafluoroborate

S. Gokul Raj, G. Ramesh Kumar, T. Raghavalu, R. Mohan and R. Jayavel

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3-(1-Methyl-1H-pyrrole-2-carboxamido)propanoic acid

P.-R. Liu, X.-C. Zeng and S.-H. Xu

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2-Amino-4-(2-chlorophenyl)-7,7-dimethyl-1-(4-methylphenyl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carbonitrile

H. Jiang, X.-S. Wang, M.-M. Zhang, Y.-L. Li and D.-Q. Shi

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(2′′S,5′′R,7′′S)-2-[2′-(2′′-Methyl-1′′,6′′-dioxaspiro[4.5]dec-7′′-yl)ethylsulfonyl]-1,3-benzothiazole

G. R. Clark, J. E. Robinson and M. A. Brimble

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4,5-Dimethyl-1,2-bis(quinoline-2-carboxamido)benzene

S. H. Nam, B. K. Park, C. Kim and Y. Kim

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Methyl 4-bromobenzoate

M. Bolte and J. Wissler

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Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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Journal news

Acta E is now included in the Thomson Reuters Emerging Sources Citation Index.

Editorial Advisory Board

S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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